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117results about How to "Improve interface effect" patented technology

Carbon fiber composite material for fused deposition 3D printing and preparation method thereof

The invention provides a carbon fiber composite material for fused deposition 3D printing and a preparation method thereof. The preparation method comprises the following steps: subjecting chopped carbon fibers to a liquid phase oxidation treatment and a coupling grafting treatment, then evenly mixing 10 to 30 wt% of chopped carbon fiber, 68 to 88 wt% of dried thermoplastic resin, 0 to 0.5 wt% of color master batch, 0.1 to 0.5 wt% of antioxidant, and 0.1 to 0.5 wt% of processing aid, heating, and extruding the mixture into filaments by a double screw extruder so as to obtain the carbon fiber composite material for fused deposition 3D printing. Compared with the prior art, the products made of the provided carbon fiber composite material has the advantages that impact strength, bending strength, and tensile strength are all prominently improved.
Owner:QINGDAO UNIQUE PRODS DEV

Organic-inorganic compound modified waterborne acrylic epoxy ester resin and preparation method thereof

The invention belongs to the field of waterborne coatings, and relates to an organic-inorganic compound modified waterborne acrylic epoxy ester resin and a preparation method thereof. The organic-mineral compound modified waterborne acrylic epoxy ester resin is synthesized by using the following raw materials in parts by weight: 30-70 parts of an epoxy ester, 5-50 parts of an acrylic monomer and 5-25 parts of silica sol, wherein the epoxy ester is prepared by carrying out catalytic reaction on 40-70 parts of an epoxy resin and 20-60 parts of an unsaturated fatty acid; the acrylic monomer comprises 20-60 parts of a vinyl monomer and 40-70 parts of an acrylic monomer; and the silica sol is obtained by reacting 10-50 parts of an organosilicone intermediate, 5-50 parts of a silane coupling agent, 20-70 parts of a cosolvent, 0.2-5 parts of a pH regulator and 5-15 parts of water. The nano silicon sol improves the tolerance and dryness of films; secondary crosslinking is formed along with pH value changes, so that the crosslinking density after film formation is increased; a structure taking the nano silicon sol as a core and taking an organic resin as a shell increases the stability of silicon hydroxyl; and the waterborned epoxy ester resin reduces the VOC content.
Owner:BEIJING JINHWEILI APPLIED CHEM PROD

Metal structure tungsten diselenide/redox graphene composite structure and preparation method thereof

The invention relates to a metal structure tungsten diselenide / redox graphene composite structure and a preparation method thereof. Firstly, a precursor aqueous solution of a WSE2 film is prepared; a monolayer graphene oxide aqueous solution and citric acid are added into the precursor aqueous solution of the WSE2 film to obtain a WSe2 / RGO precursor aqueous solution; then, after hydrothermal treatment at 165-180 DEG C, a thin-film metal structure tungsten diselenide / redox graphene composite structure is obtained on a polyethylene naphthol substrate inserted into the WSe2 / RGO precursor aqueous solution, and a precipitate in a residual solution after the hydrothermal treatment is filtered, washed and dried to obtain a powder metal structure tungsten diselenide / redox graphene composite structure. According to the invention, the preparation of metal structure tungsten diselenide can be realized through a one-step synthesis process through a hydrothermal method, and the preparation method is not only simple in process, but also has the excellent characteristics of low cost of used raw materials and equipment, low energy consumption, high efficiency and the like.
Owner:SHAANXI UNIV OF SCI & TECH

Method for forming shallow trench isolation structure

The invention discloses a method for forming a shallow trench isolation structure. The method comprises the following steps of: providing a substrate on which a gasket oxide layer and an etching stopping layer are formed sequentially, and forming a shallow trench in the substrate; forming an isolation medium layer which fills the shallow trench on the surfaces of the etching stopping layer and the gasket oxide layer; forming a first photoresist pattern on the surface of the isolation medium layer by using an active reverse mask; etching the isolation medium layer of partial thickness by using the first photoresist pattern as a mask; removing the isolation medium layer until the isolation medium layer is exposed out of the etching stopping layer by adopting a chemical mechanical polishing process after removing the first photoresist pattern; removing the etching stopping layer and the gasket oxide layer; forming a protection film which covers the isolation medium layer on the surface of the substrate; forming a second photoresist pattern on the surface of the protection film by using the active reverse mask; and removing the protection film until the protection film is exposed out of the substrate by using the second photoresist pattern as the mask to form a protection layer. A divot situation does not exist in the isolation of the shallow trench which is formed by the method.
Owner:SHANGHAI HUAHONG GRACE SEMICON MFG CORP

Preparation method for high-resistance inorganic-organic composite modified acrylic epoxy ester resin

The invention belongs to the field of water-based paints, and discloses a high-resistance inorganic-organic composite modified acrylic epoxy ester resin. The high-resistance inorganic-organic composite modified acrylic epoxy ester resin is synthesised from the following raw materials in parts by weight: 30-70 parts of epoxy ester, 5-50 parts of acrylic monomers and 5-25 parts of silica gel, wherein the epoxy ester is prepared by carrying out a catalytic reaction on 40-70 parts of epoxy resin and 20-60 parts of unsaturated fatty acid; the acrylic monomers comprise 20-60 parts of vinyl monomers and 40-70 parts of acrylic acid monomers; the silica gel is prepared by reacting 10-50 parts of an organic silicon intermediate, 5-50 parts of a silane coupling agent, 20-70 parts of a cosolvent, 0.2-5 parts of a pH value regulator and 5-15 parts of water; the nanoscale silica gel is capable of improving the resistance and dryness of a paint film; secondary crosslinking is formed along with the changes of a pH value, thus increasing the crosslinking density after film formation; the structure taking the nanoscale silica gel as a core and the organic resin as a shell is capable of improving the stability of silicon hydroxyl; the water-based epoxy ester resin is capable of reducing a VOC content.
Owner:BEIJING JINHWEILI APPLIED CHEM PROD

Preparation and application of in-situ polymerization coated modified silicon-based negative electrode material

ActiveCN113270586AAvoid uneven coating, increase of inactive substances, etc.Improve interface effectSecondary cellsNegative electrodesIn situ polymerizationPhysical chemistry
The invention discloses preparation and application of an in-situ polymerization coating modified silicon-based negative electrode material, the surface of a silicon-based material is coated with a composite coating layer of an inorganic matter and a polymer, and through the effect of a deep eutectic solvent, the silicon-based negative electrode material enables monomers of the polymer to be subjected to in-situ polymerization reaction on the surface of the silicon-based material to obtain a composite coating layer in which inorganic matters are uniformly distributed in the polymer; the inorganic matter is lithium salt, and the thickness of the composite coating layer is 5-15 nm. According to the composite coating layer, an organic-inorganic composite coating layer is constructed on the surface of the material in an in-situ polymerization manner of a polymeric monomer doped with an inorganic substance. According to the negative electrode material, in the initial lithiation/delithiation process, a layer of organic-inorganic composite artificial solid electrolyte interface (SEI) is formed in situ, the structural integrity in the lithium intercalation/delithiation process is maintained, the irreversible consumption of lithium ions is reduced due to the addition of the lithium-rich inorganic matter, and the first coulombic efficiency and the cycle stability of the negative electrode material are improved.
Owner:BEIJING IAMETAL NEW ENERGY TECH CO LTD

Preparation method of acid and alkali resistant anti-puncture anti-seepage material

The invention discloses a preparation method of an acid and alkali resistant anti-puncture anti-seepage material, and belongs to the technical field of preparation of environmental protection materials. Since fumed silica particles have large surface defects, many unpaired atoms and high surface activity, a large interfacial effect is generated on the surface of double-layered glass wool, and thefumed silica is dispersed in the gap of a polyester molecular chain, so that the elasticity of polyester resin and a fumed silica system is improved and resistant to plant root tip puncture. Quick lime reacts with water to form calcium hydroxide that reacts with sulfate in the manganese residue to form unite particles in the anti-seepage material. The heavy metal ions in the clay slurry componentmanganese slag are mostly in the form of sulfate, and the heavy metal ions of a landfill can be in complexing with modified polyester, hydrated silicate is insoluble under alkaline conditions, a claylayer in the anti-seepage material can be used as a protective film to make the clay slurry have acid and alkali resistance, so that the material has broad application prospects.
Owner:FOSHAN LINGCHAO NEW MATERIAL CO LTD

Preparation method of in-situ polymerized type halogen-free flame retardant nylon material for selective laser sintering

A preparation method of an in-situ polymerized type halogen-free flame retardant nylon material for selective laser sintering comprises the following steps: carrying out in-situ polymerization of nylon monomers, melamine, cyanuric acid, a light absorbent, a molecular weight regulator and a first antioxidant to obtain a halogen-free flame retardant nylon material; and crushing the halogen-free flame retardant nylon material to obtain a halogen-free flame retardant nylon powder. The prepared in-situ polymerized type halogen-free flame retardant nylon material for selective laser sintering not only makes a flame retardant chemically bonded into the nylon monomers or uniformly dispersed in the nylon monomers, so as to achieve a good flame retardant effect, namely meet the requirements of the aviation flame retardant standard FAR25.853; and because the light absorbent is added in the polymerization process and the light absorbent can be uniformly dispersed in a base material, the laser energy in the selective laser sintering process can be better absorbed, melt processing of materials can be effectively promoted, and thus the utilization rate of laser energy and the mechanical performance of sintering parts are improved.
Owner:HUNAN FARSOON HIGH TECH CO LTD

Silicon-based negative electrode material and preparation method and application thereof

The invention relates to a silicon-based negative electrode material and a preparation method and application thereof. The silicon-based negative electrode material comprises a silicon-based inner core and a shell coating the surface of the silicon-based inner core. The shell comprises a first coating material and a second coating material, wherein the first coating material is composed of a compound of nitrogen-doped graphene, a nitrogen-doped hydrogen-containing lithium titanium oxide compound and nitrogen-doped hexagonal phase tungsten oxide, and the second coating material is composed of amesoporous carbon layer. The preparation method comprises the following steps: (1) dispersing a silicon-based material and a first coating material in a solvent to obtain a dispersion liquid, and carrying out spray drying to obtain an inner core material; (2) dispersing a triblock copolymer, amino alcohol and the core material in the step (1) in a solvent to obtain a dispersion liquid; and (3) adding dopamine into the dispersion liquid obtained in the step (3), carrying out a polymerization reaction, and then carbonizing in an inert atmosphere to obtain the silicon-based negative electrode material. The structure and the cycling stability of the silicon-based negative electrode material are obviously improved, and the cycling performance of the silicon-based negative electrode material isalso obviously improved.
Owner:LANGFANG GREEN IND TECH CENT +1

Bifunctional interface lithium ion battery nickel-rich single crystal positive electrode material and preparation method thereof

The invention provides a bifunctional interface lithium ion battery nickel-rich single crystal positive electrode material and a preparation method thereof. According to the method, a certain amount of aluminum source and phosphate are added into a nickel-rich single crystal positive electrode material, and a bifunctional coating layer of AlPO4 and Li3PO4 is formed while surface residual alkali (Li2CO3/LiOH) is consumed. By controlling the adding amount of the aluminum source and the phosphate and adjusting and controlling the adding mode and the calcining method, the direct contact between the active material and an electrolyte can be reduced, gas production is inhibited, and the thermal stability of the material is improved; and the transmission of ions between the positive electrode and the electrolyte can be accelerated, the stress change in a charging and discharging process is relieved, and the rate capability of the material is improved. According to the method, a bifunctional interface modification layer is obtained, the electrochemical performance of the nickel-rich single crystal positive electrode material is improved through the synergistic effect of the bifunctional interface modification layer; operation is easy and convenient; and raw materials are cheap and easy to obtain. The method is suitable for large-scale commercialization of the nickel-rich single crystal positive electrode material.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Micro hole-aluminum silicate fiber sandwich type composite sound absorption board

The invention discloses a micro hole-aluminum silicate fiber sandwich type composite sound absorption board and belongs to the field of noise control devices. The micro hole-aluminum silicate fiber sandwich type composite sound absorption board comprises a micro perforation board body, an aluminum silicate fiber mat and an aluminum silicate fiber board body which are sequentially arranged from outside to inside. The micro perforation board body is provided with a plurality of penetrating holes, and the periphery of the inner surface of the micro perforation board body is provided with baffles to form a first groove, and the first groove is matched with the aluminum silicate fiber mat. The periphery of the inner surface of the micro perforation board body is provided with a plurality of protrusions, and the periphery of the aluminum silicate fiber board body is provided with second grooves matched with the protrusions. The periphery of the inner surface of the aluminum silicate fiber board body is provided with a frame. According to the sound absorption board, through hole diameter resistance, material sound absorption, the interfacial effect between high-low volume weight materials and the like, the sound absorption frequency band of the sound absorption board is greatly widened, the sound absorption coefficient of the sound absorption board is 0.87-0.95, the compressive strength is high, and the fireproof grade is A; and the sound absorption board is suitable for absorbing of low-frequency electromagnetic noise of equipment such as a transformer and an electric reactor and high-frequency aerodynamic noise of a cooling fan.
Owner:STATE GRID HENAN ELECTRIC POWER ELECTRIC POWER SCI RES INST +3
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