6240 results about "Pyrrolidinones" patented technology

The invention relates to the preparation of a hydrogel surface useful in the formation and manipulation of arrays of molecules, particularly polynucleotides and to the chemical modification of these and other arrays. In particular, the invention relates to a method of preparing a hydrogel immobilised to a solid support comprising polymerising on the support a mixture of a first comonomer which is acrylamide, methacrylamide, hydroxyethyl methacrylate or N-vinyl pyrrolidinone and a second comonomer which is a functionalised acrylamide or acrylate.

The invention relates to novel crosslinkable copolymers which are obtainable by (a) copolymerizing at least two different hydrophilic monomers selected from the group consisting of N,N-dimethyl acrylamide (DMA), 2-hydroxyethyl acrylate (HEA), glycidyl methacrylate (GMA), N-vinylpyrrolidone (NVP), acrylic acid (AA) and a C₁-C₄-alkoxy polyethylene glycol (meth)acrylate having a weight average molecular weight of from 200 to 1500, and at least one crosslinker comprising two or more ethylenically unsaturated double bonds in the presence of a chain transfer agent having a functional group; and (b) reacting one or more functional groups of the resulting copolymer with an organic compound having an ethylenically unsaturated group.

Processes for the production of metal nanoparticles. In one aspect, the invention is to a process comprising the steps of mixing a heated first solution comprising a base and/or a reducing agent (e.g., a non-polyol reducing agent), a polyol, and a polymer of vinyl pyrrolidone with a second solution comprising a metal precursor that is capable of being reduced to a metal by the polyol. In another aspect, the invention is to a process that includes the steps of heating a powder of a polymer of vinyl pyrrolidone; forming a first solution comprising the powder and a polyol; and mixing the first solution with a second solution comprising a metal precursor capable of being reduced to a metal by the polyol.

The present invention provides an assembly for the preparation of a medical device having a porous coating comprising hydrogen peroxide. Particularly interesting medical devices are catheters (such as urinary catheters), endoscopes, laryngoscopes, tubes for feeding, tubes for drainage, guide wires, condoms, urisheaths, barrier coatings e.g. for gloves, stents and other implants, extra corporeal blood conduits, membranes e.g. for dialysis, blood filters, devices for circulatory assistance, dressings for wound care, and ostomy bags. The coating is in particular a hydrophilic coating formed from cross-linked polyvinylpyrrolidone. In one embodiment, the assembly holds a dry catheter element in one compartment of a package and an aqueous hydrogen peroxide solution in another compartment. The solution may also comprise stabilizers, e.g. chelators, and osmolality increasing agents. The catheter for insertion in the urethra is useful for the treatment, alleviation or prophylaxis of microbial infections such as urinary tract infections (UTI).

The invention discloses high-performance environment-friendly type water-borne polyurethane. The high-performance environment-friendly type water-borne polyurethane is mainly prepared from the following materials in parts by weight: 80-100 parts of polyester polyol, 20-56 parts of aliphatic diisocyanate, 3.5-10 parts of hydrophilic chain extender, 0-8 parts of micromolecule chain extender, 0.01-0.05 part of environment-friendly type catalyst, 5-30 parts of solvent with a low boiling point, 3-12 parts of neutralizer, 0-10 parts of post chain extender and 160-400 parts of deionized water. The invention further discloses a preparation method of the polyurethane. The polyurethane is free of toxic and harmful substances including an organic tin catalyst, N-methylpyrrolidone, a solvent with a high boiling point and the like, capable of satisfying the requirements of latest EU environmental standard rules, anti-yellowing, extremely good in water and heat resistance, good in adhesion resistant adhesion, strong in storage stability, good in gloss, high in solid content and excellent in comprehensive performance.

The invention discloses preparation and application of magnetic nano-composite material gamma-Fe2O3/PDA (Polydopamine)-GA (Gallic Acid). The preparation comprises the following steps of carrying out a hydrothermal reaction and calcinations to obtain a gamma-Fe2O3 nano particle carrier by taking FeCl3.6H2O with low price as an iron source, ethylene glycol (EG) as a reducing agent, polyvinylpyrrolidone (PVP) as a dispersing agent and a protective agent, and natrium aceticum (NaAc) as an alkali source; then wrapping a layer of polydopamine (PDA) in a buffer solution of tris (hydroxymethyl) aminomethane-hydrochloric acid (Tris-HCl) with pH of 8.5; and finally introducing gallic acid (GA) to an ethanol system by using 1-ethyl-(3-dimethylaminopropyl) carbodiimide hydrochloride and n-hydroxysuccinimide as cross-linking agents, wherein a specific synthetic schematic diagram is seen in attached drawing 1. Then the adsorption effects of the synthesized magnetic nano-particle on metal ions Cu<2+> and Pb<2+> are discussed, the detection effects of a glassy carbon electrode modified by the magnetic nano-particle on the metal ions Cu<2+> and Pb<2+> are researched. Results show that gamma-Fe2O3/PDA-GA has excellent detection and adsorption effects on heavy metal ions in a water environment.

The invention discloses a method for preparing poly(arylene ether nitrile) resin powder, and belongs to the technical field of high polymer materials. 2,6-dichlorobenzonitrile and aromatic dihydric phenol are taken as raw materials, 1-methyl-2-Pyrrolidinone is taken as a solvent, anhydrous potassium carbonate or anhydrous sodium carbonate is taken as a catalyst, and methylbenzene or dimethylbenzene is taken as a dehydrating agent; and the method comprises the following steps of: performing reflux reaction at the temperature of between 130 and 160 DEG C for 2 to 4 hours in a reactor, slowly evaporating out water and the dehydrating agent, and raising the temperature to 180-200 DEG C until a macromolecular rod-climbing phenomenon happens; adding the solvent into the reactor, and diluting the reaction products to the mass concentration of 2 to 15 percent; and adding a precipitator into the reactor, continuously stirring, performing centrifugal solid-liquid separation, washing the solid in acidic boiling water, filtering and drying to obtain the poly(arylene ether nitrile) resin powder. The prepared poly(arylene ether nitrile) resin powder has the characteristics of superfine granularity (reaching 100-400 meshes), uniform granularity, high purity, stable performance, and excellent electrical property, and can be widely applied in the fields such as electronics, precision machines, aerospace, new energy and the like.

The present invention relates to aqueous polyurethane dispersions that are free from N-methylpyrrolidone and other solvents and wherein the polyurethanes are the reaction products of A) a mixture of 25% to 90% by weight of 1-isocyanate-3,3,5,-trimethyl-5-isocyanatomethylcyclohexane (IPDI) and 10% to 75% by weight of 4,4′-diisocyanatodicyclohexylmethane, wherein the preceding percentages are based on the weight of component A), with B) one or more polyols having average molarcular weights (Mn) of 500 to 6000, C) one or more compounds which have at least one OH— or NH-functional group and contain a carboxyl and/or carboxylate group, wherein at least 50 mol % of the acid groups, based on the total moles of acid incorporated into the polyurethane, are incorporated by dimethylolpropionic acid, D) one or more polyols and/or polyamines having average molecular weights (Mn) of below 500, and E) optionally one or more monoalcohols and/or monoamines. The present invention also relates to a process for preparing the aqueous polyurethane dispersions and to the use of the polyurethane dispersions for preparing coatings or adhesives.

A purified cannabidiol (CBD) extract and/or cannabidiolic acid (CBDA) extract is isolated from industrial hemp and comprises less than 0.5 wt % organic impurities as measured by HPLC and ¹H NMR spectroscopy exhibits no detectable peak at 4.07 ppm as measured by ¹H NMR spectroscopy. The CBD and/or CBDA extract is in crystalline form. The CBD extract exhibits a melting point as measured by differential scanning calorimetry (DSC) of 69-70° C. Dry powder compositions comprise such extracts. Additional dry powder compositions comprise polyvinylpyrrolidone and an amorphous CBD extract. An adduct comprises CBD and/or CBDA bonded to a paramagnetic trivalent lanthanide (III) metal chelate.

The invention relates to a blocking remover of a gas well shaft. The blocking remover comprises, by weight, 5-25% of an alcohol ether compound, 0.5-10% of a dispersant, 1-10% of a cleaning agent, and 0.5-5% of chelating agent, with the balance being a nitrogen-containing polar solvent, wherein the nitrogen-containing polar solvent is one selected from N,N dimethyl formamide, N,N dimethyl acetamide, and N-methyl pyrrolidone, the alcohol ether compound is one selected from glycol-ether, glycol-propyl ether, glycol-butyl ether, and diglycol-ether, the disperant whose micelle particle size is from 20nm to 100nm is a middle-phase microemulsion-type dispersant mixed by kerosene, water, a surfactant and a cosurfactant, the cleaning agent is one selected from allene diamine, acetonitrile and pentylamine, and the chelating agent is one selected from sodium citrate and EDTA. The blocking remover has the advantages that corrosivity is weak, that the speed of dissolving blockage is fast, that the product performance is stable in high temperatures, and that the blocking remover can reduce damages caused by water locking and fouling in areas close to gas wells, and can recover the permeability of storing layers.

The present invention relates to an aligning agent for liquid crystal containing at least a polymer and solvent selected from polyamic acid and polyimide gained by dewatering closed-loop, the solvent contains: (A) a first solvent containing compound with formula (I); (B) a second solvent selected from at least one of N-methyl-2-pyrrolidone, gamma-butyrolactone, 1,3-dimethyl-2-imidazolone, N, N-dimethylformamide and N, N- dimethylacetylamide; and (C) a third solvent selected from at least one of butyl cellosolve, diacetone alcohol, carbonic sub-propyl ester, diethylene glycol diethyl aether and ethyl-3- oxethyl propionic ether. (In formula (I) the R respectively represents alkyl with 3 to 10 carbon atoms).