49results about How to "Technical parameters are easy to control" patented technology

The invention relates to a method for preparing a porous bone scaffold by laser and increasing mechanical and biological performances of the porous bone scaffold by adding zinc oxide with little amount, which belongs to the bone tissue engineering field. Aiming at uncontrollable performances of aperture distribution, shape, space direction and connectivity in the preparation method of a traditional bone scaffold, and aiming at the disadvantages of poor mechanical property and fast resolving rate existed in tricalcium phosphate (beta-TCP), the invention provides the method for preparing the porous bone scaffold by using a selective laser sintering (SLS) technology, and provides the method for increasing performance by adding zinc oxide (ZnO). The method for preparing the porous bone scaffold has the advantages that the porous scaffold which enables three-dimensional interconnection is prepared by SLS, zinc oxide with little amount is added for introducing into a liquid phase, the particles densification can be promoted, crystal grain is refined, and the mechanical performance is improved, simultaneously, cell compatibility is increased, the degradation rate is reduced, and the biological performance is increased, so that the interconnected porous beta-TCP bone scaffold with enhanced mechanical performance and good biological performance can be finally prepared. The method has the advantages of simple preparation technology, convenient operation, low cost, easy control of technical parameter and the like.

The invention discloses a method for preparing 4A zeolite by using fluorine-containing white residues through single-step crystallization. The method comprises the following specific steps of: simultaneously adding a sodium metaaluminate solution, a NaOH solution and a 4A zeolite crystallization guiding agent to the fluorine-containing white residues generated in a fluorine salt production process of aluminum and fluoride chemical industries according to a certain proportion, uniformly mixing in a reaction kettle, carrying out constant temperature crystallization for 3.0-3.5 hours at 75-85 DEG C and a stirring rate of 240-300r / min, ageing for 12-14 hours, filtering, washing and drying to obtain the 4A zeolite which is used for washing and is in line with the QB / I1768-2003 standard. The method has the technical characteristics that technological process is short, synthetic conditions are mild, the product quality is stable, and the problems of comprehensive utilization of the fluorine-containing white residues and secondary pollution of the fluorine-containing white residues to environments are successfully solved.

The invention relates to method for reinforcing and toughening an akermanite bone scaffold by utilization of nano titanium oxide power and for preparing a three-dimensional porous ceramic bone scaffold with a controllable micro-pore structure by utilization of the selective laser sintering technology. The problems of low toughness and poor intensity of biological ceramics and uncontrollable micro-pore structure of a prepared scaffold in a traditional porous scaffold preparation method are solved. The method is as follows: nano titanium oxide power is added into micron akermanite power, the composite power is mixed uniformly in a mechanical mixing method, and then the mixed power is placed in a selective laser sintering system and a porous akermanite bone scaffold is prepared by utilization of a rapid forming technology. The prepared porous scaffold has tough mechanical properties and an controllable micro-pore structure, and can meet the requirements of tissue-engineered bone research and application.