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49results about How to "Technical parameters are easy to control" patented technology

Method for extracting and preparing medlar leaf flavone

The invention relates to a method for extracting and preparing medlar leaf flavone. The method comprises the following steps of: (1) after picking and removing impurities manually, drying medlar leaves indoor to obtain a medlar leaf dry sample; (2) crushing the medlar leaf dry sample and screening the crushed medlar leaf dry sample to obtain medlar powder; (3) leaching the medlar powder by using ethanol to obtain leaching liquor; (4) grinding the leaching liquor by using a colloid grinder to obtain colloidal medlar leaf leaching solution; (5) homogenizing and separating the colloidal medlar leaf leaching solution to obtain liquid supernatant and filter residue; (6) removing impurities from the liquid supernatant by using a ceramic membrane to obtain filtrate; (7) adsorbing the filtrate by using weak-polarity macroporous adsorption resin and eluting the filtrate by using ethanol solution to obtain medlar leaf flavone-containing eluent; and (8) after concentrating and drying the medlar leaf flavone-containing eluent under a reduced pressure in a vacuum, obtaining the medlar leaf flavone powder. The method has low cost and high extraction rate; and the obtained medlar leaf flavone has stable properties, high content, and high biological activity of heart head blood-vessel disease resistance, cancer resistance, oxidation resistance and the like.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST

Method for preparing porous bone scaffold by laser and increasing performance by adding zinc oxide

The invention relates to a method for preparing a porous bone scaffold by laser and increasing mechanical and biological performances of the porous bone scaffold by adding zinc oxide with little amount, which belongs to the bone tissue engineering field. Aiming at uncontrollable performances of aperture distribution, shape, space direction and connectivity in the preparation method of a traditional bone scaffold, and aiming at the disadvantages of poor mechanical property and fast resolving rate existed in tricalcium phosphate (beta-TCP), the invention provides the method for preparing the porous bone scaffold by using a selective laser sintering (SLS) technology, and provides the method for increasing performance by adding zinc oxide (ZnO). The method for preparing the porous bone scaffold has the advantages that the porous scaffold which enables three-dimensional interconnection is prepared by SLS, zinc oxide with little amount is added for introducing into a liquid phase, the particles densification can be promoted, crystal grain is refined, and the mechanical performance is improved, simultaneously, cell compatibility is increased, the degradation rate is reduced, and the biological performance is increased, so that the interconnected porous beta-TCP bone scaffold with enhanced mechanical performance and good biological performance can be finally prepared. The method has the advantages of simple preparation technology, convenient operation, low cost, easy control of technical parameter and the like.
Owner:CENT SOUTH UNIV

Method of nanometer zirconia toughened titanium alloy orthopedics implant based on 3D printing

The invention discloses a preparation method of a nanometer zirconia particle toughened biological titanium alloy porous artificial implant. The preparation method is characterized by comprising the following steps: (1) preparation of nanometer / micron mixed powder: nanometer zirconia powder with a mass fraction of 0.5-8% is weighed and added in remained micron-grade titanium alloy powder, and the two powder is uniformly mixed by using a mechanical mixing method, wherein the particle size of the titanium alloy powder is 1-50 microns, and the purity is not lower than 99%; the size of the zirconia powder is 10-100 nm; and zirconia contains a yttrium oxide stabilizing agent with 1-5% of the mass of the zirconia powder; and (2) a matched porous artificial implant model is designed according to different personal demands by using three-dimensional design software; the designed three-dimensional data model is introduced in a computer for layering and slicing to obtain profile information of each layer; the mechanically mixed powder is paved on a forming cylinder by using a powder paving device; and the area selective melting formation is performed by using laser or electronic beams. The implant has the characteristics of good toughness and high biological compatibility.
Owner:SUZHOU CLOUDMPLANT MEDICAL TECH CO LTD

Method for producing dispersion strengthening copper alloy materials

InactiveCN1844426AEvenly distributedExcellent high temperature mechanicsIngotMaterials science
This invention relates to a method of producing the dispersion consolidating copper alloy material. It uses machinery alloyed to blend the metal oxidation powder and copper powder with a certain proportion, and then agglomerating them, then using water sealing heat extrusion to do cold plastic deformation processing to obtain the product.>The advantage of this invention is that it can make sure the quality of the copper alloy material, and the cost is low, the technique parameter is easy to control.
Owner:湘潭市电磁线厂有限公司

Technique for extracting titanium slag form red mud

A technical handling method of cuprum wires cross relates to the annealing process of cuprum wires cross and comprises the following steps: putting cuprum wires cross into a annealing furnace, pumping air in the furnace to form negative-pressure in the furnace, filling the furnace with carbon dioxide protective gas; performing a heating treatment of two stages under pressure, performing a gas releasing decompression processing between stages, then cooling-down slowly in the furnace for 0.3-1 hour, and opening the furnace to cool-down naturally to atmospheric temperature. Therefore, electrical soft wires cross through such annealing treatment has brightening surfaces and excellent finish, without greasy dirt or other soils; exhibits uniform flexibility and strong antioxidant ability, and can be stored for a long time.
Owner:GUIZHOU BRANCH CHINA ALUMINUM IND

Polysiloxane modified epoxy resin and preparation method thereof

The invention discloses polysiloxane modified epoxy resin and a preparation method thereof. The preparation method comprises the following steps: firstly mixing and dissolving epoxy resin and polysiloxane in an organic solvent, dropwise adding a catalyst at a temperature of 60-100 DEG C in a nitrogen environment, then carrying out stirring for reacting to obtain polysiloxane modified epoxy resin,removing unreacted polysiloxane after the reaction is finished, and carrying out reduced-pressure distillation to remove the organic solvent to obtain the pure modified resin. The polysiloxane modified epoxy resin prepared by the invention can be cured into a film at room temperature, the obtained coating has good flexibility and impact resistance, the ultraviolet aging resistance is remarkably improved, and the service life is greatly prolonged. In addition, the process is simple, and energy consumption is low.
Owner:FUZHOU UNIV

Water-based organic silicon-modified epoxy resin and preparation method thereof

The invention discloses a water-based organic silicon-modified epoxy resin and a preparation method thereof. The epoxy resin is prepared from the following raw materials in parts by weight: 100 parts of bisphenol A-type epoxy resin, 50 to 200 parts of organic solvent, 10 to 50 parts of acrylic monomer, 0 to 50 parts of styrene, 10 to 80 parts of gamma-methacryloxy propyl tris(trimethylsiloxy)silane, and 1 to 5 parts of initiator. The preparation method comprises the following steps: dissolving the bisphenol A-type epoxy resin in the organic solvent, performing copolymerization with the acrylic monomer, the styrene and the gamma-methacryloxy propyl tris(trimethylsiloxy)silane under the action of the initiator, distilling the copolymer under a reduced pressure, and adjusting the pH value to be 7-8 to obtain the water-based organic silicon-modified epoxy resin. In the epoxy resin disclosed by the invention, the silicone content of organic silicon monomers is increased; the toughness and weather resistance of the prepared epoxy resin are remarkably improved; the preparation method is simple and is easy to operate, does not have special requirements on production equipment, and has high production efficiency; each technical parameter is convenient to control.
Owner:GUANGZHOU GEMBOND CHEM

A method for reprocessing and comprehensive utilization of red mud

The invention discloses a reprocessing and comprehensive utilization method of red mud, comprising the following steps: (1) carrying out mashing on red mud, and carrying out artificial mineral dressing on heavy mineral to respectively obtain coarse sand and mortar; (2) drying the coarse sand, then carrying out magnetic separating to respectively obtain quartz sand and level 1 magnetic material; (3) carrying out magnetic separating on the level 1 magnetic material to respectively obtain magnetite powder and tailing 1; and (4) putting the mortar in a magnet separator for magnetic separating to respectively obtain fine iron ore and tailing 2. The method is simple and practicable and has the advantages of easily controllable technical parameters, little energy consumption and low cost, can process more than 100 Mtpa per year, reduce the discharging capacity of red mud by 35-70 % and reduced the production cost of alumina. The main products of the method are magnetite powder and quartz, and the obtained two tailings can be used in preparing dry cement or in damming, so that the purpose of comprehensive utilization of red mud is achieved.
Owner:中铝山东有限公司

Composite slice type inductive element and preparation method thereof

The invention relates to a composite material chip type inductive element and the preparation method thereof. The inductive element is applicable to the extreme-high / ultra-high frequency range chip type inductive element, adopts the three-phase composite material containing hexagonal surface soft magnetic ferrite powder, metal magnetic particles and high-temperature resistant resin as the magnetic medium, and can adjust the electromagnetic property of the material based on the three-phase composite double-seepage theory; the composite material chip type inductive element comprises a flush-type helical inner electrode and a terminal electrode which is directly connected with the inner electrode, and can adopt the base metals, such as Ni and Cu to be taken as the inner electrode material, thereby greatly reducing the cost of the element; the composite material chip type inductive element is prepared by utilizing the polymer hot pressing process, thereby avoiding the difficulty of heterogeneous co-firing in the lamination co-firing technology of the traditional chip type inductive element. The element has the advantages that the weight is light, the volume is small, the magnetic screening effect is good, the requirement of the automatic solder-reflow process can be satisfied, the production process is simple, the production cycle is short, the technical parameter is easy-to-control, the production energy consumption is low, and the element is applicable to the large-scale industrialized production.
Owner:UNIV OF SCI & TECH BEIJING

Lycium ruthenicum fruit, haw and lemon compound beverage preparation method

The present invention relates to a lycium ruthenicum fruit, haw and lemon compound beverage preparation method which comprises the following steps: (1) manual cleaning, picking, purifying and squeezing the lycium ruthenicum fruits, haws and lemons respectively to obtain the lycium ruthenicum fruit juice, haw juice and lemon juice; and fully mixing the lycium ruthenicum fruit juice, haw juice and lemon juice to obtain a mixed juice liquid; (2) conducting water bath heating for the mixed juice liquid and water to obtain an extract liquid; (3) milling the extract liquid using a colloid mill for after 1-8 times to obtain a colloidal composite extract solution; (4) the colloidal composite extract solution is homogenized, enzymolysed, and centrifugal separated to respectively obtain a supernatant A and a residue; (5) the supernatant conducts ceramic film impurity removing to obtain a filtrate; (6) blending the filtrate and the haw juice, centrifuging the mixture to obtain a supernatant B, and sterilizing the supernatant B by conventional methods, and filling the sterilized supernatant B to obtain the compound beverage. The lycium ruthenicum fruit, haw and lemon compound beverage has a low cost, and the obtained product has a high content of active substance, and is natural, healthy and nutritional.
Owner:JINAN HAILAI COMMERCE & TRADE CO LTD

Purification system of anhydrous hydrogen fluoride gas

The invention relates to a purification system of anhydrous hydrogen fluoride gas, belonging to the field of chemical engineering. The purification system comprises an air inlet pipeline, an air outlet pipeline, a purification tower, a dust collecting device and a back flushing device, wherein the air inlet pipeline is positioned at the lower half part of the purification tower, and the air outlet pipeline is arranged at the upper half part of the purification tower; membrane material resisting the temperature of 20-100 DEG C and the negative pressure of 1000-3000MPa is arranged inside the purification tower; the membrane material has the aperture less than 1mu m, hydrofluoric acid corrosion resistance and the total specific surface area more than 180m2 / g; the upper end of the collecting device is connected with the bottom of the purification tower; the back flushing device is positioned at the upper half part or the top of the purification tower, one end of the back flushing device is connected with the purification tower, and the other end is connected with an air compressor. The purification system has the advantages of low cost, easy controlled technical parameters, convenient working condition operation, safety, environmental protection, large-scale continuous production, etc. By adopting the system, under the normal temperature and pressure, the anhydrous hydrogen fluoride gas contains the content of dust particles less than 5g / m3, and the removed dust particles have the size within 200-500nm and mainly comprises fluorine, silicon, phosphorus, ferrum, sulfur, oxygen, etc.
Owner:BEIJING UNIV OF TECH

Method for reinforcing akermanite bone scaffold in selective laser sintering by utilization of nano titanium oxide

The invention relates to method for reinforcing and toughening an akermanite bone scaffold by utilization of nano titanium oxide power and for preparing a three-dimensional porous ceramic bone scaffold with a controllable micro-pore structure by utilization of the selective laser sintering technology. The problems of low toughness and poor intensity of biological ceramics and uncontrollable micro-pore structure of a prepared scaffold in a traditional porous scaffold preparation method are solved. The method is as follows: nano titanium oxide power is added into micron akermanite power, the composite power is mixed uniformly in a mechanical mixing method, and then the mixed power is placed in a selective laser sintering system and a porous akermanite bone scaffold is prepared by utilization of a rapid forming technology. The prepared porous scaffold has tough mechanical properties and an controllable micro-pore structure, and can meet the requirements of tissue-engineered bone research and application.
Owner:CENT SOUTH UNIV

Process for removing impurities in production of dry-method aluminum fluoride

The invention provides a process for removing impurities in production of dry-method aluminum fluoride and belongs to the field of chemical engineering. A purifying system is used in the process; the purifying system comprises a gas inlet tube, a gas outlet tube, a purifying tower, a dust collecting device and a back-blowing device, wherein anhydrous hydrogen fluoride gas carrying a large amount of dust particles is generated by the reaction of fluorite and sulfuric acid in an acid making furnace and then enters the purifying tower through the gas inlet tube; the gas is filtered by film materials in the purifying tower and discharged by the gas outlet tube; and finally, the gas enters a fluidized bed to react with aluminum hydroxide to form the dry-method aluminum fluoride product, and in the impurity removing process, the product is blow-washed once every one to two hours by the back-blowing device, and the dust particles blown down are collected by the dust collecting device and then discharged from the bottom part of the purifying tower. The process has the advantages of low production cost, easy technological parameter control, convenient procedure operation, safety and environmental protection, industrialized continuous production and the like; and after the product of the dry-method aluminum fluoride undergoes the impurity removing process, the quality of the product of the dry-method aluminum fluoride meets all first-grade product indexes specified in national standards.
Owner:BEIJING UNIV OF TECH

Hemihydrate gypsum base material imitation wood floor and preparation method thereof

The invention relates to the technical field of chemical building materials, in particular to a hemihydrate gypsum base material imitation wood floor and a preparation method thereof. By properly proportioning and designing raw materials such as hemihydrate gypsum, cement, a coagulation accelerator and the like, the quality of the hemihydrate gypsum is improved, the activity of the hemihydrate gypsum is improved, the toughness and plasticity of a product made from the hemihydrate gypsum are improved, the flexural and compressive strength of a base material made from the hemihydrate gypsum as a raw material is enhanced, the freeze-thaw resistance of a phosphogypsum product is improved, and the weather resistance and corrosion resistance of the phosphogypsum product are improved; by combination with control on technical parameters in a preparation process after the raw materials are properly proportioned, the compatibility of the hemihydrate gypsum, the cement, the coagulation accelerator, fibers and the like is relatively good, holes of the product are uniform in size, and the waterproof and dampproof performance and mechanical strength of the hemihydrate gypsum base material are improved.
Owner:GUIZHOU KAILIN PHOSPHOGYPSUM INTEGRATION UTILIZATION

Preparation method of nano zinc oxide thin film and zinc oxide/copper oxide semiconductor material

The invention discloses a preparation method of a nano zinc oxide thin film. The preparation method comprises the following steps of: (1) taking a zinc substrate with zinc on the surface, and cleaning the surface or removing an oxide skin for later use; (2) preparing saturated copper salt solution with concentration of 0.05 mol / L, placing the zinc substrate in a copper salt bath to soak for 1 second to 1 minute, taking out and naturally drying; (3) preserving heat of the soaked zinc substrate at 400-550 DEG C in an oxygen-containing atmosphere for 30 minutes to 48 hours to obtain the nano zinc oxide thin film with a nano wall structure on the surface. According the preparation method, a loose copper layer is deposited on the surface of the zinc substrate, and then thermal oxidation is performed in the oxygen-containing atmosphere to obtain a rose structure consisting of ZnO nano wall, and meanwhile, a ZnO / CuO n-p semiconductor structure can also be prepared. The method has the characteristics of small environmental pollution, simple equipment and low preparation cost, and meanwhile, the technical parameters are easy to control, for example, the formation temperature range is wide, and the influence of partial pressure of oxygen is small. The prepared nano zinc oxide thin film can be used for preparing a photoanode of a fuel sensitized solar cell.
Owner:HENAN UNIV OF SCI & TECH

A kind of PP plastic with phosphogypsum as filler and preparation method thereof

The invention relates to the technical field of PP (Polypropylene) plastic and particularly relates to PP plastic taking ardealite as packing and a preparation method of the PP plastic. The PP plastic is prepared by carrying out proportion design on the ardealite, titanium dioxide, nano silicon dioxide, paraffin, PVC (Polyvinyl Chloride), PP, PE (Polyethylene), lauric alkanolamide, 3-aminotriethoxysilane and (3-lauramidepropyl)trimethyl ammonium methosuflate, so that the obtained PP plastic has a relatively good antistatic effect, and relatively good tensile strength, impact strength, bending strength and bending modulus; the ardealite can be used as the packing for producing the PP plastic, so that the stockpiling pressure of the ardealite in a phosphorus chemical industry is alleviated, the comprehensive utilization rate of the ardealite is improved, the effective resource utilization of ardealite resources is realized, and the environment pollution is reduced.
Owner:GUIZHOU KAILIN PHOSPHOGYPSUM INTEGRATION UTILIZATION

Working electrode, electro-adsorption system and method for adsorbing metal ions in wastewater

The invention relates to a working electrode, an electro-adsorption system and an electro-adsorption method for adsorbing metal ions in wastewater, and belongs to the technical field of electro-adsorption chemical engineering. The working electrode is formed by taking carbon cloth or carbon paper as a substrate, taking amidoxime as a functional group and taking an oxygen-containing group as a connecting site through grafting; wherein the working electrode is prepared by an oxidation-cyanation-oximation three-step method. The working electrode can selectively adsorb various metal ions in the acid wastewater, and the adsorption effect is good; after the reaction is completed, the metal ions adsorbed on the working electrode can be desorbed by applying reverse voltage, so that recovery is realized. The electro-adsorption system comprises an electric signal generator and an electro-adsorption reaction tank; the electro-adsorption reaction tank comprises the working electrode and a counter electrode; meanwhile, the electro-adsorption system is controllable in technical parameters, simple and convenient to operate and capable of realizing efficient electro-adsorption reaction. The method is carried out by adopting the electro-adsorption system, and a plurality of metal ions in the acid wastewater are effectively adsorbed by utilizing a square wave periodic electric field.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

Health-care sugar foodstuff and preparation method thereof

The invention relates to a health-care sugar foodstuff and a preparation method thereof, belonging to the technical field of health-care sugar food. According to the invention, through reasonable proportioning of raw materials like glucose syrup, peanut, maltodextrin, milk powder, cream, salad oil, starch and vanillin, the health-care sugar foodstuff with novel taste, a moderate sugar degree and special flavor is prepared; the health-care sugar foodstuff has a long shelf life and can be stored for one year in a normal temperature environment; in the preparation process of the health-care sugar foodstuff, technical parameters are easy to control, process steps are simple, energy consumption is low, cost is low, and in particular, raw materials for the health-care sugar foodstuff are easily available, so cost of the health-care sugar foodstuff is low; moreover, since the addition sequence of each raw material is restricted in the preparation process, it is guaranteed that main components of each raw material undergo accurate microscopic biochemical reaction during addition and mixing of each raw material, the nutritional value of the health-care sugar foodstuff is improved, taste is enhanced, and the appetite of people eating the health-care sugar foodstuff is whetted.
Owner:SONGTAO MIAOXIANG FOOD

Production process and equipment of Freon-resistant composite enameled wire with glass fiber wrapping

The invention relates to the technical field of composite enameled wire production, in particular to a production process and equipment of a Freon-resistant composite enameled wire wrapped with glass fiber, and the process comprises the following steps: a copper wire body which is clean and smooth in appearance quality and free of burrs, scratches, oxidation layers and oil stains is adopted and then enters a softening furnace to be preheated; then, the wire body is quickly and accurately guided, and the copper wire body is subjected to Freon-resistant insulating paint dipping by using a paint dipping device; then the processing device can carry out curing treatment on the wire body subjected to paint dipping; single-layer glass fibers are used for wrapping, wrapping needs to be tight and flat, and the wrapping fibers are free of seam exposure and accumulation; winding operation is carried out after wire winding is finished; the equipment comprises a supporting bottom plate, a guiding clamping plate, a paint dipping device, a machining device, a connecting clamping plate, a winding clamping plate, a winding device, a connecting bottom frame, a tooth-shaped belt and a servo motor. The preparation method is reasonable in design, simple in process and clear in process route, and the prepared finished product has excellent performance of high temperature resistance, high pressure resistance and corrosion resistance.
Owner:湘潭市霞城电工有限公司

Laser preparation method of porous bone scaffold and adding zinc oxide to improve performance

The invention relates to a method for preparing a porous bone scaffold by laser and increasing mechanical and biological performances of the porous bone scaffold by adding zinc oxide with little amount, which belongs to the bone tissue engineering field. Aiming at uncontrollable performances of aperture distribution, shape, space direction and connectivity in the preparation method of a traditional bone scaffold, and aiming at the disadvantages of poor mechanical property and fast resolving rate existed in tricalcium phosphate (beta-TCP), the invention provides the method for preparing the porous bone scaffold by using a selective laser sintering (SLS) technology, and provides the method for increasing performance by adding zinc oxide (ZnO). The method for preparing the porous bone scaffold has the advantages that the porous scaffold which enables three-dimensional interconnection is prepared by SLS, zinc oxide with little amount is added for introducing into a liquid phase, the particles densification can be promoted, crystal grain is refined, and the mechanical performance is improved, simultaneously, cell compatibility is increased, the degradation rate is reduced, and the biological performance is increased, so that the interconnected porous beta-TCP bone scaffold with enhanced mechanical performance and good biological performance can be finally prepared. The method has the advantages of simple preparation technology, convenient operation, low cost, easy control of technical parameter and the like.
Owner:CENT SOUTH UNIV

Process and device for preparing iron ore concentrate through mixture of aluminum oxide red mud tailings and copper tailings

InactiveCN108686829AReduce the amount of effluxReduce the number of stockpilesWet separationRed mudImpurity
The invention relates to a process for preparing an iron ore concentrate, in particular to a process and a device for preparing the iron ore concentrate through a mixture of aluminum oxide red mud tailings and copper tailings. The process comprises the steps of filter-pressing the red mud tailings, mixing with a curing agent and a drying agent, processing until the water content of the red mud tailings is smaller than 20 percent, stirring and mixing with the copper tailings, stacking and turning over; diluting the obtained materials, then screening out impurities, and after classifying other materials through a cyclone, settling overflow matters in a settling tank; and adding a chemical flocculant into the settling tank, feeding underflow solids settled in the settling tank to a magnetic separator, carrying out magnetic separation, filtering and dewatering a solid part obtained through magnetic separation, and obtaining an irony additive or medium powder. According to the process and the device for preparing the iron ore concentrate through the mixture of the aluminum oxide red mud tailings and the copper tailings provided by the invention, the discharging quantity of red mud and the stacking quantity of the copper tailings can be greatly reduced, the wastes are truly recycled, the effective utilization rate of iron elements can reach to more than 70 percent, and medium powderand iron ore concentrate powder products with high yield and high grade are obtained.
Owner:山东盛日奥鹏环保新材料集团股份有限公司

Production process of freon resistant, double glass fiber covered enamelled wire

The invention relates to a production process of a freon resistant, double glass fiber covered enamelled wire, which solves problems of lag in an existing production process of glass fiber covered enamelled wires, large waste of raw materials, high energy consumption, environmental pollution and quality instability. The production process ensures quality of finished products and work efficiency by the following steps: strictly selecting the raw materials, taking the raw materials into a softening furnace for solidifying treatment by freon resistant insulating impregnating varnish; covering with conductor glass fiber, wherein, two layers of the glass fiber are covered in reverse directions to prevent single cladding; and controlling temperature of a baking furnace and the like. The production process has rational design, simple process, low manufacturing cost, low operating cost, reliable work, high efficiency, stable quality and strong workability, can help manufacture a plurality of different single and double glass fiber, paper covered and enamelled flat copper wires, round copper wires and irregular copper wires, and various electromagnetic wires for different uses, and the production process has wide market prospect.
Owner:湘潭市霞城电工有限公司

Compounds capable of preventing anxiety, and preparation method thereof

The invention relates to compounds capable of preventing anxiety, and a preparation method thereof. The preparation method comprises following steps: 1, medicinal material herb or fruits are subjectedto selection so as to obtain herb dried samples or dried fruits, and smashing is carried out so as to obtain a medicinal material powder; 2, the medicinal material powder is subjected to heating extraction; 3, an obtained extracted solution is subjected to grinding using a colloid mill so as to obtain a colloid extracted solution, and then centrifugation is carried out; 4, filter residue is removed, and extracted components are collected; 5, an obtained extracted product is subjected to treatment using a micro-reticular resin and a silicagel column, and two-dimensional reversion-phase / hydrophilic chromatography is adopted so as to obtain monomer compounds; and 6, 8 flavonoid compounds capable of preventing anxiety are obtained via screening. No muscle relaxing or depression inducing sideeffect is caused by the 8 flavonoid compounds; the design of the preparation method is scientific and reasonable; the extraction rate and the preparation efficiency are high; the obtained compounds are stable in properties, and high in cost, and possesses excellent anxiety preventing effect.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST

Method for preparing metal nanowire array on the basis of interface reaction and solid-state phase change

The invention belongs to the technical field of preparation of one-dimensional nano materials, and particularly relates to a method for preparing a metal nanowire array on the basis of interface reaction and solid-state phase change. The method for preparing the metal nanowire array on the basis of interface reaction and solid-state phase change comprises the following steps of: firstly, cleaning a substrate; secondly, enabling a low-melting-point alloy as a cladding material to be in close contact with the substrate; thirdly, enabling the metal nanowire array to grow in the substrate through a reaction diffusion method; and fourthly, removing bumps on the surface of the substrate to obtain the metal nanowire array embedded in the substrate. The method for preparing the metal nanowire array on the basis of interface reaction and solid-state phase change has the advantages that (1) the cost is low, the reaction time is short, and the operation is simple and effective; (2) the metal nanowire prepared by the method possesses high orientation, orderliness and uniform length; and (3) the method possesses universality, the preferred orientation of substrate crystal grains can be selectively changed, the growth direction and the growth area of the nanowires can be controlled, and the metal nanowire array is expected to be attached in the substrate in a large range.
Owner:HARBIN UNIV OF SCI & TECH

Biebersteinia heterostemon Maxim extract and application thereof in preparation of anticonvulsants

ActiveCN112336755AGood anticonvulsant effectReduce the number of convulsions/convulsion rateNervous disorderPlant ingredientsConvulsionBiebersteinia heterostemon
The invention discloses a Biebersteinia heterostemon Maxim extract and an application thereof in preparation of anticonvulsants. The Biebersteinia heterostemon Maxim extract can obviously reduce the convulsion number / convulsion rate of mice, remarkably shorten the convulsion duration of the mice and remarkably prolong the convulsion incubation period, has a good anticonvulsion effect, and can prevent / treat symptoms such as febrile convulsion, convulsion and spasm. The provided Biebersteinia heterostemon Maxim extract has a broad application prospect in preparation of safe and high-activity anticonvulsants.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST
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