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52 results about "Resorcinol diglycidyl ether" patented technology

High-thermal conductivity high-performance aluminum-based copper-clad plate and preparation method thereof

The invention relates to a high-thermal conductivity high-performance aluminum-based copper-clad plate and a preparation method thereof. The copper-clad plate is composed of copper foil, a high-thermal conductivity electric insulating paste and an aluminum plate. The preparation method comprises the following steps: mixing multifunctional fluorine-containing epoxy resin with 1,4-di(2,4-diamino phenoxy) benzene for reacting, adding resorcinol diglycidyl ether epoxy resin and partial inorganic filler, and uniformly stirring and mixing to obtain a component A; uniformly mixing and stirring methyl tetrahydrophthalic anhydride and inorganic filler to obtain a component B; and uniformly mixing and stirring the component A and the component B to obtain the high-thermal conductivity electric insulating paste, then uniformly applying the high-thermal conductivity electric insulating paste onto the surface of the copper foil and the aluminum plate, and pressing and curing by a high-temperature panel pressing machine, thereby obtaining the high-thermal conductivity high-performance aluminum-based copper-clad plate. The operation process is simple; with the green and clean production process, a solvent is avoided, and the copper-clad plate has an environment-friendly effect; the copper-clad plate is wide in application range and has good market prospects, and the large-scale mass production can be easily carried out.
Owner:DONGHUA UNIV +2

Affinity chromatography medium with glutathione as ligand

The invention relates to an affinity chromatography medium with glutathione as a ligand. Agarose gel microspheres with boron nitride dispersed on surfaces are taken as a core, the surfaces of the agarose gel microspheres are activated by a first crosslinking agent and a second crosslinking agent, both the first crosslinking agent and the second crosslinking agent are coupled with glutathione as the ligand, the first crosslinking agent adopts epichlorohydrin, and the second crosslinking agent adopts resorcinol diglycidyl ether or neopentyl glycol diglycidyl ether; meanwhile, acetonitrile whichis cheaper and more environmentally friendly is selected as a solvent for coupling with glutathione, so that the dissolution degree of the crosslinking agents is increased, and the agarose gel microspheres are activated sufficiently. The affinity chromatography medium has the advantages that the density of active epoxy groups is high, the amount of coupled glutathione is large, the separation efficiency is higher, a preparation process of the affinity chromatography medium with glutathione as the ligand is simple, the production cost is lower, and large-scale popularization and application arefacilitated.
Owner:SUZHOU BOJIN BIOLOGICAL TECH

5-aldehyde resorcinol diglycidyl ether and preparation method thereof

The invention discloses 5-aldehyde resorcinol diglycidyl ether and a preparation method thereof, relates to glycidyl ether and a preparation method thereof, and aims at solving the problem of poorer bonding strength of the conventional glycidyl ether epoxy resin at high temperature. The preparation method of the 5-aldehyde resorcinol diglycidyl ether comprises the following steps: firstly, putting3,5-dihydroxy benzaldehyde, epibromohydrin and a catalyst into a reaction still, raising the temperature for reaction, decompressing and evaporating out to obtain a concentrated solution; secondly, after the temperature of the concentrated solution is lowered, adding an organic solvent and metal alkali solid particles and stirring; thirdly, after the reaction ends, repeatedly washing with water,and separating liquid to remove an aqueous phase; finally, performing reduced pressure distillation on an organic phase to remove an organic solvent, and recycling to obtain the 5-aldehyde resorcinoldiglycidyl ether. The 5-aldehyde resorcinol diglycidyl ether is used for preparing a high temperature resisting epoxy resin adhesive. The epoxy resin adhesive prepared from the 5-aldehyde resorcinol diglycidyl ether disclosed by the invention has the characteristic of high temperature resistance. The 5-aldehyde resorcinol diglycidyl ether and the preparation method disclosed by the invention are used for the field of the epoxy resin adhesives.
Owner:INST OF PETROCHEM HEILONGJIANG ACADEMY OF SCI

Electrically conductive adhesives, assemblies including the electrically conductive adhesives, and related methods

An assembly comprising a first article, a second article adjacent the first article, and an electrically conductive adhesive in electrical communication with the first article and the second article. The electrically conductive adhesive comprises nickel nanostrands dispersed in a matrix comprising a reaction product of bisphenol-F epoxy resin, resorcinol diglycidyl ether epoxy monomer, and at least one amine-containing curing agent. The electrically conductive adhesive exhibits a tensile adhesion strength greater than about 5,000 psi and a volume resistivity less than about 0.01 Ω·cm. Electrically conductive adhesives including nickel nanostrands, precursor packages of the electrically conductive adhesive, related methods of forming the electrically conductive adhesive and an assembly including the electrically conductive adhesive are also disclosed.
Owner:NORTHROP GRUMMAN SYST CORP

Active carbon prepared from wastes and method thereof

The invention discloses active carbon prepared from wastes. The active carbon is prepared from the following raw materials in parts by weight: 10 to 15 parts of waste ceramic sheets, 10 to 15 parts of waste tire rubber, 6 to 10 parts of coal slag, 10 to 16 parts of 1,4-cyclohexanedimethanol, 3 to 6 parts of 2-naphthol-6,8-dipotassium disulfonate, 7 to 10 parts of ethopabate, 6 to 12 parts of isoamyl salicylate, 3 to 7 parts of dimethicone, 10 to 15 parts of mercaptosuccinic acid and 8 to 12 parts of resorcinol diglycidyl ether. The waste ceramic sheets, the waste tire rubber and the coal slag are used as raw materials to be prepared into active carbon with high mechanical strength, good adsorption performance and long service life by virtue of steps such as immersing, carbonization and the like, so that the cost is saved, and the resource utilization rate is increased.
Owner:SUZHOU DINGYU ENERGY EFFICIENT EQUIP

High-strength fireproof crucible and production method thereof

The invention relates-the field of refractory materials, and discloses a high-strength fireproof crucible and a production method thereof. The crucible is produced from a mud material and additives; the mud material comprises 55-65 parts of magnesium ores, 5-15 parts of zirconia, 5-15 parts of fused magnesia, 5-15 parts of waste graphite micro-powder, 1-5 parts of metallic magnesium micro-powder,1-5 parts of chromium oxide micro-powder, 0.3-0.5 part of resorcinol diglycidyl ether, 0.1-0.3 part of sodium dodecyl benzene sulfonate, 20-30 parts of ethanol and 10-20 parts of water; and the additives include 0.05-0.1 part of a cationic photocuring initiator, 0.05-0.2 part of tetradecyltrimethylammonium bromide, 3-7 parts of ethanol and 3-7 parts of water. The reduction of the use amount of theadditives effectively increases the strength of the crucible. A crucible blank is pre-cured through a photocuring technology before being sintered in order to effectively prevent the cracking of thecrucible.
Owner:长兴正发热电耐火材料有限公司

Long-lasting wear-resisting aging-resisting UV (Ultraviolet) curing coating and preparation method thereof

The invention discloses a long-lasting wear-resisting aging-resisting UV (Ultraviolet) curing coating which is characterized by being prepared from the following raw materials in parts by weight: 50-55 parts of urethane acrylate, 9-12 parts of cyclopentane, 7-9 parts of methoxy-polyethylene glycol monoacrylic ester, 3-4 parts of epoxidized soybean oil, 4-5 parts of photoinitiator 2959, 7-9 parts of resorcinol diglycidyl ether, 5-8 parts of ethylene glycol diethyl ether, 5-7 parts of ethyl acetate, 1-2 parts of titanate coupling agent TMC-TTS, 1-2 parts of grape essential oil, 5-7 parts of montmorillonoid, 2-3 parts of chromic oxide, 2-3 parts of antimonous oxide and 4-5 parts of additive. Due to addition of the natural anti-oxidation component grape essential oil, the aging-resistance of the coating is improved, and the coating is safe and non-toxic; due to addition of the antimonous oxide, a good flame retarding effect is achieved; due to addition of the additive, a good leveling property is achieved, a uniform coated layer can be formed, and the coating is fast in curing speed, high in hardness, wear-resisting, good in toughness, high in adhesion property, long-lasting in property and high in universality.
Owner:WUHU EDISON AUTOMATION EQUIP

Anti-thick coating pinhole, excellent acid and alkali resistance powder coating and preparation method thereof

ActiveCN112011260BGood acid and alkali resistanceOvercome the shortcomings of poor acid and alkali resistanceAnti-corrosive paintsPolyether coatingsPolymer scienceLow temperature curing
The invention belongs to the technical field of powder coatings, and in particular relates to a powder coating with excellent pinhole resistance and acid and alkali resistance and a preparation method thereof. The parts by weight of the main raw materials of the powder coating of the present invention are: 530-550 parts of hydroxyl polyether resin, 40-50 parts of B1530 curing agent, 150-200 parts of talcum powder, 120-150 parts of barium sulfate, 8-12 parts of brightening agent Parts, 7-10 parts of leveling agent; Hydroxy polyether resin is prepared by polycondensation of materials with the following molar fractions: the molar fractions of each component are: 1,4-cyclohexanedimethanol 4-8 , 1,6-hexanediol 3-6, resorcinol diglycidyl ether 5-10, propylene oxide 30-45, triglycidyl isocyanurate 4-8, octyl glycidyl ether 6-13 . The present invention uses high-functionality hydroxyl polyether resin as the raw material, the hydroxyl value is 15-20mgKOH / g, the amount of B1530 curing agent required for curing is small, the cost of powder coating is low, and it can be cured at 175°C / 15min at low temperature, and The prepared coating film has good resistance to pinholes in thick coating, and the high-functionality polyether has excellent acid and alkali resistance, and can be used for coating metal facilities in industrial cleaning places.
Owner:安徽鑫友高分子新材料科技有限公司
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