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5216results about How to "Convenient source" patented technology

High energy optical fiber amplifier for picosecond-nanosecond pulses for advanced material processing applications

InactiveUS20050041702A1Sufficient bandwidthImprove mode qualityActive medium shape and constructionNon-linear opticsPulse energyNonlinear fiber
A fiber-based source for high-energy picosecond and nanosecond pulses is described. By minimizing nonlinear energy limitations in fiber amplifiers, pulse energies close to the damage threshold of optical fibers can be generated. The implementation of optimized seed sources in conjunction with amplifier chains comprising at least one nonlinear fiber amplifier allows for the generation of near bandwidth-limited high-energy picosecond pulses. Optimized seed sources for high-energy pulsed fiber amplifiers comprise semiconductor lasers as well as stretched mode locked fiber lasers. The maximization of the pulse energies obtainable from fiber amplifiers further allows for the generation of high-energy ultraviolet and IR pulses at high repetition rates.
Owner:IMRA AMERICA

Single inductor dual output buck converter with frequency and time varying offset control

A single-inductor dual-output buck converter and control method that facilitates power conversion by converting a single DC power source / supply into two separate DC outputs, each of which can be configured to provide a selected / desired voltage by selection of respective duty cycles. The topology of the inverter includes a pair of diodes or switches that can selectively re-circulate inductor current. The converter is generally operated at a fixed frequency with four stages of operation. A first and third stage of operation provide power to a first and second output, respectively. A second and fourth stage of operation re-circulate inductor current and can partially recharge a battery type power source. The power output for each stage (voltage and current) can be selectively obtained by computing and employing appropriate time periods for the stages of operation that correspond to appropriate duty cycles.
Owner:TEXAS INSTR INC

Guided buying decision support in an electronic marketplace environment

A system (10) for providing guided buying decision support within an electronic marketplace environment includes a server (42) that interacts with buyers (12) to receive procurement parameters for items. An option generator (50) receives procurement parameters for a particular item needed by a particular buyer (12), determines one or more acceptable item-supplier combinations consistent with the procurement parameters for the item, and generates one or more recommended options for communication to the buyer (12), each recommended option specifying a service through which it is possible to procure the item consistent with the procurement parameters. The server (42) further interacts with the buyer (12) to receive a selection of a particular recommended option. A manager application (46) automatically initiates the service specified in the selected recommended option in an attempt to procure the item consistent with the procurement parameters.
Owner:JDA SOFTWARE GROUP

High-temperature resisting adhesive and preparation method thereof

The invention relates to a high-temperature resisting adhesive and a preparation method thereof; the adhesive is formed by the following ingredients: carboxyl contained polyimide resin powder, epoxide resin, curing agent and organic solvent with weight ratio of 1:10-20:0.1-2:20-30. The preparation method of the high-temperature resisting adhesive comprises the following steps: adding the carboxylcontained polyimide resin powder, the epoxide resin and the curing agent into a reaction kettle, heating the reaction kettle to 80-90 DEG C for carrying out stirring reaction for 0.5-1.5 hours, and then adding the organic solvent continuously, and stirring the mixture uniformly at room temperature, thus obtaining the high-temperature resisting adhesive. The preparation method has simple process and low cost and is environment-friendly, the preparation process can be carried out in a general device, thereby being suitable for industrial production.
Owner:DONGHUA UNIV +1

Alicyclic-containing polyimide film and preparation method thereof

The invention relates to an alicyclic-containing polyimide film. The molecular structure general formula of the film is the right formula, wherein, -CA- is a bivalence connection group of an alicyclic dibasic primary amine, -Ar- is a bivalence connection group of an aromatic dibasic primary amine, and -R- is a bivalence connection group of an aromatic dibasic estolide. The preparation thereof includes: the alicyclic dibasic primary amine and the aromatic dibasic primary amine are dissolved in non-proton organic solvent with strong polarity, the aromatic dibasic estolide is added, the non-proton organic solvent with strong polarity is used for regulating the viscosity of the alicyclic-containing polyamic acid resin solution after reaction for 1-3 hours, forming is carried out in a curtain coating machine, and dehydration fever imidization, cooling and demoulding are carried out so as to obtain the film. The preparation method has mild reaction condition and low cost and is environmentally friendly; and meanwhile, the alicyclic-containing polyimide film has excellent mechanic property and heat resistant property and low water absorption, and the visible light transmission thereof is as high as more than 97%. The film has good application prospect in the fields of optical waveguide material, photorefractive material and photoelectric material in optical communication field and direct action membrane material in the liquid crystal display field and the like.
Owner:DONGHUA UNIV

High-temperature-resistant modified polyfunctional epoxy matrix resin for advanced composite material and preparation thereof

The invention relates to high-temperature-resistant modified polyfunctional epoxy matrix resin for an advanced composite material. The resin comprises tetramaleimide resin, carboxy terminated nitrile rubber, polyfunctional epoxy resin, a curing agent and an organic solvent. A preparation method comprises the following steps of: adding the tetramaleimide resin, the carboxy terminated nitrile rubber and the polyfunctional epoxy resin into a reaction kettle and reacting at the temperature of 110 DEG C for one hour; adding the organic solvent and dissolving under stirring to obtain a component A;mixing the curing agent and the organic solvent and dissolving under stirring to obtain a component B; and mixing the component A and the component B and uniformly stirring during use. The high-temperature-resistant modified polyfunctional epoxy matrix resin provided by the invention has the advantages of high room temperature tensile shear strength, high heat resistance, wide application prospect in the fields such as electronics, micro-electronics, printed circuit boards (PCB), motors, aerospace and the like, simple preparation process, low cost and contribution to realizing industrial production.
Owner:DONGHUA UNIV +1

Tablet case

A tablet case with a cover, the tablet case comprising a housing having three upstanding walls, at least one of the three upstanding walls having a flange, the housing being adapted to receive and retain a tablet. The tablet case further comprises a cover having a substantially rectangular foldable planar member and an elongated member which extends from the cover into an indentation on the inside of the housing. A section of the elongated member is secured to the indentation to form a substantially planar surface arranged to abut the rear wall of a tablet. First and second magnetic means are provided on the housing and cover respectively to allow the cover to be folded into a stand and secured to the housing or to allow the cover to simply shield a tablet screen.
Owner:C6 LIFE

Full aromatic fluorine containing transparent polyimide film and preparation method thereof

The invention relates to a full aromatic fluorine containing transparent polyimide film. Structural formula of molecule thereof is shown above, wherein -R1 is a divalent residue of fluorine containing aromatic binary primary amine, and -R2 is a divalent connecting group of aromatic binary anhydride molecule. The preparation method thereof comprises steps of adding the fluorine containing aromatic binary primary amine and strongly polar non-protonic organic solvent into a polymerizing bottle, stirring at room temperature, after being completely dissolved, adding the aromatic binary anhydride, stirring, after 3 hours reaction, obtaining transparent and thick fluorine containing aromatic polyamide acid resin solution having homogeneous phase; and using the strongly polar non-protonic organic solvent to regulate viscosity of the fluorine containing aromatic polyamide acid resin solution, forming film, heating, carrying out dehydrating hot-imidization reaction, cooling, demoulding, thus obtaining the full aromatic fluorine containing transparent polyimide film. The preparation method has mild reaction condition, simple operation and low cost and is environment friendly. The full aromatic fluorine containing transparent polyimide film has excellent mechanical property and heat tolerance and visible light transmission thereof is up to 95%.
Owner:DONGHUA UNIV

Preparation method of high temperature resistant single-component solventless epoxy adhesive

The invention relates to a preparation method of high temperature resistant single-component solventless epoxy adhesive. The method comprises the following steps: adding aromatic binary primary amine and strongly polar non-proton organic solvent in a reaction tank, stirring at room temperature to dissolve, adding aromatic binary acid anhydride to perform refluxing and water-segregating reaction at 120-150 DEG C for 6-12h, cooling, adding the reaction solution in a stamp tank with precipitant to precipitate solid powder, namely white thermoplastic polyimide powder, adding white thermoplastic polyimide powder and tertiary amine compound or imidazole compound in epoxy resin to react for 1-2h, adding active diluent and latent curing agent to stir evenly and obtaining the product. The production process is easy and the cost is low so as to realize industrialized production; the tensile shear intensions of the epoxy adhesive at room temperature and 120 DEG C are respectively up to 28Mpa and26Mpa and the epoxy adhesive has broad application prospect in fields such as electronics and microelectronics, electrical motors, aviation and aerospace and the like.
Owner:DONGHUA UNIV

Method for preparing aromatic polybenzimidazole resin film

The invention relates to a preparation method for aromatic series polybenzimidazole resin film, comprising: (1) under function of polyphosphoric acid / phosphorus pentoxide system, condensation polymerization reaction is carried out to aromatic series amine and aromatic series dicarboxylic acids mixed according to mol ratio of 1:1 in nitrogen atmosphere; (2) after cooling, polymer is poured into water and broken down into powder in a resin pulper and washed over and over again by distilled water and soaked for 48 hours in NaHCO3 solution and washed till pH value shows neutral and drawn and filtered for drying in vacuum; (3) the polymer dried is dissolved in even solution prepared by organic solvent with mass percent of 5 percent, and then is dried at temperature of 130 DEG C for 12 hours, and is soaked in hot water for boiling and striping, and is dried in vacuum at temperature of 100 DEG C for 5 hours and then is obtained. The polybenzimidazole prepared by the invention has the advantages of big molecule weight, stable thermal stability, fine solubility and film forming performance, etc. The preparation has simple technology, low cost, convenient operation and can be finished in common equipments through preparation procedure.
Owner:DONGHUA UNIV

Polyimide film with high visible light permeability and preparation thereof

The invention related to a polyimide film with high visible light permeability, molecular structure formula of which is: (shown in figure). Preparation comprises steps of: dissolving primary diamine in a strongly polarnon-proton solvent, cooling the same by cold water to 5 DEG. C to 10 DEG. C, adding aromatic dianhydride, mixing, reacting 4h to 10h at 5 DEG. C to 10 DEG. C, acquiring homogeneous, transparent, sticky polyamic acid resin solution; wherein mol number of aromatic dianhydride is equal to that of primary diamine; adjusting viscosity of polyamic acid resin solution by N,N-dimethyl acetamide, forming film in a casting machine, heating to raise temperature, processing dehydration heat imidization, cooling, deciduating to acquire homogeneous and transparent polyimide thin film. The preparation method has mild reaction condition, sample to operate, low in cost and environmental friendly; mechanical property and thermal stability of the polyimide thin film are excellent with high visible light permeability reaching 94% and film thickness 50 micrometers.
Owner:DONGHUA UNIV +1

Preparation method for high strength macro graphene conductive fiber

The invention discloses a preparation method for high strength macro graphene conductive fiber. According to the method, graphite is oxidized to obtain a graphene oxide; the graphene oxide is dispersed in water or a polar organic solvent to prepare a spinning liquid sol with the mass concentration of 1-20%; the spinning liquid sol is transferred to a spinning device; the spinning liquid is continuously extruded from a spinning head capillary at a uniform speed; the extruded spinning liquid enters a solidification liquid; the solidified primary fiber is collected by using a polytetrafluoroethylene roller; a drying treatment is performed to obtain the graphene oxide fiber; the graphene oxide fiber is subjected to chemical reduction to obtain the graphene fiber. According to the present invention, the spinning process is simple; the operation is performed at the room temperature; no strong corrosive reagent is used; the process has the characteristics of green environmental protection; the prepared graphene fiber has characteristics of good conductivity, excellent mechanical property and good toughness, can be woven into the pure graphene fiber cloth, can further be woven into various fabrics with other fibers, and can further be added to the polymer as the conduction enhancing additive and the like; the prepared graphene fiber can replace the carbon fiber to use in a plurality of fields.
Owner:杭州德烯科技集团有限公司

Colorless transparent aromatic polyimide film and preparation method thereof

The invention discloses a colorless and transparent aromatic polyimide film which has the general formula of molecular structure as follows; the preparation thereof includes: aromatic primary amine and aromatic acid anhydride with specific molecular structures are adopted for polymerization in a strong polar aprotic organic solvent system within the temperature range of 0 DEG C to 35 DEG C to prepare a colorless and transparent viscous polyamide acid solution with homogeneous phase. Viscosity adjustment, casting for forming the film, heating for rising temperature and solvent removal are carried out simultaneously when partial imidization reaction is carried out, and then demoulding and stretching, further deep thermal imidization and rolling are carried out to obtain the colorless and transparent aromatic polyimide film. No special production equipment is required by the invention so that production can be carried out on the conventional production line of the polyimide film and the polyimide film is applicable to industrialized production.
Owner:DONGHUA UNIV +3

Method for preparing high-strength conductive graphene fiber by large-size graphene oxide sheet

The invention discloses a method for preparing high-strength conductive graphene fiber by a large-size graphene oxide sheet. The method comprises the steps of: oxidizing expanded graphite and obtaining graphene oxide; dispersing the graphene oxide into water, carrying out centrifugal classification treatment on the dispersed graphene oxide, and obtaining the large-size even graphene oxide sheet; and finally, dispersing the graphene oxide into water or polar organic solvent, preparing spinning solution liquid crystal sol with the mass concentration of 1-20%, transferring the spinning solution liquid crystal sol into a spinning device, continuously squeezing spinning solution out from a spinning head capillary tube at the uniform velocity, leading the squeezed spinning solution into solidification liquid, drying the solidified primary fiber, obtaining graphene oxide fiber, and then obtaining the graphene fiber by chemical reduction. A spinning technology is simple; and the obtained graphene fiber is good in electrical conductivity, excellent in mechanical property and better in toughness, can be woven into pure-graphene fiber cloth, and also can be woven with other fibers in a blending way so as to make various functional fabrics, so that the high-strength conductive graphene fiber can be used for replacing carbon fiber in a plurality of fields.
Owner:杭州德烯科技集团有限公司

Medicinal fibre used for treating cutaneous inflammation and pain, preparation and application thereof

The invention relates to medicinal fibre used for treating cutaneous inflammation and pain, which comprises the components of cellulose acetate nano fibre, a ketoprofen ester precursor medicine and a medicinal percutaneous sorbefacient, wherein the ketoprofen ester precursor medicine accounts for 0.1-30% of the total weight of the fibre, the medicinal percutaneous sorbefacient accounts for 0.1-10% of the total weight of the fibre, and the cellulose acetate nano fibre accounts for 1-99% of the total weight of the fibre; the preparation of the medicinal fibre comprises the following steps: dissolving the ketoprofen ester precursor medicine, the medicinal percutaneous sorbefacient and the cellulose acetate into an organic solvent to prepare spinning liquid and then spinning to prepare the required medicinal fibre. The medicinal fibre has the effect of treating cutaneous inflammation and pain, has simple preparation method, convenient source of the raw materials and low cost, is friendly to the environment and is suitable for industrialized production; the fibre can be prepared into medicine-carrying clothings or other fabrics which directly contact with the skin of a human body, and the percutaneous administration is safe and comfortable.
Owner:DONGHUA UNIV +1

Acid-cleaning inhibiter for cleaning boiler and use method thereof

The invention discloses an acid-cleaning inhibiter for cleaning a boiler and a use method thereof. The acid-cleaning inhibiter comprises the following components by weight percent: 2.0%-10.0% of acid liquor, 0.08-0.25% of urotropine, 0.04-0.15% of dimethylbenzene thiourea or thiourea, 0.01-0.05% of thiocyanate, 0.03-0.12% of dodecyl-cetyl phenmethyl chloride or bromide, 0.05-0.12% of a surface active agent and the balance of water. Acids suitable for the acid-cleaning inhibiter include hydrochloric acid, citric acid, sulphuric acid, hydrofluoric acid, aminosulfonic acid and phosphoric acid, which are suitable for boiler steel, mild steel, alloy steel and steam steel. The inhibition effect of the invention is over 98% with less toxicity under the boiler chemical cleaning condition, the value of LD50 (orally taken by mice) is 5.74 g / kg. The invention can be stored for 2 years, resistant Fe<3+> ion is 800 mg / kg in the acid cleaning. The preparation method has simple steps, easily obtained raw materials and convention operation.
Owner:湖南省湘电试验研究院有限公司 +2

Gaming device having a replicating display

A gaming device that provides a second or replicating display that is an enlarged, preferably simulated replica of the actual display of the reels, paylines and indicia of the paystops of the gaming device. The second or replicating display can exactly recreate the actual rotation or random generation of the reels, represent the random generation of the reels, and do so by providing a slight delay. The present invention also contains a method by which the replicating display presents each of a plurality of award generating or winning paylines individually and sequentially for a predetermined amount of time before culminating in a display of the accumulated winning paylines. The method enables the player to easily see the source of an award, which would otherwise be difficult to discern from a multitude of paylines.
Owner:IGT

Intelligent power supply station storeroom management system and method based on internet of things

The invention provides an intelligent power supply station storeroom management system and method based on the internet of things. The intelligent power supply station storeroom management system comprises a master control terminal, a background management server connected to the master control terminal, an intelligent security tool cabinet management sub system capable of being connected to the master control terminal in a communication mode, an intelligent warehouse management sub system and an intelligent key library management sub system. The master control terminal is internally provided with intelligent security tool cabinet management system software, intelligent warehouse management software and intelligent key library management system software. A three-in-one comprehensive management model of real-time voice, data and images is adopted for the system, use of a security tool, consumption of spare parts and borrowing of keys are managed through an intelligent means, the failure repair time of a response field can be effectively shortened, the failure reaction speed is increased, the agricultural distribution network construction, overhauling and repairing work efficiency is improved, the work procedure of operation personnel is standardized, the safe production awareness is enhanced, a novel intelligentized power supply station storeroom based on a technology of the internet of things is constructed, and powerful guarantee is provided for safe production of a power enterprise.
Owner:STATE GRID FUJIAN JINJIANG POWER SUPPLY

Benzimidazole diamine curing type epoxy adhesive and preparation method thereof

InactiveCN102031082AHigh tensile and shear strength at room temperatureConvenient sourceNon-macromolecular adhesive additivesCarboxyl rubber adhesivesViscous liquidElectronics
The invention relates to a benzimidazole diamine curing type epoxy adhesive and a preparation method thereof. The adhesive is prepared from the following raw materials: a component A, namely a benzimidazole diamine curing agent and a component B, wherein the component B is prepared from terminal carboxyl group butadiene-nitrile rubber, epoxy resin and a reactive diluent. The preparation method comprises the following steps of: (1) adding the terminal carboxyl group butadiene-nitrile rubber and the epoxy resin into a reaction kettle, reacting at the temperature of 90 DEG C with stirring, cooling to the temperature of 50 DEG C, adding the reactive diluent, and stirring at the temperature of 80 DEG C to obtain homogeneous and transparent viscous liquid, namely the component B; and (2) mixingthe components A and B, and stirring uniformly to obtain the adhesive. The tensile shear strength of the adhesive is 33.5MPa at the room temperature, and the adhesive has wide application prospect infields of electronics and microelectronics, rigid copper-clad laminates, motors, aerospace and the like; and the preparation process is simple, is low in cost and is convenient to operate, the resources of reaction raw materials are wide, and the adhesive can be conveniently industrially produced.
Owner:DONGHUA UNIV +1

Method for cooperatively promoting agglomeration growth of PM (particulate matter) 2.5 and treating desulfuration wastewater in evaporation manner and device of method

The invention discloses a method for cooperatively promoting agglomeration growth of PM (particulate matter) 2.5 and treating desulfuration wastewater in an evaporation manner and a device of the method. The method particularly includes steps that agglomeration liquor prepared by desulfuration wastewater, high polymer adhesive and wetting agent is sprayed into an inlet flue of an electric precipitator and is evaporated by the aid of heat of flue gas, in an evaporation process, the wetting agent promotes dust to enter drops of the agglomeration liquor, the high polymer adhesive is connected with PM2.5 via a polymer chain with polar groups, the grain diameter of the PM2.5 is prompted to be enlarged, so that the PM2.5 can be gathered by the follow-up electric precipitator, the desulfuration wastewater is evaporated completely, suspended matters and dissolvable pollutants in the wastewater are converted into solid to be dissolved out, and the suspended matters and the dissolvable pollutants in the wastewater, together with dust in the flue gas, are gathered by the electric precipitator. The device consists of a boiler, an air preheater, the electric precipitator, a desulfurizing tower, a hydraulic cyclone, a desulfuration wastewater clarification tank and an agglomeration liquor preparation tank, and a double-fluid atomizing nozzle is arranged in the flue between the air preheater and the electric precipitator.
Owner:SOUTHEAST UNIV

High-performance conducting resin and preparation method thereof

The invention relates to a high-performance conducting resin, comprising the following components: epoxy, latent curing agent, active toughener and conducting particles. The preparation method comprises the following steps: adding the epoxy and the active toughener in a reaction bulb to react, then adding the latent curing agent, uniformly stirring, adding the surface-treated conducting particles, uniformly stirring, and defoaming in vacuum to obtain the high-performance conducting resin. The conducting resin in characterized in that the bonding strength reaches up to 24.1 MPa; the volume resistivity is 4.30*10<-5>-2.12*10<-4> ohm.cm; the Tonset thermal decomposition temperature reaches up to 398.7 DEG C; the water absorption is only 0.2%; and storage life at the room-temperature is as long as more than 3 months. The invention has the advantages of simple preparation process, low cost, convenient operation and convenient reaction material source, can complete the preparation process in universal devices, is beneficial to realizing industrial production, and has wide application prospects in the fields of electronic components, resonators, relays, electronic capacitors and the like.
Owner:DONGHUA UNIV +1

Single inductor dual output buck converter with frequency and time varying offset control

A single-inductor dual-output buck converter and control method that facilitates power conversion by converting a single DC power source / supply into two separate DC outputs, each of which can be configured to provide a selected / desired voltage by selection of respective duty cycles. The topology of the inverter includes a pair of diodes or switches that can selectively re-circulate inductor current. The converter is generally operated at a fixed frequency with four stages of operation. A first and third stage of operation provide power to a first and second output, respectively. A second and fourth stage of operation re-circulate inductor current and can partially recharge a battery type power source. The power output for each stage (voltage and current) can be selectively obtained by computing and employing appropriate time periods for the stages of operation that correspond to appropriate duty cycles.
Owner:TEXAS INSTR INC

2,2-bis[4-(2,4-diamidophenoxy)phenyl]hexafluoropropane high-temperature-resistant epoxy adhesive and preparation method thereof

The invention relates to a 2,2-bis[4-(2,4-diamidophenoxy)phenyl]hexafluoropropane high-temperature-resistant epoxy adhesive and a preparation method thereof. The 2,2-bis[4-(2,4-diamidophenoxy)phenyl]hexafluoropropane high-temperature-resistant epoxy adhesive is composed of a component A and a component B, wherein the component A is a copolymer prepared by reacting 2,2-bis[4-(2,4-diamidophenoxy)phenyl]hexafluoropropane and epoxy resin; and the component B is a homogeneous transparent solution with the solid content of 15-30%, which is prepared by reacting 2,2-bis[4-(2,4-diamidophenoxy)phenyl]hexafluoropropane and aromatic dibasic acid anhydride in a strong-polarity non-proton organic solvent and toluene. The preparation method comprises the following step: evenly mixing the component A and the component B in a mass ratio of 1:(1-2) at room temperature. The preparation technique is simple; and the adhesive has excellent comprehensive properties, can be widely used for bonding steel, copper, aluminum or any other metal with ceramic, glass, resin-base composite material or any other substrate, and has favorable industrialization prospects.
Owner:DONGHUA UNIV +1

PD-1 gene recombinant virus plasmid, construction thereof, recombinant retrovirus Lenti-PD-1-Puro and packaging and application of recombinant retrovirus Lenti-PD-1-Puro

The invention discloses a PD-1 gene recombinant virus. The collection number of the recombinant virus Lenti-PD-1-Puro is CCTCC No:V201601. According to the PD-1 gene recombinant virus, PD-1gRNA sequences are cloned into a retrovirus plasmid Lenti-CRISPR / Cas9-Puro, and a PD-1 recombinant virus plasmid Lenti-CRISPR / Cas9-PD-1-Puro is obtained; then the PD-1 recombinant virus plasmid Lenti-CRISPR / Cas9-PD-1-Puro, a plasmid pSPAX and pMD2.G are jointly transfected by 293T cells, and packaging of the recombinant virus Lenti-PD-1-Puro is completed. After T cells of peripheral blood of tumor patients are infected by the PD-1 recombinant virus, PD-1 on the T cells is successfully knocked out, the inhibitory state of the T cells of the tumor patients is relieved, the capacity of attacking tumor cells of the T cells embellished by the PD-1 recombinant virus is recovered accordingly, and the effect of immune cell treating is achieved.
Owner:安徽柯顿生物科技有限公司

4,4'-bis(2,4-diamidophenoxy)diphenylsulphone high-temperature-resistant epoxy adhesive and preparation method thereof

The invention relates to a 4,4'-bis(2,4-diamidophenoxy)diphenylsulphone high-temperature-resistant epoxy adhesive and a preparation method thereof. The 4,4'-bis(2,4-diamidophenoxy)diphenylsulphone high-temperature-resistant epoxy adhesive is composed of a component A and a component B in a mass ratio of 1:(1-2), wherein the component A is a copolymer prepared by reacting 4,4'-bis(2,4-diamido phenoxy)diphenylsulphone and epoxy resin; and the component B is a homogeneous-phase transparent solution with the solid content of 15-30%, which is prepared by reacting 4,4'-bis(2,4-diamidophenoxy)diphenylsulphone and aromatic dibasic acid anhydride in a strong-polarity non-proton organic solvent and diphenylsulphone. The preparation method comprises the following step: evenly mixing the component A and the component B in a mass ratio of 1:(1-2) at room temperature. The preparation technique is simple; and the adhesive has excellent comprehensive properties, can be widely used for bonding steel, copper, aluminum or any other metal with ceramic, glass, resin-base composite material or any other substrate, and has favorable industrialization prospects.
Owner:DONGHUA UNIV +1

Continuous extractive distillation separation method of dimethyl carbonate-methanol azeotropic mixture

The invention discloses a continuous extractive distillation separation method of a dimethyl carbonate-methanol azeotropic mixture, and relates to a continuous extractive distillation method. The technical process of the method is as follows: ethylene glycol is used as an extraction agent at normal pressure; the solvent ratio is 1-3; the separated dimethyl carbonate-methanol azeotropic mixture is fed from the middle part of a tower, the extraction agent is fed from the top of the tower, and the reflux ratio is 2; high-purity methanol is extracted from the tower top of an extractive distillation tower, and the dimethyl carbonate and the extraction agent are extracted from the tower bottom; the fraction at the tower bottom enters an extraction agent recovery tower, and the reflux ratio is 3; and dimethyl carbonate is extracted from the tower top, and the extraction agent extracted from the tower bottom can be recycled. The method disclosed by the invention adopts ethylene glycol as an extraction agent, and improves the separation effect of the dimethyl carbonate-methanol azeotropic mixture; and since ethylene glycol is a co-production product in synthesizing dimethyl carbonate by a transesterification method, the source is conveniently available, and the cost caused by introducing other substances is avoided.
Owner:SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY

Biological mixed bacterial fertilizer and preparation method and application thereof

The invention discloses a biological mixed bacterial fertilizer and a preparation method and application thereof. The biological mixed bacterial fertilizer is prepared from, by weight, 1-20 parts of a compound bacterial agent, 300-400 parts of organic materials, 500-600 parts of inorganic materials, 800-1000 parts of chemical fertilizers, 5-10 parts of trace elements, 300-500 parts of waste liquid, 30-50 parts of amino acid salts and 50-100 parts of additives.
Owner:英丽华

Method of recovery copper, nickel and noble metal in waste water and slag by combined technology of wet method and fire method

InactiveCN1718784AAdaptableSolve the adaptive problemProcess efficiency improvementSlagWastewater
A process for recovering the copper, Ni and noble metals from the sewage and dregs by the combination of wet method and fire method includes the wet process including extracting, Cu-Ni separation, removing Fe, extracting, and refining nickel carbonate, and the fire process including sintering and smelting to produce nickel matte and black copper. Its advantages are high recovery rate of Ni, Cu, Au, Ag and Pd, and no secondary pollution.
Owner:孙涛 +1

Cured tobacco perfume formulation

The invention provides a formula of a cured tobacco flavor, and pertains to the technical field of flavors. The formula of the cured tobacco flavor takes vanillin, isoamyl isovaleriate, aglaia odorate flower concrete extract, rhodinol and Maillard reactant as the main raw materials. The formula is applied to the tobacco to cause the cigarette to have a novel and nice fragrance, in particular to cause the cigarette to have a pure and mellow fragrance, thus obviously improving the impure fragrance and the smoke taste and causing the characteristic of the cigarette fragrance to be obvious. The formula has available flavor raw materials, and does not need to increase devices and change the production process. The addition amount is 1.2-2.5 per mill of the tobacco usually.
Owner:SHANGHAI BAIRUN INVESTMENT HLDG GRP CO LTD
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