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355 results about "Tris hydroxymethylaminomethane" patented technology

Preparation and application of magnetic nano-composite material gamma-Fe2O3/PDA (Polydopamine)-GA (Gallic Acid)

InactiveCN103721688ASolve the problems of low adsorption efficiency, difficult separation, easy to produce secondary pollution, etc.Reduce sensitivityOther chemical processesAlkali metal oxides/hydroxidesPyrrolidinonesEthyl group
The invention discloses preparation and application of magnetic nano-composite material gamma-Fe2O3 / PDA (Polydopamine)-GA (Gallic Acid). The preparation comprises the following steps of carrying out a hydrothermal reaction and calcinations to obtain a gamma-Fe2O3 nano particle carrier by taking FeCl3.6H2O with low price as an iron source, ethylene glycol (EG) as a reducing agent, polyvinylpyrrolidone (PVP) as a dispersing agent and a protective agent, and natrium aceticum (NaAc) as an alkali source; then wrapping a layer of polydopamine (PDA) in a buffer solution of tris (hydroxymethyl) aminomethane-hydrochloric acid (Tris-HCl) with pH of 8.5; and finally introducing gallic acid (GA) to an ethanol system by using 1-ethyl-(3-dimethylaminopropyl) carbodiimide hydrochloride and n-hydroxysuccinimide as cross-linking agents, wherein a specific synthetic schematic diagram is seen in attached drawing 1. Then the adsorption effects of the synthesized magnetic nano-particle on metal ions Cu<2+> and Pb<2+> are discussed, the detection effects of a glassy carbon electrode modified by the magnetic nano-particle on the metal ions Cu<2+> and Pb<2+> are researched. Results show that gamma-Fe2O3 / PDA-GA has excellent detection and adsorption effects on heavy metal ions in a water environment.
Owner:NANJING UNIV OF SCI & TECH

Super-hydrophobic super-lipophilic emulsion separating mesh membrane, and production method and application thereof

InactiveCN104826363AHas the effect of demulsification and separationHigh mechanical strengthNon-miscible liquid separationChemistryNon toxicity
The invention discloses a super-hydrophobic super-lipophilic emulsion separating mesh membrane, and a production method and an application thereof. The method comprises the following steps: 1, dissolving dopamine hydrochloride and tris(hydroxymethyl)aminomethane in water, and uniformly stirring to obtain a mixed solution A; 2, dipping a fabric net in the mixed solution A, and carrying out a reaction 1 to obtain a polydopamine membrane modified fabric net; 3, dissolving a siloxane precursor, a silane coupling agent 1, a silane coupling agent 2 and a titanium dioxide precursor in an organic solvent, and uniformly stirring to obtain a mixed solution 2; and 4, taking out the fabric net in step 2, washing, dipping the washed fabric net in the mixed solution B, adding water and ammonia water, and carrying out a reaction 2 to obtain the emulsion separating mesh membrane. The emulsion separating mesh membrane has the advantages of non-toxicity, harmlessness, environmental protection, easy cleaning and preservation, repeated use and good stability, can be widely used in separation of oil-water emulsions, and has a good separating effect.
Owner:TSINGHUA UNIV

Synthetic method and application of polydopamine-modified carbon nanotube composite material

The invention belongs to the field of nanotechnology, and particularly relates to a synthetic method and application of a polydopamine-modified carbon nanotube composite material. The synthetic method comprises the following steps in sequence: dispersing carbon nanotubes into dopamine-containing aqueous solution; quickly adding trismetyl aminomethane buffer solution into the dopamine-containing aqueous solution in which the carbon nanotubes are uniformly dispersed under magnetically stirring; mechanically stirring for 10 hours at room temperature; washing by water; and centrifugally separating to obtain the carbon nanotube composite material of which the surface is modified by polydopamine, wherein the carbon nanotube composite material shows high dispersibility in water. The polydopamine-modified carbon nanotube composite material adopts the carbon nanotubes as the framework, and therefore, a large specific surface area is provided; the polydopamine-modified carbon nanotube composite material is excellent in environmental stability and biocompatibility and high in dispersibility in water; the synthetic method is simple and low in cost; and the polydopamine-modified carbon nanotube composite material can be used as the substrate for analyzing metabolite micromolecule under high-throughput MALDI-TOFMS (Matrix Assisted Laser Desorption Ionization Time of Flight Mass Spectrometry).
Owner:FUDAN UNIV

Functionalized polydopamine derived carbon layer coated carbon substrate preparation method and application

The invention relates to the technical field of preparation of nanometer materials, and discloses a functionalized polydopamine derived carbon layer coated carbon substrate preparation method and application. The preparation method comprises the following steps: 1) immersing a carbon substrate into a trihydroxymethyl aminomethane aqueous solution, the pH value of which is adjusted to be alkaline, and then, reacting with dopamine hydrochloride to obtain a polydopamine coated carbon substrate; 2) carrying out high-temperature carbonization on the obtained polydopamine coated carbon substrate to obtain a polydopamine derived carbon layer coated carbon substrate; and 3) enabling the obtained polydopamine derived carbon layer coated carbon substrate to react with a bimetallic saline solution to obtain a functionalized polydopamine derived carbon layer coated carbon substrate. The functionalized polydopamine derived carbon layer coated carbon substrate is stable in structure, is high in electrochemical activity, and has a series of advantages of high specific capacitance and good rate capability and the like when serving as the electrode material of a super capacitor; and the preparation method thereof is simple and easy to operate.
Owner:DALIAN UNIV OF TECH

Hydrophilic antibacterial ultrafiltration membrane and preparation method for same

The invention relates to a preparation method for a hydrophilic antibacterial ultrafiltration membrane. The method comprises the following steps of providing a basic filter membrane; dissolving dopamine into a trihydroxymethyl aminomethane buffer solution to prepare a dopamine solution; coating the surface of the basic filter membrane with the dopamine solution to form a polydopamine coating on the surface of the basic filter membrane; coating the surface of the polydopamine coating with an amino-modified polyethylene glycol solution to form an amino-modified polyethylene glycol layer on the surface of the polydopamine coating; arranging antibacterial nanoparticles on the surface of the amino-modified polyethylene glycol layer to obtain the hydrophilic antibacterial ultrafiltration membrane.
Owner:TSINGHUA UNIV

Nasal peptide pharmaceutical formulation

InactiveUS20050158247A1Optimal therapeutic dose levelConstant ratePeptide/protein ingredientsAerosol deliveryEpitheliumDiluent
The invention provides a pharmaceutical formulation comprising: (1) THAM, which is tris(hydroxymethyl)aminomethane, as a selective absorbefacient to enhance through the nasal mucosa-lined epithelium the absorption of substances of peptide nature; and (2) a therapeutically effective amount of active nasal peptide, its pharmaceutically acceptable salt or its peptidic fragment; in a pharmaceutically acceptable, aqueous liquid diluent or carrier, said formulation being in a form suitable for nasal administration.
Owner:THERAPICON SRL

Method for modifying polytetrafluoroethylene-aramid blended fabric jointly by dopamine-polyethyleneimine-nanoparticles

The invention discloses a method for modifying polytetrafluoroethylene-aramid blended fabric jointly by dopamine-polyethyleneimine-nanoparticles; the method includes: adding polytetrafluoroethylene-aramid blended fabric, dopamine hydrochloride, polyethylenimine and nanoparticles into trihydroxymethyl-aminomethane / hydrochloride buffered solution, stirring, ultrasonically dispersing well, and continuously stirring at room temperature to allow for 2-24 h of reaction; after the reaction, taking out the blended fabric, sufficiently washing with deionized water to remove unreacted impurities on thesurface, and then drying in a vacuum oven to obtain the surface-modified polytetrafluoroethylene-aramid blended fabric. An organic-inorganic hybrid functional coating is constructed on the fiber surface through modifying; therefore, both active functional groups and greater surface roughness are imparted to the surface of the blended fabric, and the interface adhesion performance between the blended fabric and phenolic resin matrix can be improved through chemical bonding and mechanical interlocking.
Owner:LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Optimized in vitro cell-free protein synthesis system and application

The invention discloses an optimized in vitro cell-free protein synthesis system. The system comprises a cell extract, a carbohydrate material, a phosphate compound, a buffering agent and a DNA molecular template for encoding an exogenous protein, wherein the cell extract is a yeast cell extract inserted into a T7 RNA polymerase gene; the carbohydrate material is a mixture of glucose and maltodextrin; the buffering agent is a trihydroxymethyl aminomethane buffering agent; and the DNA molecule template is prepared by a nucleic acid isothermal amplification method, and a sequence as shown in SEQID NO.1 is inserted into the upstream of the coding sequence of the exogenous protein in the DNA molecular template. By optimizing, the cost of in vitro protein synthesis is reduced and the yield ofthe target protein is increased.
Owner:KANGMA SHANGHAI BIOTECH LTD

Liquid-based thin-layer cell preservation solution and use thereof

The invention discloses liquid-based thin-layer cell preservation solution and use thereof. The preservation solution comprises 5 to 28 volume percent of aldehyde solution, 0.1 to 3 volume percent of acid solution, 0.1 to 6 mass volume percent of chloride, 0.1 to 3 mass volume percent of tris(hydroxymethyl)aminomethane and the balance volume percent of double distilled water. The preservation solution of the invention can remove red blood cells, preserve white blood cells, timely fix the original state of cells of diagnostic value, soften mucilage and epidermal tissues, weaken mucous effect and separate effective cells from mucilage. The microscopic examination piece manufactured by using the preservation solution has clear microscopic examination view field and high cellular staining contrast and is widely suitable for gynecological and non-gynecological exfoliative cytological specimens and manual, semi-automatic or fully-automatic liquid-based cell substrate making processes. The production cost of the preservation solution is low, so the application and promotion of a liquid-based thin-layer cell detection technique are convenient.
Owner:山东龙奥生物技术有限公司

Crystalline Salts of a Potent HCV Inhibitor

This invention relates to novel tris(hydroxymethyl)aminomethane, choline and N-methyl-D-glucamine salt forms of the following Compound (1) and methods for the preparation thereof, pharmaceutical compositions thereof, and their use in the treatment of Hepatitis C Viral (HCV) infection:
Owner:BOEHRINGER INGELHEIM INT GMBH

Method for biocatalyzing ester exchange reaction of high acid value lipid to produce biodiesel oil

The invention relates to a process for preparing diesel fuel through biological catalyzed high acid value grease ester interchange which comprises, using alkaline substance such as trishydroxy methyl amino methane as addition agent, subjecting high acid value grease as raw material to ester exchange reaction with short-chain fatty acid ester at the presence of biological enzyme catalysis, separating the reaction product to obtain end product of biological diesel.
Owner:SOUTH CHINA UNIV OF TECH

Zinc-cobalt sulfide/carbon nano negative electrode material and preparation method thereof

The invention discloses a zinc-cobalt sulfide / carbon nano negative electrode material and a preparation method thereof. The negative electrode material is of a hollow irregular spherical shell structure formed by distributing zinc-cobalt sulfide nano particles in a carbon matrix and on the surface of the carbon matrix, wherein the mass ratio of the zinc-cobalt sulfide to the carbon is (0.5 to 4.0): 1. The method comprises the steps of (1) adding a surfactant and 2-methylimidazole into an alcoholic solution, stirring, adding a zinc source alcoholic solution, stirring, standing and centrifuging;(2) dissolving in an alcoholic solution, adding a surfactant and 2-methylimidazole, stirring, adding a cobalt source alcoholic solution, stirring, carrying out solvothermal reaction, cooling, centrifuging, washing and drying; (3) adding trihydroxymethyl aminomethane into an alcoholic solution, stirring, adding dopamine hydrochloride, stirring, carrying out suction filtration, washing and drying;and (4) pre-roasting, cooling, mixing with sulfur powder, roasting and cooling. The material provided by the invention is excellent in electrochemical performance. The method provided by the inventionis mild, low in cost, environmentally friendly and suitable for industrial production.
Owner:CENT SOUTH UNIV

Novel coronavirus earlier-stage screening method

A novel coronavirus earlier-stage screening method disclosed by the invention can be used for detecting the novel coronavirus, and is particularly used for screening the SARS-CoV-2IgA antibody in theearly stage. A kit comprises an SARS-CoV-2 magnetic bead coating material used as R1, containing a magnetic bead coating material trihydroxymethyl aminomethane buffer solution coated by an SARS-CoV-2recombinant antigen, wherein the pH value is 7.1-7.4; and an acridinium ester marker of the anti-human IgA antibody as R2, wherein the acridinium ester marker is a 2-(N-morpholine) ethanesulfonic acidbuffer solution containing an acridinium ester labeled mouse anti-human IgA monoclonal antibody. The kit and the SARS-CoV-2IgA antibody immunoassay reagent disclosed by the invention can be used forsupplementing and diagnosing new coronal pneumonia at an earlier stage, and have the characteristic of accurate detection result.
Owner:GUANGZHOU KANGRUN BIOTECHNOLOGY CO LTD +1

Preparation method of modified activated carbon fiber for adsorbing ultra-micro sulfur dioxide

The invention relates to a preparation method of modified activated carbon fiber for adsorbing ultra-micro sulfur dioxide, belonging to the technical field of gas adsorption and separation. The method comprises the following steps: taking viscose-based activated carbon fiber which is oxidized by dilute nitric acid as a matrix, and taking tris hydroxyl methyl aminomethan, alanine, serine and arginine as modifiers; and successfully preparing chemically modified activated carbon fibers in which the surfaces are modified by much amidogen through a hydro-thermal reaction under certain conditions. Compared with the prior art, the preparation method has the following advantages: (1) a micromolecule modifier is used for chemically modifying the surface to keep the structural advantage of the activated carbon fibers such as high specific surface and more micro pores so that the activated carbon fibers simultaneously have abundant micro-pore structures and high activity reaction surfaces to represent relatively longer penetrating time and larger saturation adsorption capacity; (2) the modifying method is temperate in condition, small in pollution, energy-saving and environment-friendly, and easy for scaled production; and (3) the modified absorbing capacity can be increased to that 1 g of the absorbent can absorb 40-60 mg of SO2, which is improved by 4-6 times compared with the absorbing capacity of the absorbent before the modification.
Owner:DALIAN UNIV OF TECH

Photo-thermal conversion material, preparation method and applications thereof

The invention discloses a photo-thermal conversion material, which has a double-layer structure, wherein the double-layer structure is a polydopamine layer on a polyurethane sponge layer, the top layer of the double-layer structure is dark black, the thickness of the top layer is 0.5-2.0 mm, and the total thickness of the double-layer structure is 10-25 mm. The preparation method of the photo-thermal conversion material comprises: S1, purifying polyurethane sponge; S2, loading polydopamine: immersing the polyurethane sponge purified in the step S1 into a container filled with a hydrochloric acid-containing dopamine trihydroxymethyl aminomethane buffer solution (Tris-HCl buffer solution), and carrying out a water bath reaction for 4-24 h at a temperature of 25-80 DEG C without any disturbance condition and container sealing to obtain modified sponge; and S3, drying. The invention also provides applications of the photo-thermal conversion material. According to the invention, with the photo-thermal conversion material, the problems of low efficiency, high cost, complex process and the like of the existing solar steam photo-thermal conversion are solved.
Owner:SDIC XINJIANG LUOBUPO POTASH CO LTD

Preparation and application of Fe3O4@C@MoS2 composite material with core-shell structure

The invention discloses a preparation and an application of an Fe3O4@C@MoS2 composite material with a core-shell structure. The preparation method includes the following steps: S1. adding FeCl3 and NaOH into water, uniformly mixing, loading the mixed solution into a polytetrafluoroethylene stainless steel autoclave, and reacting to obtain uniform cubic Fe2O3 particles; S2, adding the Fe2O3 particles prepared in S1 and dopamine hydrochloride into a trimethylolaminomethane buffer solution, stirring and reacting at room temperature with a magnetic stirrer, then washing the reaction product, and collecting an Fe2O3@PDA composite with a core-shell structure through a centrifugal method; S3. adding the Fe2O3@PDA prepared in S2, ammonium molybdate tetrahydrate and thiourea into water in sequenceand stirring uniformly, washing the product after the reaction is finished, and collecting Fe2O3@PDA@MoS2 composite through the centrifugal method; and S4. calcining the Fe2O3@PDA@MoS2 composite underthe flow of hydrogen and argon to finally obtain the Fe3O4@C@MoS2 composite. The Fe3O4@C@MoS2 composite material prepared by the method has excellent microwave absorption performance.
Owner:ANHUI UNIV OF SCI & TECH

Preparation method of frozen diluent of sheep semen and application of preparation method

InactiveCN108094409AAvoid Application DefectsIncrease vitalityDead animal preservationYolkPenicillin
The invention discloses a preparation method of a frozen diluent of sheep semen and an application of the preparation method. The preparation method of the frozen diluent of the sheep semen comprisesthe following steps: firstly, accurately weighing tris(hydroxymethyl) aminoethane, dihydrate trisodium citrate, fructose, an inositol compound, ethanediol or glycerinum, and oxytocin, adding the materials into ultrapure water, dissolving, adding a fresh yolk centrifuged liquid supernatant, penicillin and streptomycin, mixing evenly, fixing the volume after adjusting the pH value to 6.8-7.2, thus obtaining the frozen diluent of the sheep semen. The inositol compound is used to replace an antifreeze protein, the defect of the application of the antifreeze protein is avoided, meanwhile, the oxytocin is added when the semen is conveyed, and the sperm vitality and the acrosomal integrity are improved, so that the fertility rate is increased.
Owner:刘铮铸

Bionic nanofiltration membrane for extracting humic acid from landfill leachate membrane concentrate and preparation method of bionic nanofiltration membrane

InactiveCN111013399ADeposition method is simpleModulation of surface propertiesSemi-permeable membranesMembranesEnvironmental engineeringNanofiltration
The invention discloses a bionic nanofiltration membrane for extracting humic acid from landfill leachate membrane concentrate and a preparation method of the bionic nanofiltration membrane. The preparation method of the bionic nanofiltration membrane comprises the following steps: firstly, dissolving polyethyleneimine, an oxidizing agent and dopamine hydrochloride in a trihydroxymethyl aminomethane hydrochloride buffer solution, and fully mixing to prepare a membrane modification solution; then, fixing base membranes with different molecular weight cutoff into an interface reaction device, pouring the membrane modification liquid, and enabling the membrane modification liquid to be in full contact with the surfaces of the base membranes for deposition reaction; finally, after reaction fora period of time, enabling a polydopamine bionic layer to grow on the surfaces of the base membranes, taking out the modified base membranes and cleaning, and thus obtaining the bionic nanofiltrationmembrane. According to the bionic nanofiltration membrane, the rejection rate of humic acid can be greatly increased, so that enrichment, concentration and extraction of humic acid in the landfill leachate membrane concentrate are realized; in addition, the bionic nanofiltration membrane is endowed with excellent anti-pollution performance due to high hydrophilicity of the polydopamine bionic layer.
Owner:FUZHOU UNIV

High-sensitivity high-linearity D-D dimer detection kit and application method thereof

The invention discloses a high-sensitivity high-linearity D-D dimer detection kit and an application method thereof. A reagent one is a 30mmol / L trihydroxymethyl aminomethane buffer solution. A reagent two comprises a mixed liquid of large-diameter mouse-anti-human D-D dimer monoclonal antibody latex particles with a concentration of 0.01-0.04% (w / v) and small-diameter mouse-anti-human D-D dimer monoclonal antibody latex particles with a concentration of 0.05-0.2% (w / v). Specific antibody content in the small-diameter mouse-anti-human D-D dimer monoclonal antibody latex particles is 0.05-10% of that in the large-diameter mouse-anti-human D-D dimer monoclonal antibody latex particles. Through optimizing the average diameter of large and small particles and concentrations thereof in the reaction system, D-D dimer high-sensitivity detection under low-concentration situation can be realized, and detection range under high-concentration situation can be expanded.
Owner:NINGBO RUI BIO TECH

Pegylation polyoxometallate and preparation method thereof

The invention discloses pegylation polyoxometallate and preparation method thereof. According to the invention, polyethylene glycol and polyoxometallate are connected by utilizing a covalent bond mode, and a pegylated tungsten-containing polyoxometallate hybrid polymer is obtained. The method comprises the following synthesis steps: 1) reacting polyethylene glycol with succinic anhydride to obtain carboxyl polyethylene glycol; 2) carrying out an amidation reaction between the carboxyl polyethylene glycol and trihydroxymethyl aminomethane to obtain trihydroxymethyl polyethylene glycol; and 3) reacting the trihydroxymethyl polyethylene glycol and the tungsten-containing polyoxometallate to obtain the hybrid compound. The pegylated polyoxometallate hybrid compound is synthesized in the covalent bond mode. According to the synthetic method, a novel organic-inorganic hybrid compound can be obtained, the preparation method is easy and feasible, and the reaction process is easy to control, simple in purification and high in yield. According to the hybrid compound, the excellent performances of the inorganic polyoxometallate and organic polyethylene glycol are kept, so that the hybrid molecule has potential application values in the aspects of catalysis, materials, medicines and the like.
Owner:NANKAI UNIV

Method and detection kit for detecting cervical fluid heme

The invention provides a method for detecting cervical fluid heme. The method comprises the following steps of: wiping at the cervical part with little pressure to obtain the fluid; processing the fluid with a tri-hydroxymethyl aminomethane-hydrochloric acid buffer solution with a pH value of 7.4; and then reacting with a color producing reagent, comparing with a shade guide and recording the detection result. The method provided by the invention is simple and practical and low in cost, and can quickly screen the sample without heme, the sample with heme and the sample possibly with heme in the cervical fluid, thereby providing preparation for further screening. The invention also relates to a detection kit for detecting the cervical fluid heme.
Owner:青岛宏利源高新技术有限公司

Magnetic bead composition for improving nucleic acid extraction rate and application of magnetic bead composition

The invention belongs to the field of molecular biology technologies, and particularly relates to a magnetic bead composition for improving a nucleic acid extraction rate and an application of the magnetic bead composition. The magnetic bead composition comprises the following components by concentration: nano magnetic beads of 1mg / mL, polyethylene glycol 8000 of 0.018-0.026mol / L, sodium chloride of 2.2-2.6mol / L, an ethylenediamine tetraacetic acid solution of 0.5-2mol / L, and a trihydroxymethyl aminomethane solution of 10-20mmol / L. The magnetic bead solution provided by the invention can strengthen the adsorption efficiency of the magnetic beads and nucleic acid and can greatly improve the extraction rate; and especially for extraction of a trace-amount nucleic acid sample, the magnetic bead solution is more obvious in advantage, and reduces the operation time.
Owner:广州奇辉生物科技有限公司

Extracting method for plant chloroplast total protein and special extract therefor

The invention discloses an extracting method for a chloroplast total protein and a special extracting solution thereof. The special extracting solution for the chloroplast total protein is the aqueous solution which contains the following matters with the end concentration: 90 to 100mM ethylenediaminetetraacetic acid, 90 to 100mM trihydroxymethyl aminomethane, 40 to 60mM sodium tetraborate, 0.9 to 1.1 volume percent Triton X-100, 1.9 to 2.1 volume percent beta-mercaptoethanol, and 28-32g / 100ml sucrose. The high quality chloroplast total protein obtained through the special extracting solution and extracting method solves the problem of preparing the chloroplast total protein sample in the dielectrophoresis, and simultaneously has the mass spectrum compatibility. The method can be applied to the proteomics study as a general chloroplast total protein extracting method.
Owner:INST OF BOTANY CHINESE ACAD OF SCI

Preparation of fibrous catalyst loaded with metal nanoparticles and application

The invention discloses preparation of a fibrous catalyst loaded with metal nanoparticles and application. The preparation method comprises the following steps: adding metal salt into a solution system containing trihydroxy methyl aminomethane, fiber and dopamine hydrochloride to obtain mixed solution, then stirring, polymerizing dopamine to obtain polydopamine, wrapping fiber with the polydopamine, and simultaneously loading the metal nanoparticles; then, carrying out heat annealing treatment under the atmosphere of inertial gas to prepare a fiber@nitrogen-doped carbon metal compound material, namely the fibrous catalyst loaded with metal nanoparticles. The preparation and the application disclosed by the invention have the beneficial effects that by setting of a whole process flow of thepreparation method and improvement on reaction conditions and parameters of all key process steps, the activity and the cycling stability of the loaded nano-metal catalyst can be effectively improved.
Owner:HUAZHONG UNIV OF SCI & TECH

Electrophoresis gels

A polyacrylamide gel utilising a buffer system comprising Tris(hydroxymethyl)aminomethane at the concentration range 0.15 to 0.25 M titrated with hydrochloric acid to a pH between 6.5 and 7.5. The gel is substantially stable to polyacrylamide hydrolysis during storage for at extended periods and has an acceptable shelf-life of at least 6 months after storage at about 4° C.
Owner:DYCENT BIOTECH SHANGHAI CO LTD

Stainless steel surface three-dimensional nanocarbon film and preparation method thereof

The invention relates to a stainless steel surface three-dimensional nanocarbon film and a preparation method thereof. According to the technical schem, the preparation method comprises the following steps: firstly, performing electrochemical anode oxidation treatment on stainless steel in a sodium dihydrogen phosphate solution, wherein the surface of the stainless steel is pretreated; then under a stirring condition, placing the stainless steel subjected to electrochemical anode oxidation treatment in a mixed solution of dopamine and trihytdroxy methyl-aminomethane for 4-24 hours, taking out and cleaning; then raising to 500-800 DEG C from a room temperature at a temperature raising rate of 5-15 DEG C / min in an argon atmosphere, insulating heat for 3-10 hours, and naturally cooling with a furnace to obtain the stainless steel surface three-dimensional nanocarbon film. The stainless steel surface three-dimensional nanocarbon film has the characteristics of simple process, environment friendliness and low cost; and the stainless steel surface three-dimensional nanocarbon film is regular and ordered in structure, uniform in components, high in nano hole density, large in carbon film specific surface area, controllable in pore diameter, pore depth and carbon film thickness, and compact in combination with a base material, and does not involve other impurity elements. According to the stainless steel surface three-dimensional nanocarbon film, the stainless steel corrosion resistance performance, the high temperature resistance, the electrochemical sensing performance and the biological medicine performance can be improved.
Owner:WUHAN UNIV OF SCI & TECH

Preparation method of temperature-responsive self-repairing super-hydrophobic fabric

ActiveCN109576997AWith temperature responseMeet the requirements of superhydrophobicityLiquid repellent fibresPolymer scienceCotton cloth
The invention discloses a preparation method of a temperature-responsive self-repairing super-hydrophobic fabric, and belongs to the field of super-hydrophobic fabrics. In the method, dopamine hydrochloride and tris(hydroxymethyl)aminomethane are adopted to prepare a bionic polydopamine solution, the high adhesion, namely, the role of double-faced adhesive tape of the polydopamine is utilized to make polycarbonate firmly adhere to the fabric surface, a good rough structure is constructed on fabric cotton cloth as polycarbonate can swell in paraxylene, then low-surface-energy substances octadecylamine and 1-dodecanethiol are adopted to modify the fabric surface, and the temperature-responsive self-repairing super-hydrophobic fabric is obtained. Tests show that the fabric still can meet thesuper-hydrophobicity requirement after being subjected to 100 times of fabrication and 30 times of washing, the fabric has no super-hydrophobic property when wetted by water, but the super-hydrophobicproperty of the fabric can be restored after the fabric is dried for 80 min at 60 DEG C, and thus conversion between a super-hydrophobic fabric and a non-super-hydrophobic fabric is realized.
Owner:厦门市北顶纺织科技有限公司

Modified polymer film and preparation method and application thereof

The invention discloses a modified polymer film as well as a preparation method and application thereof, and particularly relates to the field of modified polymer films. The preparation method comprises the following steps: dropwise adding a sulfanilic acid diazonium salt solution into Na<+> intercalated MXene, and after reaction, centrifuging, filtering, washing, ultrasonically treating and freeze-drying to obtain sulfonated MXene powder; immersing a polymer film in a GA / polyethyleneimine (PEI) mixed solution containing trihydroxymethyl aminomethane and metal salt, and reacting to obtain a GAcoating modified polymer film; and depositing the sulfonated MXene powder on the GA coating modified polymer film, and repeating the operations to obtain the single-layer or multi-layer GA / MXene modified polymer film. According to the invention, two methods, namely vacuum assisted suction filtration and layer-by-layer self-assembling, are combined, and the method has the characteristics of uniform film coating, controllable film thickness, better stability, low energy consumption and easiness in operation. In addition, the prepared modified polymer film has the functions of efficiently removing medium and small molecular toxins and having good oxidation resistance and protein adsorption resistance.
Owner:TIANJIN POLYTECHNIC UNIV

Caron-coated stannous oxide compound and preparation method and application thereof

The invention discloses a carbon-coated stannous oxide compound. The carbon-coated stannous oxide compound is prepared by the steps of dissolving trihydroxymethyl aminomethane into water, stirring and preparing into a buffer solution; weighing the buffer solution, adding stannous oxide, stirring to form a black turbid solution; adding dopamine and continuously stirring; performing washing, centrifuging and drying; and performing calcining in nitrogen atmosphere to obtain the carbon-coated stannous oxide composite material. Dopamine is used as the carbon source for coating the surface of SnO, so that volume expansion of SnO in a circulation process is relieved, thereby improving the cycling performance in the application when SnO is used as a negative electrode material of a sodium ion battery; in the synthesis process, the solvent is non-toxic and harmless, the cost is relatively low and the operation is simple; the carbon-coated stannous oxide composite material has the most major advantage of excellent cycling performance; the initial-circle charging specific capacity can be close to 500mAh / g and the capacity is barely attenuated after 300 cycles, so that possibility is provided for the actual application of the composite material in the sodium ion battery material in the future.
Owner:NORTHEAST NORMAL UNIVERSITY
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