3405 results about "Acid value" patented technology

Contact of a crude feed with one or more catalysts produces a total product that include a crude product. The crude feed may a total acid number of at least 0.3. The crude product is a liquid mixture at 25° C. and 0.101 MPa. The crude product may have a total acid number of at most 90% of the total acid number of the crude feed. At least one of the catalysts may include one or more Column 6 metals of the Periodic Table and one or more Column 10 metals of the Periodic Table. One or more other properties of the crude product may be changed by at least 10% relative to the respective properties of the crude feed.

The present invention provides a toner and a developer which includes the toner. The toner is produced in an aqueous medium and includes at least a binding resin, a colorant and a dispersant which disperses the colorant. The binding resin contains 50% by mass to 100% by mass of a polyester resin, and the colorant is a pigment whose surface is given an acid treatment. The acid value of the dispersant is 1 mg KOH / g to 30 mg KOH / g, and the amine value of the dispersant is 1 mg KOH / g to 100 mg KOH / g.

A photoreceptor including an electroconductive substrate; a photosensitive layer; and optionally a protective layer, wherein an outermost layer thereof includes a filler, an organic compound having an acid value of from 10 to 700 mg KOH / g and at least one compound selected from the group consisting of compounds having the following formulae (1) and (2): wherein R1 (R3) and R2 (R4) independently represent a substituted or an unsubstituted aromatic hydrocarbon group, or a substituted or an unsubstituted alkyl group, and optionally share bond connectivity to form a heterocyclic group including a nitrogen atom; Ar1 (Ar3) and Ar2 (Ar4) independently represent a substituted or a unsubstituted aromatic ring group; k (K) and m (M) independently represent 0 or an integer of from 1 to 3, wherein k (K) and m (M) are not 0 at the same time; and n (n′) represents an integer of from 1 to 3.

A coating composition which comprises (A) a resin having a glass transition temperature of 50 to 120 DEG C., a number average molecular weight of 2,000 to 100,000, a hydroxyl value of 50 to 150 mgKOH / g and an acid value of 1 to 25 mgKOH / g, which is produced by copolymerizing 10 to 90 percent by weight of (a) a (meth)acrylic acid ester of a C1 to C12 alkyl alcohol, 10 to 50 weight % of (b) a first polymerizable double bond-containing and hydroxyl group-containing monomer, 0.1 to 10 weight % of (c) a polymerizable double bond-containing and carboxyl group-containing monomer, 0 to 20 weight % of (d) styrene, 0 to 20 weight % of (e) acrylonitrile and 0 to 10 weight of (f) a second polymerizable double bond-containing monomer, (B) at least one compound selected from the group consisting of a polyisocyanate compound having two or more unblocked isocyanate groups and / or blocked isocyanate groups in the molecule and an aminoplast resin, (C) a dispersing component of at least one inorganic oxide sol selected from the group consisting of an aluminum oxide sol, a silica sol, a zirconium oxide sol and an antimony oxide sol, wherein an amount of a nonvolatile matter of component (C) is 5 to 60 percent by weight based on a total amount of nonvolatile matter of resin (A), compound (B) and component (C). The coating composition provides cured films having excellent weathering resistance, light resistance, stain resistance, stain-removing property, chemical resistance, moisture resistance and appearance and is environmentally friendly and safe.

A motor vehicle having an internal combustion engine and a lubricating oil circulation system provides estimates of the distance remaining before an oil change becomes imperative. An indirect estimate of the depletion of various additives and the deterioration of oil operating characteristics is based on engine operating variables including oil temperature, ignition timing and engine load. The limit of depletion of total base number is dynamic, since it is set against total acid number and the two figures are independently calculated.

The object of the present invention is to provide a polycarbonate resin composition which has excellent transparency and durability against molding heat, which gives a molded article having an excellent mold release property, reduced strains, improved cracking resistance and, preferably, weatherability, and which is particularly suitable for a transparent member for a vehicle, pellets thereof and a molded article thereof, and the present invention provides a polycarbonate resin composition obtained by blending 100 parts by weight of a polycarbonate resin (Component A) and 0.005 to 2 parts by weight of a full ester (Component B) from an aliphatic polyhydric alcohol having 4 to 8 hydroxyl groups and 5 to 30 carbon atoms and an aliphatic carboxylic acid having 10 to 22 carbon atoms, said Component B having a 5% weight loss temperature, measured by TGA (thermogravimetric analysis), of 250 to 360° C. and having an acid value of 4 to 20, pellets thereof and a molded article thereof.

A toner which is negatively charged to develop an electrostatic latent image is provided that contains a colorant; and a binder resin, wherein the toner has an acid value of from 5 to 20 mg KOH / g and an amine value of from 0.5 to 10 mg KOH / g.

An object of the invention is to provide a pressure-sensitive adhesive sheet. Provided is an acrylic polymer for use in a pressure-sensitive adhesive composition for a touch screen panel, the acrylic polymer being obtained by copolymerizing monomer components comprising (a) a (meth)acrylic acid ester monomer having a C1-12 hydrocarbon group, (b) a hydroxy group-containing (meth)acrylic acid ester monomer, (c) an amide group-containing monomer, and (d) a vinyl ester monomer. The acrylic polymer has an acid value of 0.1 mg KOH / g or less, a weight-average molecular weight of 400,000 to 2,000,000, a Tg of −80 to 0° C., and a permittivity of 3 to 6.

A process for preparing the biological diesel oil from the animal fat or vegetative oil with high acid number includes esterifying by glycerine under existance of strong acid catalyst, distilling in azeotropic solvent for removing water, mixing with methanol, transesterifying reacting to remove glycerine, water washing, and low-temp treating for removing high-smelting-point substances to obtain methyl ester of fatty acid, which is just the biological diesel oil.

A polymerizable composition which comprises a cycloolefin monomer (A), a filler (B), a polymer (C) having a carboxyl group or a carboxylic acid anhydride group and having an acid value of 0.1 to 100 mgKOH / g, and a metathesis polymerization catalyst (D). The polymerizable composition comprises a cycloolefin monomer and a large amount of a filler, and has a low viscosity and is excellent in fluidity, and further can provide a molded product which is excellent in the lowness of dielectric constant, the lowness of dielectric loss tangent, the lowness of linear expansion coefficient, high heat resistance and adhesiveness, and further is free of bubble inclusion.

The present invention provides a recording ink including a composite pigment particle, a water-soluble solvent, and water, wherein the composite pigment particle is a primary particle coated with a coating resin, wherein the primary particle is a white pigment on the surface of which an oil-soluble dye is adsorbed or attached. In one aspect, the white pigment is preferably at least one selected from a white inorganic pigment, a pearl pigment, and an extender pigment, in another aspect, the coating resin is preferably one of a (meth)acrylic resin, a polyester resin, and a polyurethane resin, wherein the acid value of the coating resin is from 50 mgKOH / g to 250 mgKOH / g, and in another aspect, an average particle diameter (D50%) of the composite pigment particle is preferably 150 nm or less.

An acrylic polymer powdery material, which is a particularly useful powdery material as a modifier for cementitious material, comprising fine particles of a core-shell structure comprising a core polymer being comprised of an acrylic polymer having a glass transition temperature (Tg) of -20-+15° C., a weight average molecular weight of 100000-2000000, an acid value of 25 mg KOH / g or less and a shell polymer being comprised of an acrylic polymer having a Tg of 50-90° C., a weight average molecular weight of 100000-2000000, an acid value of 30-130 mg KOH / g, wherein the weight ratio of the core polymer and shell polymer is 30 / 70-80 / 20 (% by weight).

The invention provides a preparation method of annular phosphonate or annular organic phosphate flame retardant. The steps are that (1) trimethylolpropane and trimethyl phosphate or triethyl phosphate are taken as the material, and react to synthesize into midbody under the condition of catalyzer; (2) phosphonate or organic phosphate is added into the midbody and is heated, and then the product of annular phosphonate or annular organic phosphate flame retardant can be obtained. The phosphite ester is selected from trimethyl phosphate and triethyl phosphate. The phosphonate is selected from dimethyl-phosphine and diethyl ethyl phosphine. The organic phosphate is selected from trimethyl phosphate, triethyl phosphate, phosphate propyl, tributyl phosphate and tricresyl aromatic ester. The invention overcomes the shortcomings of the prior art, the new preparation method of annular phosphonate or annular organic phosphate flame retardant is environment-friendly, solution is not needed, and the operation is simple. The termination product has excellent color and luster, low acid value and excellent viscosity; and does not need additional decoloration.

The invention discloses a polyester resin with a high acid value and a low acid value for an environment-friendly dry blended low-gloss weather-resistant powder coating. The polyester resin is made from the following raw materials by weight percentages by virtue of esterification and condensation reaction: 15%-60% of polyol, 30%-65% of polyacid, 0%-5% of a branching agent, 5%-15% of an acidolysis agent and 0.01%-0.15% of an esterification catalyst. The invention further discloses a preparation method of the polyester resin with the high acid value and the low acid value for the environment-friendly dry blended low-gloss weather-resistant powder coating. Thepolyester resin with the high acid value and the polyester resin with the low acid value have the characteristics of proper glass transition temperature, proper softening point and good storage stability. A powder coating made by curing beta-hydroxyalkyl amide with the polyester resin has the advantages of excellent deglossing effect and good mechanical properties.

Oil color and luster acid value integrated automatism detection instrument and its method based on computer visual, it relates to the oil detection field. It solves the disadvantage that not integrated, big error, not automatism in the exist technology. The CCD numeral camera links with the PC, the PC outputs the signal to the control instrument and the locale technology parameter adjustment control groupware separately, the control end of the control instrument links with the controlled end of the execute setup, the light source, CCD numeral camera and the sample bottle which is set in the electromagnetism beater are set in the same axes and set in the illumination box. The steps are: firstly, start up and set the parameter; value whether detect the acid value, if it detects, collects the oil sample and add in reagent, then titrates liquid collects the image to value whether reach the end point, if it does not, titrates again, if it reaches, stop titrating and calculates the acid value, detects twice and calculates its average value and output; if it is not, detects the color and luster, compares the standard image data and the collection image data twice, and output the data. This invention based on equipment, its error is small, and the veracity and reliability is high.

There are provided a liquid composition for making pigment fixed having a high resistance to rubbing and a good dry-cleanability; an ink set including the liquid composition for making pigment fixed and an ink composition excellent in terms of color intensity, discharge stability, and adhesiveness; and a method for producing ink-jet-recorded matter on a fabric having a high resistance to rubbing and good dry-cleanability using the liquid composition for making pigment fixed and the ink composition.The liquid composition for making pigment fixed according to the present invention contains at least a reactant and polymer fine particles synthesized from an alkyl (meth)acrylate and / or cyclic alkyl (meth)acrylate, the glass transition temperature and acid value of the liquid composition being equal to or lower than −10° C. and equal to or lower than 100 mg KOH / g, respectively.

Provided is an aqueous binder for inorganic fibers, which is formaldehyde-free, has excellent strength, and is suitable for use under conditions of weakly acidic to weakly basic, and by which a cured product composed of the binder having excellent strength is obtained, and an thermal and / or acoustical insulation material made of inorganic fiber using the same. The thermal and / or acoustical insulation material is molded by using an aqueous hinder for inorganic fibers including: an acrylic resin with an acid value of 350 to 850 mgKOH / g; a crosslinking agent containing at least one dialkanolamine; and a curing accelerator, in which a molar ratio of the total number of the hydroxyl groups and imino groups in the crosslinking agent to the total number of carboxyl groups in the acrylic resin is 0.8:1 to 1.5:1, and in which pH of the hinder is adjusted to 6.0 to 8.0 with a volatile basic compound.

The invention discloses a method for preparing a multi-sulfonic acid group functionalized ionic liquid. In the method, a poly-nitrogen tertiary amine reacts with a sultone to an obtain multi-sulfonic acid radical betaine, and the obtained betaine is subjected to acidification by an acid to obtain the multi-sulfonic acid group functionalized ionic liquid. The ionic liquid prepared by the invention has the characteristics of high thermal stability, high acid value, low synthesis cost and good catalytic effect, etc.

A method for producing highly acid value crude oil consists of preheating the crude oil which is total acid number of more than 0.5mg potassium hydroxide per gram after the pretreatment and injecting them into the fluidized catalytic cracker to contact the catalyst, and reacting in catalytically cracked reaction condition, separating the oil gas and the catalyst, in which the oil gas is put into the subsequent separation system, while the catalyst can be circularly used after stripping and regenerating. The method is characterized in that it is of strong industrial practicability, low running cost and fine deacidification effect and so on.

An alkali development type photocurable composition comprises (A) an alkali-soluble macromolecular binder having a weight-average molecular weight in the range of 5,000 to 100,000 and an acid value in the range of 50 to 150 mg KOH / g and obtained by causing (d) a compound possessing one glycidyl group in its molecule to react with a carboxyl group of (A-1) a copolymer of (a) an ethylenically unsaturated bond-containing compound possessing one carboxyl group in its molecule with (b) an ethylenically unsaturated bond-containing compound possessing neither hydroxyl group nor acidic group in its molecule, or a carboxyl group of (A-2) a copolymer of the compounds (a) and (b) mentioned above and (c) an ethylenically unsaturated bond-containing compound possessing a hydroxyl group and then causing (e) a polybasic acid anhydride to react with a hydroxyl group caused by the above reaction, (B) an inorganic powder, (C) a photopolymerizable monomer, (D) a photopolymerization initiator, and (E) an organic solvent. By using this composition, such calcined patterns as a conductor pattern and a dielectric pattern of high fineness may be formed by the photolithographic technique.

The invention relates to a preparation method of cosmetics camellia oil. High-quality camellia seeds are selected to be used as the raw material; the camellia seeds are roasted under the negative pressure and at the lower temperature, and are husked after natural cooling and are squeezed at the room temperature to obtain high-quality crude oil with low acid value and pale yellow color; impurities are removed through filtration under the heating condition, alkali refining and ethanolic extracting two-stage process is utilized for acid stripping and de-coating; then the mixture composed of active carbon and floridin is used as de-coloring agent for de-pigmentation; peroxide and unclean flavor are removed through deodorization; then the drying winterization is acted; finally, the cosmetics camellia oil is obtained, wherein, the acid value is less than 0.1 mgKOH / g, the peroxide value is less than 0.5 mmol / kg, the appearance is colourless approximately as well as clear and translucent, and no unclean flavor exists. The cosmetics camellia oil reaches or exceeds the requirement of the national standard GB11765-2003 on first level expressed tea-seed oil, and can be directly used for manufacturing the cosmetic such as skin care oil for babies; in addition, an edible camellia oil fabrication plant can be improved for production, thereby lowering the investment cost greatly.

The present invention is solid catalysis process of preparing biodiesel oil continuously with high acid value material, and belongs to the field of grease chemistry and regenerable energy source technology. The process includes following four steps: material pre-treating, reaction, methanol rectifying recovery and vacuum rectification of fatty acid methyl ester; and features the high acid value material, such as acidified oil, waste edible oil, etc. The present invention has the advantages of low material cost, high activity and easy separation of the solid catalyst, high esterification efficiency, high product purity, high yield, less waste, no pollution, etc.

This invention provides cellulose ester interpolymers, and methods of oxidizing cellulose interpolymers and cellulose ester interpolymers. The invention also provides routes to access carboxylated cellulose ester derivatives with high acid numbers wherein the carboxyl group is attached directly to the cellulose backbone by a carbon-carbon bond. Through functionalization of an intermediate aldehyde, the corresponding cationic or zwitterionic cellulose ester derivatives can also be accessed. The interpolymers of the present invention have a number of end-use applications, for example, as binder resins in various types of coating compositions and as drug delivery agents.

A toner for image formation is provided, which is produced by dispersing in an aqueous solvent a toner composition which includes a composition thermally soluble in an organic solvent and a coloring agent, thereby forming toner particles, wherein the thermally soluble composition includes (a) a polyester having an acid value and (b) a metal alcolate and / a metal chelate compound. The toner is capable of attaining image fixing at a sufficiently low image fixing temperature and a sufficiently broad image fixing temperature range for use in practice. Furthermore, toner containers such as a toner cartridge and a process cartridge are provided, which are loaded with the toner. Such toner containers can be detachably mounted on an image forming apparatus.

In the invention, a polyester resin having dicarboxylic acid constitutional units and diol constitutional units wherein 5 to 60 mol % of the diol constitutional units has a cyclic acetal skeleton is produced by a process including an oligomerization step and a polymerization step. In the oligomerization step, an ester having a limited acid value is transesterified with a diol having a cyclic acetal skeleton in the presence of a titanium compound to obtain an oligomer. The oligomer is then polymerized in the subsequent polymerization step to increase the molecular weight.

Disclosed is an electrically conductive paste which can be used for the formation of an electrically conductive thin film that has significantly improved adhesion to a substrate having a transparent electrically conductive layer or the like and can impart high reliability and high electrical conductivity to the substrate. The electrically conductive paste comprises: a component (A) which is a binder resin having an acid value of 50 to 500 eq / ton and a glass transition temperature of 60 to 150 DEG C and comprising a polyurethane resin; a component (B) which is a metal powder; and a component (C) which is an organic solvent.

A yellow toner for developing electrostatic images is formed of yellow toner particles containing a binder resin and a yellow colorant. The yellow toner has a storage modulus G'180 at 180 DEG C. and a minimum storage modulus G'min(120-170) in a temperature range of 120-170 DEG C. giving a ratio [G'180 / G'min(120-170)] of 2.0-8.0. The binder resin comprises a polyester resin having a glass transition temperature of 50-65 DEG C. and an acid value of 2.0-25.0 mgKOH / g. The yellow toner is a compound represented by Formula (1) below: Formula (1): The primary particles of the yellow colorant exhibit a length / breadth ratio of at most 1.5. The yellow colorant is dispersed in the toner particles as independent particles (including primary particles and secondary particles) providing a number-average particle size of 0.1-0.7 mu m. The yellow toner is provided with improved fixability and anti-offset property as well as good color toner performances.

The present invention relates to a novel method of using industrial dicyclopentadiene of purity of 75 percent to 85 percent to prepare modified unsaturated polyester resin. In the preparation of the resin, the industrial dicyclopentadiene separated from the saturated or unsaturated dicarbonic acid or acidic anhydride and the distilled part of mixed C5 is used as the raw material. After hydrolysis and addition reaction, the diol or polyol of appropriate amount is added. The polymerization and dehydration reaction is done with the influence of acidic catalyst. When the mixture is condensed to the designated acid value, the inhibitor and cross-linking monomer of appropriate amount are added and then stirred to prepare the product. The present invention has the advantage that the cost of resin is lower than the common type unsaturated resin. At the same time, the air-drying performance, heat resistance, volumetric shrinkage rate and other performances are all superior to the common type unsaturated polyester resin. The product can be widely used in the fields of glass steel, mold, plastic clothing, sealing, and adhesive and so on.

The object of the present invention is to provide a polycarbonate resin composition which has excellent transparency and durability against molding heat, which gives a molded article having an excellent mold release property, reduced strains, improved cracking resistance and, preferably, weatherability, and which is particularly suitable for a transparent member for a vehicle, pellets thereof and a molded article thereof, and the present invention provides a polycarbonate resin composition obtained by blending 100 parts by weight of a polycarbonate resin (Component A) and 0.005 to 2 parts by weight of a full ester (Component B) from an aliphatic polyhydric alcohol having 4 to 8 hydroxyl groups and 5 to 30 carbon atoms and an aliphatic carboxylic acid having 10 to 22 carbon atoms, said Component B having a 5% weight loss temperature, measured by TGA (thermogravimetric analysis), of 250 to 360° C. and having an acid value of 4 to 20, pellets thereof and a molded article thereof.