4560 results about "Autoclave" patented technology

A method for producing a nitride semiconductor, comprising controlling temperature and pressure in a autoclave containing a seed having a hexagonal crystal structure, a nitrogen element-containing solvent, a raw material substance containing a metal element of Group 13 of the Periodic Table, and a mineralizer so as to put said solvent into a supercritical state and/or a subcritical state and thereby ammonothermally grow a nitride semiconductor crystal on the surface of said seed, wherein the crystal growth rate in the m-axis direction on said seed is 1.5 times or more the crystal growth rate in the c-axis direction on said seed. By the method, a nitride semiconductor having a large-diameter C plane or a nitride semiconductor thick in the m-axis direction can be efficiently and simply produced.

A method for large-scale manufacturing of gallium nitride boules. Large-area single crystal seed plates are suspended in a rack, placed in a large diameter autoclave or internally-heated high pressure apparatus along with ammonia and a mineralizer, and grown ammonothermally. The seed orientation and mounting geometry are chosen to provide efficient utilization of the seed plates and of the volume inside the autoclave or high pressure apparatus. The method is scalable up to very large volumes and is cost effective.

The double bag vacuum infusion process of the present invention provides a low cost method for producing complex composite assemblies without an autoclave. It also enables the production of highly innovative structures. The quality of the composites produced using such an infusion process are comparable to composites made using prepregs, hand layup or fiber placement, and autoclave curing. Double bagging provides vacuum integrity, controls bag relaxation while flow media controls the flow front to allow high quality aerospace-grade products.

A method for large-scale manufacturing of gallium nitride includes a process for reducing and/or minimizing contamination in the crystals, for solvent addition to an autoclave, for improving or optimizing the solvent atmosphere composition, for removal of the solvent from the autoclave, and for recycling of the solvent. The method is scalable up to large volumes and is cost effective.

A terminally sterilizable container includes a polypropylene bottle having a body with a manually squeezable sidewall and a thickness preventing water loss. The bottle body includes shoulders for providing autoclave produced pressure distribution and deformation resistance along with an elongated tips outfitted to a neck of the body and having a lumen therethrough with a drop dispensing orifice. A cap enclosed the elongated tip and includes enclosed with a nub for sealing the orifice to prevent autoclave produced pressure leaks.

A composite part is cured out-of-autoclave using an inductively heated, stand-alone tooling. The part in placed on a tool and is covered by a heating blanket. One side of the part is heated by inductive coil circuits in the tool, and the other side of the part is heated by inductive coil circuits in the blanket.

The invention discloses a hydrothermal synthesis method of lithium-ion battery anode material of lithium iron phosphate, relating two kinds of metal phosphate. The steps are as follows: lithium source and phosphorus source are dissolved in water or mixed with water, and added into the reaction autoclave, the quaternary cationic surfactants and the alkylphenols polyoxyethylene ethers nonionic surfactant is also added into the reaction autoclave, the air in the dead volume of the autoclave inside is purged by the inert gas, the autoclave is sealed and heated to 40-50 DEG C with stirring, a feed valve and an exhaust valve are opened, pure ferrous salting liquid is added into the autoclave, and then the autoclave is sealed for the reaction of the material at 140 to 180 DEG C for 30 to 480 minutes; the mixture ratio of the invention is set as follows: the molar ratio of Li, Fe and P is 3.0-3.15:1:1.0-1.15, and then the resultant is filtered, washed, dried and carbon-coated, thus the lithium iron phosphate is obtained. The lithium iron phosphate which is produced by the invention has the advantages that: the electrochemical performance is excellent, the particle size distribution of which the D50 is between 1.5 um to 2 um is even, the phase purity is above 99 percent and the electronic conductivity of the material is improved.

An apparatus and associated method for large-scale manufacturing of gallium nitride. The apparatus comprises a large diameter autoclave or internally-heated high pressure vessel, a seed rack, and a raw material basket. Methods include effective means for utilization of seed crystals. The apparatus and methods are scalable up to very large volumes and are cost effective.

A method for growing III-V nitride films having an N-face or M-plane using an ammonothermal growth technique. The method comprises using an autoclave, heating the autoclave, and introducing ammonia into the autoclave to produce smooth N-face or M-plane Gallium Nitride films and bulk GaN.

The invention discloses a technological method for preparation of sphere-shaped ultrafine metallic powders through hydro-thermal treatment, which relates to a technological method for preparation of sphere-shaped ultrafine nickel powders or ultrafine cobalt powders through the procedures such as precipitation, dispersing agent surface finish, high-pressure hydro-thermal treatment, washing, drying and high-temperature hydrogen reduction and the like, and which belongs to the technical field for preparation of metal powder materials. The technological method adopts water soluble salts with nickel and cobalt, cobalt oxide, sub-carbonate, carbonate or hydroxide as raw materials, which are prepared into water solution after processing, the dispersing agent is added, then nickel ion and cobalt ion in the water solution are precipitated through alkali, carbonate, oxalic acid or ammonium oxalate and the like, the hydro-thermal treatment of water pulp of the precipitate is performed in an autoclave, and products of sphere-shaped ultrafine nickel powders or ultrafine cobalt powders with even graininess and good dispersibility can be obtained through washing, drying and high-temperature hydrogen reduction. The technological method is not only suitable for medium- and small-scale discontinuous-type manufacture, but also used for large-scale continuous manufacture, and the manufacturing cost is low.

The invention provides a method and a device for synchronous measurements on dynamic and static elastic parameters of rocks by using a rock triaxial anti-compression testing device. The method comprises: sealing a test rock sample in a triaxial autoclave filled with hydraulic oil, applying an oil pressure by an axial pressure control system, applying a confining pressure by a confining pressure control system, and applying a pore pressure by a pore pressure control system; acquiring propagation speeds of longitudinal waves and transverse waves in the test rock sample by a computer acquisition and control system, and calculating the dynamic Young modulus and the dynamic Poisson ratio according to the propagation speeds; and acquiring deformation parameters of the test rock sample during a loading process by the computer acquisition and control system, and calculating the static Young modulus and the static Poisson ratio according to the deformation parameters. The method and the device can ensure validity and accuracy of hydrocarbon reservoir rock mechanical parameter measurements in thousands of meters deep underground and under the conditions of complex confining pressure, high temperature, high pore pressure and polyphase fluid.

The invention relates to a method of synthesizing nickel cobalt oxide electrode material using a hydrothermal method and an application thereof. The method comprises dissolving CoCl2.6H2O, NiCl2.6H2O and CO(NH2)2 into an appropriate amount of deionized water, wherein the mole ratio of CoCl2.6H2O to NiCl2.6H2O is 1 : 2; uniformly stirring the mixed solution by using a magnetic stirrer, transferring the solution into an autoclave, heating the solution to 100 DEG C and keeping the temperature constant for 10 hours; cooling the solution to room temperature, filtering, washing and drying reactants, and then annealing the reactants for 2 hours in an air atmosphere of 250 DEG C. The method is simple to operate and environmental-friendly. The prepared nickel cobalt oxide nanowire is a spinel-type cubic phase and porous, has high purity and relatively high specific surface area, and can be used as electrode materials for super capacitors, with specific capacitance thereof being 722 F/g.

A novel approach is offered to produce a sterilizable medical package by laminating either a nonwoven fabric or a perforated film to a paper web. The laminate construction exhibits properties of heat stability, strength, microbial barrier, air/gas permeability and printability. The laminate construction becomes a self-sealing package that can be sterilized by various techniques, e.g. autoclave (heat), ethylene oxide or gamma radiation.

Disclosed are polymer blends composed of from 25 to 75 wt % of ethylene homopolymer produced in a high pressure tubular reactor and from 75 to 25 wt % of ethylene homopolymer produced in a high pressure autoclave reactor, provided that each homopolymer is removed from the reaction zone prior to being blended together. The blends so formed have a good combination of neck-in and adhesion properties. A process for the extrusion coating of a substrate with these new polymer blends is also described.

One embodiment describes a handheld, sterile input device to control one or more devices in the operating room. The embodiment's disposable component contains no electronics while its removable sensing module can be autoclaved and recharged for multiple procedures. Another embodiment describes a fully autoclaveable sterile input device with a detachable control assembly that enables thorough cleaning and disinfecting prior to steam sterilization in an autoclave.

The invention relates to a method for preparing large-scale graphene through supercritical carbon dioxide exfoliation. Supercritical carbon dioxide is adopted as an exfoliant, a surfactant is adopted as a dispersant, graphite powder and the dispersant are put in an autoclave, the carbon dioxide is pumped in the autoclave and circularly flows in a supercritical state, and then the pressure is reduced quickly to be normal pressure; the process is repeated so that the materials undergo pressure increment and pressure reduction several times; and the layers of the graphene is controlled by controlling the times of pressure increment and pressure reduction, so as to prepare the large scale graphene. Compared with the prior art, the invention has the advantages as follows: large-scale (hundreds of micrometers) high-quality graphene can be prepared; the method belongs to physical exfoliation, the treatment conditions are mild, and the quality of the graphene cannot be damaged; besides, the carbon dioxide used in the method is nontoxic, cheap and easy to obtain, and the technology is simple.

A method for preparing uniformly scattered nanocrystal of iron-lithium phosphate by hydrothermal synthesis includes using ferrous salt and phosphoric acid as well as lithium hydroxide as raw materials to obtain reaction pioneer matter under temperature of 40-100deg.c first, then reacting on obtained pioneer matter in high pressure reactor with temperature of 150-200deg.c under hydrothermal condition and processing obtained product by high temperature under protection of inert gas to finally obtain said uniformly scattered nanocrystal with average particle diameter of 0.2-0.5micron.