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131 results about "Metaboric acid" patented technology

Metaboric acid is the name for a family of inorganic compounds formed by the dehydration of boric acid. Metaboric acids are colourless solids with the empirical formula HBO₂. There are two forms of metaboric acid, all are white solids. One form of metaboric acid is molecular, and the other forms are polymers.

Preparation method of hexagonal boron nitride

The invention relates to a preparation method of hexagonal boron nitride. The method comprises the following steps: uniformly mixing a boron source and a nitrogen source to obtain a mixture of the boron source and the nitrogen source, wherein the boron source is boric acid, metaboric acid or boric oxide and the nitrogen source is tripolycyanamide, ammonium chloride, ammonium bromide or urea; under a protective gas atmosphere, heating the mixture to 500-900 DEG C, and insulating for 5-20 hours at 500-900 DEG C; and grinding the insulated mixture to obtain the hexagonal boron nitride. The boron source and the nitrogen source used by the preparation method of hexagonal boron nitride are materials easy to decompose and less in residue, so that metal impure particles by using metal boride are avoided and the subsequent tedious pickling and washing steps are avoided. The method is simple in process, and hexagonal boron nitride after reaction can be used after being grinded. Reaction is not carried out at high temperatures, so that the energy consumption is low and the production is low.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Boric fertilizer water dispersing granule and preparing method thereof

The invention belongs to a new boric fertilizer, referring to a boric fertilizer water dispersing granule and preparing method thereof. The invention comprises one or more than one boric fertilizers and at least one surfactant; the materials are processed as the regular or irregular granules water dispersing granule; the weight part of the boric fertilizer is 5-95 parts; the rest is the assistant. The preferable solution of the invention is following: the boric fertilizer comprises one of the boric acid, boron oxide, boric acid ammonium, sodium tetraborate, calcium borate side, partial sodium borate, sodium borate tetrahydrate, magnesium diboride, sodium perborate, zinc borate, boric acid manganese, high-sodium borate, partial acid potassium, boron and magnesium fertilizer, boron and magnesium phosphate and boron mud or the mixture of the two or more than two of the above. The preparing method of the invention is scaling the prescription, mixing, crushing, and granule and drying to obtain the product. The boric fertilizer water dispersing granule of the invention has a fast disintegration, dissolving (dispersing) completely, not plugging the nozzle and the dropping pipe lines, no heating while using, easy to absorb moisture, packaging, storage and transportation, measurement, the use of low cost, widely used in food crops, cash crops, horticulture, lawns and urban greening; the market prospect is very broad.
Owner:SHENZHEN LANGTAI BIOTECH

Method for synthesizing diisoborneol oxalate

The invention discloses a method for synthesizing diisoborneol oxalate. The diisoborneol oxalate is prepared from such raw materials as industrial camphene, camphene, tricyclene and isoborneol. The method comprises the following steps: dissolving raw materials in a certain amount of an organic solvent, reacting with anhydrous oxalic acid at certain temperature for a certain duration in the presence of such catalysts as boron anhydrous, pyroboric acid or metaboric acid or titanium sulfate, or metatitanic acid, filtering and removing the catalysts and unreacted anhydrous oxalic acid, washing for several times, rotatably evaporating upper liquid to remove most solvents, removing camphene and tricyclene as raw materials which are not reacted completely as well as a few of isoborneol as a byproduct to obtain a crude product, and recrystallizing to obtain diisoborneol oxalate. The method disclosed by the invention can adopt such organic solvents as aromatic hydrocarbon and branched paraffin as reaction mediums in reaction. The method, which adopts conventional heating, is moderate in conditions, simple and convenient to operate, low in side reaction and high in product yield, and raw materials are easily separated from products.
Owner:株洲松本药业有限公司

Extreme-pressure anti-wear lubricating agent

InactiveCN104450143ALow high temperature coefficient of frictionImprove the lubrication effectLubricant compositionCelluloseSodium tetrafluoroborate
The invention provides an extreme-pressure anti-wear lubricating agent, and relates to the technical field of high-temperature lubricating agents. The extreme-pressure anti-wear lubricating agent comprises components in weight ratio as follows: 0.1%-3% of a component A, 8%-35% of a component B, 2%-6% of a component C, 0.5%-5% of a component D, 0.5%-4% of a component E, 0.5%-4% of a component F, 0.8%-4% of a component G, 0.2%-1% of a component H and the balance of water, wherein the component A is one of or a mixture of sodium carboxymethylcellulose and xanthan gum; the component B is one of or a mixture of talc powder and bentonite; the component C adopts sodium silicate; the component D adopts one of or a mixture of two or three of sodium fluoborate, borax decahydrate and calcium metaborate; the component E adopts one of zinc stearate and lithium stearate; the component F adopts one of nano fullerene and alkaline sulfonate; the component G adopts sodium polyacrylate; and the component H adopts a water-based defoaming agent. The high-temperature friction coefficient value is very low, the lubricating property is excellent, and the lubricating requirement of current equipment under the high-temperature and high-load conditions can be well met.
Owner:NANHUA UNIV +1

Manufacture of boron-containing compound using cotton balls hydrothermal method and its comprehensive utilization

The invention provides a boron-containing compound prepared by ulexite hydrothermal method and the synthetic utilization thereof. And the raw material is 80-200 mesh ulexite or probertite powder containing B2O3 >=37.5 wt%, which is prepared into calcium borate product and sodium polyborate solution containing B2O3 >=40wt% and Na2O >=0.5wt%, meeting alkali free glass and boron-containing raw material requirements; synthetically utilizing the sodium polyborate solution, evaporating and concentrating, cooling and crystallizing without adding in sodium- containing alkali or salt, so as to be able to prepare borax product; adding less sulphuric acid into borax mother liquor after crystallization and separation processing to be able to prepare boric acid; adding CaO or Ca(OH)2 into the borax mother liquor or sodium-containing polyborate with borax to be able to prepare purer calcium metaborate and simultaneously sodium metaborate by-product.
Owner:DALIAN UNIV OF TECH

Bathing agent possessing health and medical function and its preparation method

The invention relates to a bathing lotion with the action of medical treatment, which comprises the following ingredients (by weight portion), sodium hydrogen carbonate 2.0-40.0%, sodium carbonate 1.5-6.0%, metasillicio acid 20.0-26.0%, sodium fluoride 0.5-5.0%, metaboric acid 2.5-6.0%, sodium bromide 5.0-8.0%, strontium chloride 2.0-6.0%, sodium chloride 10.0-15.0%, complexing agent 18.0-25.0%, and perfume compound 0.5-1.0%. The lotion has the effect of moistening and whitening skin.
Owner:高明全

Method for preparing special magnesium borate for oriented silicon steel

The invention relates to the field of oriented silicon steel plate manufacture, in particular to a method for preparing special magnesium borate for oriented silicon steel. The method solves the problems of poor adhesion, dispersibility and electromagnetic performance and the like of the conventional boron aid. The method comprises the following steps of: (1) pouring aqueous solution of magnesium bicarbonate and boric acid in a ratio into a reaction kettle; (2) performing sedimentation treatment on the mixed solution; (3) then conveying the sediment into a pyrolysis tank, adding finished magnesium borate crystal seeds and silane coupling agent into the pyrolysis tank, and producing a mixture of nano magnesium carbonate and metaboric acid by using a liquid phase precipitation method; (4) filter-pressing the pyrolysis product to obtain filter cakes; (5) treating the filter cakes in a high-temperature crystal oven to form nano magnesium borate powder with complete crystal; and (6) grading the material discharged out of the high-temperature crystal oven with jet milling to obtain a screened substance of less than or equal to 320 meshes. All indexes of the special magnesium borate are superior to that of the primary product, and in particular, the adhesion, dispersibility and electromagnetic performance are remarkably improved, and the quality of the oriented silicon steel plate is improved; and the method has the advantages of simple production process, lower cost and no three-waste pollution.
Owner:山西银圣科技有限公司

Heat insulation anti-sticking coating for mechanical cast steel machining and preparation method of heat insulation anti-sticking coating

The invention discloses a heat insulation anti-sticking coating for mechanical cast steel machining and a preparation method of the heat insulation anti-sticking coating. The preparation method comprises the steps of weighing magnesia powder, meta-barium borate, water glass, N-methyl-2-pyrrolidinone, activated bentonite, dimethyl formamide, magnesium chloride, xylene, barium chloride, polytetrafluoroethylene, polyimide, ethyl acetate, aluminum paste and paint, feeding magnesia powder, activated bentonite and barium chloride into an edge runner, performing dry mixing, and adding water glass for mixed grinding; feeding polyimide, polytetrafluoroethylene, xylene, ethyl acetate and dimethyl formamide into a reaction kettle for uniform mixing to obtain a mixture, mixing the mixture with the mixed-ground raw materials, adding the rest of the raw materials, grinding the raw materials in a three-roller machine, and adjusting the viscosity. The relative density of a product is 16-18, and the product can be solidified at low temperature; the product can resist high temperature of 1,000-1,200 DEG C, cannot be separated, does not corrode metal equipment, protects steel materials from being oxidized, avoids decarbonization and can be widely produced to continuously replace the conventional material.
Owner:珠海市龙圣模具材料有限公司

Preparation method for specimen used for measuring silicon contents in ferrosilicon by X-ray fluorometric analysis method

The invention relates to a preparation method for a specimen used for measuring silicon contents in ferrosilicon by an X-ray fluorometric analysis method. The preparation method comprises the following steps of primary burdening, pre-oxidation, secondary burdening and fusion. In primary burdening, filter paper and mixed oxidizing agent are used for coating a ferrosilicon specimen, and the specimenis coated into a sphere; in pre-oxidation, a crucible is full of graphite, the spherical specimen is put into a graphite pit, and then, the spherical specimen is oxidized in a high-temperature mufflefurnace to obtain an elliptical specimen; in secondary burdening, ammonium iodide release agent is laid in a platinum vessel, the cooled elliptical specimen is placed and is covered with lithium borate and metaboric acid mixed fusing agent; and in fusion, the platinum vessel is put in a piece fusion machine and is subjected to fusion at the temperature of 900-1050DEG C for 19min to obtain the fused piece, i.e., the specimen, and the specimen can be directly used for an X-ray spectrum analyzer for analysis. By use of the method, various specimens can be simultaneously manufactured, in addition, process controllability is simple, time consumed for experiments is short, manufacture cost is low, and an X-ray fluorometric analysis result is high in accuracy.
Owner:唐山瑞丰钢铁(集团)有限公司

Oil-resistant mildew-resistant modified bituminous paint and preparation method thereof

The invention discloses oil-resistant mildew-resistant modified bituminous paint. The oil-resistant mildew-resistant modified bituminous paint is prepared from 16-21 parts by weight of modified asphalt, 12-14 parts by weight of urea-formaldehyde resin, 0.5-1.0 part by weight of oxalic acid, 0.5-1.0 part by weight of aluminum phosphate, 6-8 parts by weight of modified waste sodium silicate sand, 19-22 parts by weight of terpolycyantoamino-formaldehyde resin, 4-6 parts by weight of methylene bis(cyclohexylammonium), 2-3 parts by weight of disodium sebacate, 2-4 parts by weight of cuprous thiocyanate, 1-3 parts by weight of liquid nitrile rubber, 3-4 parts by weight of nanometer diatomite, 1-2 parts by weight of nanometer calcium carbonate, 1-2 parts by weight of a silane coupling agent KH-560, 0.5-1.0 part by weight of a JWK 200 antistatic agent, 2-3 parts by weight of barium metaborate, 1-2 parts by weight of di-n-octyltin-dithioglycolate, 4-6 parts by weight of coal tar, 7-9 parts by weight of acetone and 10-13 parts by weight of xylene. The oil-resistant mildew-resistant modified bituminous paint utilizes modified asphalt as a main body. The used urea-formaldehyde resin improves paint wear resistance, oil resistance, mildew resistance and insulating properties. The used modified waste sodium silicate sand improves poor asphalt resistance to heat and improves paint resistance to heat, acids and fire. The used cuprous thiocyanate can prevent aquatic organism adhesion and reduce fuel consumption of maritime ships.
Owner:TIANCHANG JULONG TRAVEL PAINT

Vinyl acetate latex paint and preparation method thereof

The invention discloses vinyl acetate latex paint. The vinyl acetate latex paint comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 15-20 parts of anatase type TiO2, 20-25 parts of barium metaborate, 8-10 parts of talcum powder, 10-15 parts of hydroxymethyl cellulose, 5-8 parts of ethylene glycol, 3-5 parts of a surfactant and 100 parts of deionized water; the component B comprises the following components in parts by weight: 100 parts of vinyl acetate emulsion, 3-5 parts of sodium benzoate and 3-5 parts of ester alcohol-12. The vinyl acetate latex paint prepared by the method disclosed by the invention is low in cost, excellent in performance, good in water resistance and capable of being widely used for indoor decoration; the needed color is added into the prepared paint to prepare the paint with color, and the paint with color is very convenient and durable.
Owner:QINGDAO BAIRUIJI BIOTECH
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