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7328results about How to "Good film forming" patented technology

Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant

In an aspect of the invention, a fluoropolymer dispersion, preferably a PTFE dispersion, is provided that comprises fluoropolymer particles having an average particle size of 10 to 400 nm dispersed in water whereby the dispersion has an amount of solids between 35 and 70% by weight. The dispersion is free of fluorinated surfactant having a molecular weight of less than 1000 g / mol (hereinafter called low molecular weight fluorinated surfactant) or contains the low molecular weight fluorinated surfactant in an amount of not more than 0.05% by weight based on the total weight solids of the dispersion. The dispersion further comprises a non-ionic non-fluorinated surfactant or mixture of non-ionic non-fluorinated surfactants and one or more non-fluorinated anionic surfactants. Through the use of a non-fluorinated anionic surfactant, a dispersion is obtained that has a low viscosity at room temperature (20° C.). The dispersion is further free of aromatic group containing non-ionic surfactants and is accordingly environmentally more friendly and can yield coatings that are less susceptible of discoloration. The amount and nature of the non-ionic non-fluorinated surfactant or mixture of non-ionic non-fluorinated surfactants is selected such that the Viscosity Transition Temperature (VTT) (measured as set forth in the examples) of the fluoropolymer dispersion is at least 26, preferably at least 28° C. In a further aspect of the invention, a method is provided to obtain the aforementioned dispersion.
Owner:3M INNOVATIVE PROPERTIES CO

Multifunctional coatings and preparation method thereof

The invention relates to multifunctional paint with the functions of water and fire prevention, lighting, noise reduction, safe escape and decoration and a preparation method thereof. The multifunctional paint comprises a polymer emulsion, a filler, a flame retardant, a long afterglow luminescent material, an addition agent and water, and the paint comprises raw materials in weight percentage: 10 to 50 percent of the polymer emulsion, 5 to 30 percent of the filler, 10 to 30 percent of the flame retardant, 10 to 60 percent of the long afterglow luminescent material, 0.1 to 5 percent of the addition agent and 1 to 50 percent of the water. The multifunctional paint is applied to a highway tunnel, an underground garage, an underground urban traffic passage, a civil defence engineering, an underground fortification, an underground warehouse, an underground production workshop and other underground buildings, can well meet the requirements of waterproof and fireproof functions and has obvious energy-saving effect; and with the characteristic of the long afterglow of the luminescent paint, the multifunctional paint exerts the function of illumination after power failure and is used to guide personnel to safely evacuate the scene of an accident. In addition, the multifunctional paint also has certain functions of noise absorption and noise reduction.
Owner:ANHUI ZHONGYI NEW MATERIAL TECH CO LTD

Polymer composite diaphragm and its preparing method

This invention discloses a polymer compound membrane and its preparation method, in which, the method includes: mixing strengthening bodies of a matrix film and inorganic nm materials in an organic solvent to get a uniform slurry to be coated on both sides of a non-woven cloth to get a polymer compound membrane, in which, said strengthening bodies are selected from the following three: 1, an organic monomer and its related initiator, 2, two or more than two polymers, 3, organic monomers and their related initiators and two or more than two polymers, 4, organic monomers and two or more than two polymers.
Owner:PEKING UNIV

Preparation method of high-solid-content aqueous polyurethane for leather

The invention relates to the field of synthetic leather material polyurethane, in particular to a preparation method of high-solid-content aqueous polyurethane for leather. The method comprises the process steps of: prepolymerization reaction: reacting polyol, a hydrophilic chain extender and isocyanate monomer; monomer modification: adding polyhydroxy monomer to be modified together with polyurethane prepolymer; salt formation by neutralization: adding a neutralizing agent so that an emulsion forms salt ion groups; and chain extension subsequent to emulsification: dissolving an external emulsifying agent and a sulfonic acid chain extender in water to obtain a solution and adding the solution to the system for performing emulsification. In the invention, the emulsification property of theemulsion is improved by using carboxylic acid type and sulfonic acid type chain extenders, so that polyurethane and water are fully emulsified; simultaneously, due to the employment of the method in which self emulsification and external emulsification are combined, not only the stable emulsion can be synthesized, but also the solid content can be increased; in addition, the use of water as the solvent in emulsification is consistent with the requirement of clean production process; and the finally-synthesized emulsion has good film forming performance, high drying speed, no yellowing, excellent mechanical properties and short process flow, is suitable for the synthesis of leather substrates or surface materials, and can take the place of solvent-type products.
Owner:溧阳常大技术转移中心有限公司

2-thiophene-benzotriazole-based polymer materials and photovoltaic application thereof

The invention discloses a series of 2-thiophene-benzotriazole-based polymer materials. In the invention, a 2-thiophene-benzotriazole unit is connected with another aromatic ring, aromatic heterocyclic ring or derivatives thereof by a carbon-carbon single bond or a carbon-carbon double bond to obtain the 2-thiophene-benzotriazole-based polymer materials. The series of 2-thiophene-benzotriazole-based polymer materials are applied to polymer solar cells and have good photoelectric conversion function. The application of the 2-thiophene-benzotriazole-based polymer materials has the following steps of: mixing the 2-thiophene-benzotriazole-based polymer materials with a C60 receptor; spreading on ITO (Indium Tin Oxide) glass to form a layer of semitransparent film; and finally evaporating a metal electrode on the polymers in a vacuum evaporating way to obtain a polymer solar cell device.
Owner:CENT SOUTH UNIV

Preparation method of proteins and protein-based sizes for warp sizing

The invention relates to a preparation method of proteins and protein-based sizes for warp sizing. The method comprises the following steps: (1) taking, putting the protein raw materials, such as plant proteins, animal proteins or animal-protein-based-materials, which are taken as size raw materials, into a sodium hydroxide solution or an alcohol solution, heating the obtained mixture for 30-60 minutes under the constant temperature condition of 20-90 DEG C, adjusting the pH value of the obtained mixture to be 7-8, removing undissolved precipitates through centrifugation or suction filtration, and eventually producing proteins or protein-based sizes; and (2) soaking thick yarns, spun yarns, fabrics or other textile materials into the sizes for 5-10 minutes at 20-90 DEG C, and after fabrics are soaked in the sizes, carrying out constant-speed rolling in the thickness direction of the fabrics. The proteins and the protein-based sizes prepared by using the method disclosed by the invention have good biodegradable properties, and can be directly applied to the sizing of cotton yarns, polyesters, polyester cotton blended yarns and other blended yarns, and the size preparation is low in cost and does not pollute the environment.
Owner:DONGHUA UNIV

Preparation method of graphene-titanium dioxide composite material

The invention discloses a preparation method of a graphene-titanium dioxide composite material, and relates to the graphene-titanium dioxide composite material. The preparation method of the graphene-titanium dioxide composite material is high-efficient and environment-friendly, and comprises following steps: 1) preparing a solution by dissolving a titanium iron-containing precursor into absolute ethyl alcohol, and adding oxidized graphene solution, so that titanium irons are adsorbed by the surface of oxidized grapheme, hydrolyzation is performed, and amorphous titanium hydroxide nano-particles are obtained; precipitating and drying an obtained oxidized graphene-titanium hydroxide composite material so as to obtain a oxidized graphene-amorphous titanium oxide composite material; 2) adding an aqueous solution into a sealed high-pressure hydrothermal reaction vessel, adding the oxidized graphene-amorphous titanium oxide composite material which is obtained in step 1) on the aqueous solution, and performing reduction reaction of oxidized graphene and crystallization reaction of amorphous titanium oxide so as to obtain the graphene-titanium dioxide composite material.
Owner:大正(江苏)微纳科技有限公司

Polymer single-ion electrolyte and preparation method thereof

The invention discloses random copolymerization single-ion polymer electrolyte or block copolymerization single-ion polymer electrolyte which is obtained through copolymerization between a (p-vinyl phenylsulfonyl) (perfluoroalkyl sulfonyl) lithium imide monomer and a methoxyl polyethylene glycol acrylate monomer, and a preparation method of the electrolyte. The polymer single-ion electrolyte prepared by the method disclosed by the invention has the advantages of high room-temperature conductivity, high lithium ion transference number, low glass state temperature and degree of crystallinity, good mechanical strength and film-forming properties, wide electrochemical window, good thermal stability and the like, and has potential application values in the aspects of lithium (ion) batteries, carbon-based super-capacitors, solar batteries and the like.
Owner:武汉市瑞华新能源科技有限公司

Preparation method for high-wave permeability super-hydrophobic moisture-proofing coating for antenna housing material

The invention discloses a preparation method for high-wave permeability and super-hydrophobic moisture-proofing coating for an antenna housing material. The preparation method is characterized by comprising the following steps of: preparing hole-sealing emulsion; preparing super-hydrophobic moisture-proofing emulsion; coating the hole-sealing emulsion on the antenna housing material, surface-drying the film coating under a room temperature, and then curing the film coating under the temperature of 100 DEG C to 140 DEG C; cooling and immersing the film coating to the super-hydrophobic moisture-proofing emulsion; surface-drying the film coating under the room temperature, and curing the film coating under the temperature of 80 DEG C to 160 DEG C to acquire the high-wave permeability and super-hydrophobic moisture-proofing coating for the antenna housing material. Micron-level silicon dioxide and fluorine-containing polymer are used in the method to perform accumulating and hole-sealing;a micron surface structure with certain roughness is provided, and epoxy resin with good viscosity is added to the hole-sealed coating, so that the mechanical property of the hole-sealed coating is improved; a self-growth method is adopted for depositing micron-level fluorine-containing polymer, which is in-situ packaged by organic silicon resin and attached with hydrophobic nanometre silicon dioxide, to the surface of the hole-sealed coating, so that the high-wave permeability and super-hydrophobic moisture-proofing coating of the antenna housing material is prepared.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant

In an aspect of the invention, a fluoropolymer dispersion, preferably a PTFE dispersion, is provided that comprises fluoropolymer particles having an average particle size of 10 to 400 nm dispersed in water whereby the dispersion has an amount of solids between 35 and 70% by weight. The dispersion is free of fluorinated surfactant having a molecular weight of less than 1000 g / mol (hereinafter called low molecular weight fluorinated surfactant) or contains the low molecular weight fluorinated surfactant in an amount of not more than 0.05% by weight based on the total weight solids of the dispersion. The dispersion further comprises a non-ionic non-fluorinated surfactant or mixture of non-ionic non-fluorinated surfactants and one or more non-fluorinated anionic surfactants. Through the use of a non-fluorinated anionic surfactant, a dispersion is obtained that has a low viscosity at room temperature (20° C.). The dispersion is further free of aromatic group containing non-ionic surfactants and is accordingly environmentally more friendly and can yield coatings that are less susceptible of discoloration. The amount and nature of the non-ionic non-fluorinated surfactant or mixture of non-ionic non-fluorinated surfactants is selected such that the Viscosity Transition Temperature (VTT) (measured as set forth in the examples) of the fluoropolymer dispersion is at least 26, preferably at least 28° C. In a further aspect of the invention, a method is provided to obtain the aforementioned dispersion.
Owner:3M INNOVATIVE PROPERTIES CO
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