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266results about How to "Simple preparation equipment" patented technology

Method for preparing length-diameter-ratio nano-silver wire by pH-value regulation solvothermal method

The invention relates to a method for preparing a length-diameter-ratio nano-silver wire by a pH-value regulation solvothermal method. The method comprises the following steps of: preparing the following ethylene glycol solution, namely an ethylene glycol solution A of silver nitrate or silver acetate, an ethylene glycol solution B of polyvinyl pyrrolidone (PVP), an ethylene glycol solution C of water-soluble chloride and concentrated acid D; mixing the components according to a certain amount and fully stirring to form a final mixed solution; moving the final mixed solution into a reaction kettle; placing in an oven for reaction for a certain time; taking the reaction kettle out and cooling to room temperature to obtain mother liquid of the nano-silver wire; adding alcohol into the mother liquid for diluting, and removing supernatant liquor to obtain a precipitate; and repeatedly performing centrifugal separation, and thus obtaining nano-silver wire dispersion liquid uniformly dispersed in the alcohol. The method is simple, high in efficiency and low in cost, and can prepare high-quality nano-silver wires within a wider range of reaction condition; and prepared products are high in length-diameter ratio, good in length uniformity and low in impurity content.
Owner:JIANGSU NANOWELL ADVANCED MATERIALS SCI&TECH

Preparation method of crystal phase controllable titanium dioxide nanometer crystal

A process for preparing the crystal phase controllable TiO2 nanocrystals includes such steps as hydrolyzing the Ti-cotnained compound in the aqueous solution of alcohol to obtain amorphous TiO2 powder, adding inorganic acid, hydrothermal treating, filtering, washing and drying. Its resultant TiO2 nanocrystal has the continuously regulatable ratio of anatase phase to rutile phase.
Owner:FUDAN UNIV

Method for preparing liquid crystal thin film material with controllable reflection bandwidth

The present invention is preparation process of liquid crystal film material with controllable reflecting bandwidth, and relates to preparation of material for light enhancing film and infrared shielding film for LCD. The liquid crystal film material is prepared through mixing nematic liquid crystal monomer capable of being light polymerized in 39.8-98.8 wt%, chiral compound in 1-60 wt% and photoinitiator in 0.2-5 wt% dissolved in solvent, and volatilizing the solvent to separate out cholest liquid crystal mixture; selecting powder of liquid crystal materials in different pitches based on required reflection bandwidth and reflection center and mixing; vacuum heating to cholest phase, pouring into preheated liquid crystal box in planar orientation, and ultraviolet radiating for 1-20 min for cross-linking reaction to prepare the liquid crystal film material. The liquid crystal film material has wide and adjustable reflection bandwidth.
Owner:UNIV OF SCI & TECH BEIJING

High heat-resisting ceramic cooking cook ware suitable for electromagnetic induction furnace

The present invention discloses one kind of high temperature resistant ceramic cooker suitable for use in electromagnetic induction furnace. The high temperature resistant ceramic cooker is produced with the main materials, including lithium-containing mineral material, quartz, kaolin, etc, and through grinding, mixing, forming, drying, glazing and high temperature baking to obtain the ceramic body; coating far infrared radiation layer, electromagnetically inducing eddy flow heating layer and far infrared reflecting layer to the bottom of the ceramic body; and roasting. It has high heat stability, no cracking even in no-water cooking state, high heat utilization rate and long service life. It is especially suitable for cooking in electromagnetic induction furnace.
Owner:JINGDEZHEN CERAMIC INSTITUTE

Thermally dissolving and catalytic method for preparing liquid fuel by lignite as well as catalyst and solvent used therefor

The invention belongs to the technological field of coal chemical processing and discloses a heat dissolving and catalyzing method using brown coal to prepare liquid fuel. The method comprises the following steps: 1) the brown coal is smashed and dried to prepare pulverized coal; 2) the pulverized coal, solvent and catalyst are stirred and mixed well to prepare coal slurry; wherein, the weight percent of the pulverized coal is 30 percent to 40 percent; the weight percent of the solvent is 60 percent to 70 percent; the quantity of the added catalyst is 0.5 percent to 1 percent of the weight of the pulverized coal; 3) the coal slurry is dissolved by heat and catalyzed to prepare heat dissolved and liquefied products; wherein, the temperature is 390 DEG C to 450 DEG C; the pressure is 5.0MPa to 9.0MPa; the reaction time is 30 minutes to 60 minutes; 4) the heat dissolved and liquefied products are separated to form gas-phase, liquid-phase and solid-phase products; 5) the liquid products are extracted and processed to form liquid fuel. The invention also discloses catalyst and solvent used in the method. The operation condition of the method of the invention is mild; the conversion ratio of the organic substances in the brown coal can achieve a higher level; after being processed, the liquid fuel product can be used for preparing engine fuel suiting national standards; and the preparation equipment is simple; the investment is small; the cost is low; and the invention is a coal liquefaction method suiting the national conditions of China.
Owner:ZHAOQING SHUNXIN COAL CHEM TECH

Artificial wood grain floor and its press-paste technique and equipment

This invention relates to a simulate wood card, in addition to a plaster technique and device, characterized in that it based on a hot press, and the lower of the bay has a working bench, and the upper of the bay is connected with a press hydraulic cylinder and a connecting board which can be moved up and down; the work bench can be a transforming bench which can be shifted outside; on the connecting board upon the bay it sets at least one wood sheet steel form with inner heating system and wood grain in the lower surface; the bay also has at least two infrared generators; the method of using the device comprises the following steps: fixing the wood sheet steel form on the top of the hot press, aligning the impregnated wood paper according to the interior wiring of the flooring base material, laying it on the transforming working bench and aligning with the upper wood sheet steel form, plastering with the hot press to get the base material, which has a wood paper with at least one wood pattern, and on the surface of the wood paper it has warp wood grain.
Owner:SENJIA WOOD IND MFG PLANT HANGZHOU +1

Hollow fiber ultrafiltration composite membrane, preparation method and application thereof

InactiveCN101703893AStrong resistance to solute pollutionImprove blood compatibilitySemi-permeable membranesDialysis systemsUltrafiltrationChemistry
The invention relates to a hollow fiber ultrafiltration composite membrane composed of the components in the following weight percent: 15-25% of membrane material, 5-15% of pore-making agent, 55-75% of organic solvent and 5-10% of lithium chloride; the membrane material is a mixture of chitosan and one of polysulfone, polyether sulfone, polyacrylonitrile, polymethyl methacrylate, or cellulose triacetate, wherein the chitosan accounts for 1-5% of the total weight of the raw material, and the average molecular weight of chitosan ranges from 300,000 to 1,000,000; the pore-making agent is one of polyvinylpyrrolidone, polyethyleneglycol, or polyvinyl alcohol, or a mixture thereof; and the organic solvent is one of N-methyl-2-pyrrolidone, dimethyl fomamide, dimethyl acetamide, or dimethyl sulfoxide. The invention has good bioactivity, biocompatibility, anti-coagulation property and other properties.
Owner:江苏朗生生命科技有限公司

Non-ionic self-emulsifying epoxy resin curing agent and preparation method thereof

The invention discloses a non-ionic self-emulsifying epoxy resin curing agent and a preparation method thereof. The method comprises that polyethylene glycol and epoxy resin of low molecular weight are adopted to pre-prepare a water-based chain segment under the function of a catalytic agent, the water-based segment is reacted with a mannich base which is prepared from cardanol, formaldehyde and polymine, and at the same time, organosilicone is added to conduct partial end blocking, compatibility of a system on an inorganic component is increased, and the non-ionic cashew phenol amine epoxy curing agent with the self-emulsifying capacity is obtained. The natural cardanol and the polyethylene glycol in the main raw materials of the curing agent have no adverse effect on environment. The prepared curing agent integrates the advantages of non-ionic emulsion and cashew phenol amine.
Owner:GUANGDONG UNIV OF TECH

Liquid gallium alloy and preparation method thereof

The invention discloses a liquid gallium alloy and a preparation method of the alloy. The liquid gallium alloy comprises the following components in percentage by weight: 60-75% of gallium, 10-25% of indium, 1-11% of tin, and 1-8% of zinc. The preparation method of the liquid gallium alloy comprises the following steps: firstly weighing gallium, indium, tin and zinc according to the mass percent of each component, heating gallium to 29 DEG C to melt, and stopping heating; pouring the liquid gallium into a stainless steel container, and pouring indium, tin and zinc into the stainless steel container too; at normal temperature, using a stainless steel made spoon to mix and stir the metals uniformly until the four raw materials are totally dissolved to be liquid, and finishing the preparation of the liquid gallium alloy. The liquid gallium alloy can be taken as a working medium for power generation of a liquid-metal magnetic fluid generator.
Owner:INST OF ELECTRICAL ENG CHINESE ACAD OF SCI

Catalyst loading CoCr(Mn/Al)FeNi high-entropy alloy nano particles and preparation method and application of catalyst

The invention discloses a catalyst loading CoCr(Mn / Al)FeNi high-entropy alloy nano particles and a preparation method and application of the catalyst. Activated carbon or a mineral material is adoptedas the matrix of the catalyst, the CoCr(Mn / Al)FeNi high-entropy alloy nano particles are loaded on the surface of the matrix, wherein the mass content of the matrix is 90-97% by weight. The CoCr(Mn / Al)FeNi high-entropy alloy nano particles loaded on the carrier are uniformly distributed, the loading capacity is controllable, the catalytic performance is excellent, and a galvanic effect can be achieved by the high-entropy alloy particles and the matrix at a nanometer scale, so that the catalytic degradation performance on azo dye is improved greatly.
Owner:CHINA UNIV OF MINING & TECH

Low expansion superhigh silicon aluminum alloy and method for making same

The low expansion Si-Al alloy has very high Si mass ratio of 61.6-70.8 %. The preparation process includes loading Si into mold cavity and pressing with punch head to form pre-fabricated block; preheating the mold to 500-600 deg.c and heating aluminum material to melt; casting aluminum into the mold; pressing with punch head; maintaining the pressure of the punch head while cooling the mold; demolding; and high temperature annealing of the cast ingot. The Si-Al alloy has high Si content, low density, high compactness, low expansion and other performance. The extrusion casting process to add Si element into Al alloy to form Si-Al alloy with very high Si content uses simple preparing apparatus and has low cost.
Owner:哈尔滨天行健航天新材料有限责任公司

Dry-film lubricant and method of use thereof

The invention provides an environmental friendly dry-film lubricant and a use method thereof, which belongs to the technical field of lubricant preparation. The dry-film lubricant comprises a solid lubricant, a dispersing agent, an anti-wear additive, an antioxidant, a reaction promoter, and a film-coated resin monomer; counted in weight percentage, the components and weight ratio thereof are as follows: 10 to 60 percent of solid lubricant, 0.5 to 5 percent of dispersing agent, 2 to 10 percent of anti-wear additive, 1 to 3 percent of antioxidant, 0 to 0.5 percent of reaction promoter, as well as 35 to 80 percent of film-coated resin monomer; the monomer of acrylic ester type is used to initiate copolymerization in situ to form a solid lubricant film. The dry-film lubricant does not contain organic volatiles, has a gentle preparation condition, and has a usage temperature range from -20 DEG C to 250 DEG C. The environmental friendly dry-film lubricant is suitable for the lubricating anti-wear coating on the parts of heat-sensitive base materials like plastics, alloys, and the like, in particular, and is suitable for the lubricating anti-wear coatings of running-in and high / low temperature sliding parts without oil lubrication and spare parts, as well as of microseism wear parts.
Owner:泰州市嘉鼎新材料有限公司

Drilling fluid for drilling

ActiveCN101974316AImprove pressure bearing capacityOvercome the disadvantage of difficult density controlDrilling compositionFoaming agentWell drilling
The invention discloses a low temperature microbubble drilling fluid for offshore oil drilling. The drilling fluid comprises water, sodium carbonate, sodium hydroxide, a flow type modifier, a foaming agent and a stabilizing agent in a mass part ratio of 100: (0.1-0.3): (0.1-0.2): (0.3-0.4): (0.2-0.3): (0.1-0.4). A perforation fluid also comprises a collapse prevention inhibitor, a clay stabilizer, a temperature stabilizing agent and a bactericide. The low temperature microbubble drilling fluid for offshore oil drilling provided by the invention is the novel drilling fluid. In performance, thelow temperature microbubble drilling fluid for offshore oil drilling has the novel advantages of leakage controlling and leakage stopping and a characteristic of adjustable density besides the characteristics of the common bubble drilling fluid in the prior art.
Owner:CHINA NAT OFFSHORE OIL CORP +1

Method for preparing okra polysaccharide and pectin as well as pill preparation thereof

The invention relates to a method for preparing an okra polysaccharide and pectin as well as a pill preparation thereof, belonging to the technical field of health foods. The method comprises the steps of: in the extraction of the okra polysaccharide and the pectin, drying and grinding young fruits of the okra as raw materials into coarse powders, carrying out percolation extraction, and concentrating a percolation extracting solution with a vacuum film to obtain a concentrated solution; carrying out alcohol precipitation on the concentrated solution to obtain a polysaccharide and pectin precipitate, transferring to a refrigerator for cooling, staying overnight, and then pouring an upper-layer solution to obtain a polysaccharide and pectin extractum object; freeze-drying or spray-drying the extractum object to obtain an okra polysaccharide and pectin dry powder; and mixing the okra polysaccharide and pectin dry powder as the raw material with a mixed substrate according to the ratio of 1:1-1:3 to prepare the pill preparation. The prepared product has the health care efficacy of resisting fatigue, delaying aging, improving digestion, invigorating the stomach, moistening the intestine, protecting the liver, strengthening the kidney, reducing the blood fat, enhancing the human endurance and the immunity of the organism, and the like and has the advantages of high bioavailability, quick oral-taking absorption, high content of functional components, remarkable health care function and convenience eating and carrying.
Owner:ZHEJIANG FORESTRY UNIVERSITY

Preparation method of porous diatomite-based AgO ceramic material

The invention discloses a preparation method of a porous diatomite-based AgO ceramic material, comprising the following steps of: firstly, preparing fine diatomite by raw diatomite, mixing the find diatomite, water, sodium carbonate, polyacrylamide and polyvinyl alcohol to prepare wet powder, extruding and sintering the wet powder to prepare porous ceramic strips, and then preparing the porous ceramic strips into required ceramic particles; soaking the ceramic particles in a silver nitrate solution, adding a potassium persulfate solution and a potassium hydroxide solution into the solution for reaction for 1-4 hours, and filtering out the ceramic particles; and washing and drying the filtered ceramic particles to obtain the porous diatomite-based AgO ceramic material. The porous AgO-carried ceramic material is prepared with method provided by the invention, AgO is an efficient bactericide, and porous ceramic is a filter medium with high cost performance, thereby the prepared novel material can be used for sterilizing and filtering in water, reducing the loss of the AgO, and lowering the water treatment cost. The preparation method has the advantages of simplicity in process and preparation equipment, low preparation cost and no pollutant discharge.
Owner:XIAN UNIV OF TECH

Modified cellulose nanofiber membrane based on layer-by-layer self-assembly of lysozyme and silk protein based as well as preparation and application thereof

The invention discloses a modified cellulose nanofiber membrane based on layer-by-layer self-assembly of lysozyme and silk protein as well as preparation and application thereof and belongs to the technical fields of high polymer materials and biomedical materials. According to the invention, a cellulose acetate nanofiber membrane is prepared by utilizing an electrospinning technique and lysozyme and silk protein which are opposite in charges are alternately assembled on the surface of the cellulose nanofiber membrane by adopting a layer-by-layer assembly technique so as to obtain the modified cellulose nanofiber membrane disclosed by the invention. The membrane disclosed by the invention has the advantages that the preparation equipment is simple, raw materials are low in cost, non-toxic and biodegradable, the whole process is simple to operate and the number of lysozyme / silk protein layers is controllable. Proved by antibacterial tests, cell survival tests, cell fluorescence staining tests, cell adhesion tests and in vitro wound healing tests, the modified cellulose nanofiber membrane disclosed by the invention has good antibacterial performance and cell adhesiveness and is capable of increasing the wound healing efficiency and preventing the wound infection, so that the membrane is a very good wound repairing material and can be used in the wound repairing field.
Owner:HUBEI SAILUO BIOLOGICAL MATERIAL CO LTD

Aluminum alloy surface B4C particle reinforced Al base composite cladding layer and preparation method

The invention discloses an aluminum alloy surface B4C particle reinforced Al base composite cladding layer and a preparation method, overcomes the problem that a traditional technology is difficult to remove compact oxide films quickly grown on surfaces of aluminum and an alloy of the aluminum, solves the problems of difficult powder feeding due to light mass of B4C particles and weak wettability with aluminum alloy molten liquid, and effectively leads the B4C particles in the aluminum alloy surface layer to form an Al base composite cladding layer with excellent metallurgic bonding. In cooperation with the powder-wire composite cladding technical scheme, by using consumable electrode inert gas protective welding-MIG welding, aluminum alloy welding wires are transited to the aluminum alloy wire, the side injection of the B4C particles is assisted to fuse in the Al base cladding layer, that is, the B4C particle reinforced Al base composite cladding layer is prepared on the aluminum alloy surface. The B4C particle reinforced Al base composite cladding layer and an aluminum alloy substrate are excellently bonded, and the B4C particles in the cladding layer and an Al matrix are excellently bonded, and obvious defects such as air holes and cracks are avoided; and the aluminum alloy surface B4C particle reinforced Al base composite cladding layer is higher in wear resistance compared with 45 steel.
Owner:HUBEI UNIV OF AUTOMOTIVE TECH

Noble metal monolithic catalyst for purifying organic waste gas and preparation method thereof

The invention provides a noble metal monolithic catalyst for purifying organic waste gas and a preparation method thereof. The catalyst is a noble metal monolithic catalyst which uses cordierite ceramic pretreated by dilute nitric acid as a carrier and is loaded with zirconium-manganese mixed oxide serving as a first coating layer and a noble metal palladium active ingredient serving as a second coating layer. The method for preparing the catalyst comprises the following steps of: acidifying the carrier by adopting the dilute nitric acid to increase the specific surface area and the surface coarseness of the carrier, soaking and roasting a precursor loaded with zirconium and manganese serving as the first coating layer, and soaking a precursor loaded with noble metal palladium serving as the second coating layer of the main active ingredient. The catalyst has uniformly-loaded active ingredients, high catalytic performance, little using amount and low cost of noble metal, easy popularization, high catalytic combustion removal efficiency of triphenyl, polycyclic aromatic hydrocarbon and other organic waste gas and low ignition temperature and can be widely applied to the purification treatment of industrial organic waste gas.
Owner:SOUTH CHINA UNIV OF TECH

Composite nutritional body beautifying agent

The invention relates to a composite nutritional body beautifying agent which has comprehensive and abundant nutrients, replenishes qi and blood after being eaten for a long time and has the special functions of nourishing and beautifying the body to females. The composite nutritional body beautifying agent is especially suitable for pregnant women, puerperae, ladies with valetudinarianism and all beauty-conscious ladies. The invention combines Chinese wolfberry, Chinese date, pawpaw, yam, radix puerariae, honey, soybean, milk, eggs, fish meal, licorice, ginger and brown sugar into a whole for the first time to realize the nutritional effect of beautifying the body. The invention can be prepared into various preparation forms with convenient eating and has simple process, abundance and easy purchase of raw materials, no any toxic or side reaction, obvious food therapy function of each component and high cognitive strength; and the invention can be used as functional food, medical auxiliary food, health-care food and even medicine for popularization.
Owner:永安康健药业(武汉)有限公司

Near infrared photo-thermal conversion agent for tumor photo-thermal excision treatment

The invention relates to a near infrared photo-thermal conversion agent based on prussian blue and application of the agent in tumor photo-thermal excision treatment. The prussian blue is an ancient dye, and is also a clinical medicine for treating thallium radiation poisoning; the prussian blue has the high absorption capability in a near-infrared area, the absorbed near-infrared light can be converted into heat to excise tumor cells through the converted high heat in a targeted manner, so that the prussian blue can be applied to photo-thermal treatment on tumor. Compared with the conventional photo-thermal treatment agent, the prussian blue has the advantages of high photo-thermal conversion rate, low cost and simple preparation, and most importantly, as the prussian blue has clinical medication experience for years, the biosecurity of the prussian blue in human bodies can be ensured.
Owner:PEKING UNIV

Nano bullet proof tyre and its manufacturing method

InactiveCN1769077ANovel, unique and diverse technical structureIncreased elasticity and comfortNon-inflatable tyresTyresNanometreEnvironmental resistance
The invention relates to a nanometer-bullet-proof tire and relative producing method, which is characterized in that: a layer of micro-porous flexible tire body is arranged inside one layer of high-density polyurethane tire surface, while the tire body contains one or several specially-produced inner tube in variable shapes and integration and one or several thread bands. The invention combines the nanometer technique with the one-step casting flospinning or two-step casting flospinning to produce the tire in sealed type or porous type as well as the tire which has color in night. The invention has variable structures; fresh technique; lower cost; bullet-proof; slide-proof; abrasion-proof; lower inner heat emission and better heat endurance without aerating and explosion.
Owner:FUJIAN ZHANGZHOU TIANTIANLI TIRE

Flexible supercapacitor with nickel sulfide-molybdenum sulfide heterogeneous nano-sheet array structure based on carbon cloth loading and preparation method thereof

The present invention relates to a flexible supercapacitor with with NiS-MoS2 heterogeneous nano-sheet array structure based on carbon cloth loading and a preparation method thereof, belonging to thetechnical field of new energy material and device preparation. The flexible supercapacitor grows high-purity, high-density and high-orientation carbon cloth-loaded NiS-MoS2 heterogeneous nanosheet array by using anode material, carbon cloth coated with activated carbon as cathode material, PVA / KOH gel as diaphragm and electrolyte respectively. The anode has the advantages of high purity, high density, tidy appearance, strict controllable growth condition, simple equipment and process, low cost, high capacitance and good charge-discharge stability. The cathode material has excellent conductivity and large double-layer capacitance. The preparation process of the capacitor is simple, economical and environmentally friendly, and no post-treatment is needed. The supercapacitor provided by the invention has the advantages of light weight, large capacity, good cycle charging and discharging stability, and good flexibility, and can be used for power supply equipment of wearable electronic devices.
Owner:BEIJING UNIV OF POSTS & TELECOMM

Method for manufacturing full-fiber quarter wave plate

The invention discloses a method for manufacturing a full-fiber quarter wave plate. A Sagnac interferometer type full-fiber current transformer comprises modules such as a sensing light path, a transmission fiber from a high-voltage part of 110kV to 550kV to 1,000kV to a control room of a power station, a signal processing electronic circuit, an interface circuit of a merging unit and the like, accords with the standard of IEC 60044-8, and is applicable to the industry of electric transmission and transformation and other situations for measuring high current. A full-fiber current sensor realizes current sensing by changing a phase of circularly polarized light of a (gauge outfit) in a sensitive coil through the current. The method for manufacturing the quarter wave plate, namely a key component for realizing mutual conversion of linearly polarized light and circularly polarized light in the full-fiber current transformer comprises the steps of selecting a wave plate, welding the wave plate, a transmission light path and the sensing light path, and protecting welding spots.
Owner:SHANGHAI XINYUE METER FACTORY

Method for preparing Al-Ti-C grain refiner

The invention relates to a method for preparing an Al-Ti-C grain refiner. The method comprises the following steps of: smelting titanium into an aluminium solution, controlling the temperature within a range from 800 to 1,400 DEG C, preserving the heat, and dispersing nano TiC into a titanium and aluminium melt by adopting nitrogen or argon to obtain the Al-Ti-C grain refiner. By the method, required equipment is simple; the technical flow is short; the preparation efficiency is high; TiC particles can be dispersed; and the method is simple and feasible. The Al-Ti-C grain refiner prepared by the method has a good grain refining effect; 0.2 percent of Al-Ti-C grain refiner is added into pure aluminium, and the heat is preserved for 2 hours, but the refining effect is not obviously decayed; and the Al-Ti-C grain refiner has good industrial application prospect.
Owner:JIANGXI UNIV OF SCI & TECH

Fenofibrate pellet and method for preparing the same

The present invention relates to a new method for making insoluble medicine fenofibrate be prepared into micropills in liquid phase. Said method includes the following steps: making the fenofibrate and macromolecular material be dissolved in solvent to form medicine-macromolecular material solution; then making insoluble material be uniformly mixed and suspended in the medicine-macromolecular material solution, adding poor solvent, using medicine-macromolecular material solution as inner phase and using poor solvent as outer phase to form metastable emulsion; along with the continuous diffusion of good solvent in emulsion drop the medicine and macromolecular material in said emulsion drop can be simultaneously separated out and precipitated on the internal and external surfaces of diffusion agent, under the bridge-forming action of liquid bridge-forming agent and stirring action the spherical granules can be obtained.
Owner:ANHUI PROV INST OF BIOLOGICAL MEDICINE

Manufacturing method and device of non-homogeneous entity

The invention provides a manufacturing method and device of a non-homogeneous entity. The manufacturing method comprises the following steps: 1, firstly slicing and layering a formed entity according to a designed thickness to obtain two-dimensional laminate information of each layer; 2, under the control of an application program, mixing the separation slurry in different material components in a material supply cavity in proportion according to the information requirement by a mixing extruding forming head to obtain a manufacturing slurry; c, under the control of CAD (computer-aided design)software, finishing the manufacturing of the first laminate of the entity by the mixing extruding forming head so that the material components in the two-dimensional laminate continuously changes in gradient along an appointed direction; 4, moving the height of one laminated in the formed entity by the mixing extruding forming head to finish the manufacturing of a second laminate of the entity; 5, repeating above method, performing one layer by one layer until the non-homogeneous entity is obtained. The manufacturing device provided by the invention is suitable for the manufacturing method provided by the invention, comprises a three-dimensional movement control platform, a multi-component material mixing extruding forming head, a gas supply and pressure control device and a control system.
Owner:HEBEI UNIV OF TECH

High efficient three-lamination-layer heterojunction film solar cell and preparation method thereof

The utility model provides a high efficient three-lamination-layer heterojunction film solar cell which comprises three sub cells in stacked series connection. The first sub cell is a bottom cell which is a PN junction structure formed by a P1 layer and an N1 layer, the P1 layer is a CuInSe2 material, and the N1 layer is a CdS material. The second cell is a middle cell, the third cell is a top cell, and both the second cell and the third cell are NIP structures. A transition layer with the 10nm thickness is arranged between the first cell and the second cell. A intrinsic amorphous silicon material is employed, contact interfaces of the transition layer with the first cell and the second cell are subjected to processing of plasma bombardment. A SiOx intermediate layer is plated between the second cell and the third cell. The first cell is plated on a glass substrate with a back electrode molybdenum layer. The top of the third cell is orderly plated with a conductive window layer, an antireflection layer and a gate electrode. According to the high efficient three-lamination-layer heterojunction film solar cell, the photoelectric conversion efficiency is raised, the unit cost is effectively reduced, the structure performance of the cell is stable, and the stability of electrical properties in long-term use can be ensured.
Owner:北京大昱光伏科技有限公司

Method for synthesizing amino functionalized rare earth-doped lanthanum fluoride nano fluorescent marker material

The invention relates to a method for synthesizing an amino functionalized rare earth-doped lanthanum fluoride nano fluorescent marker material, which comprises the steps of: with phosphorylethanolamine as a surface active agent, mixing sodium fluoride, lanthanum nitrate and rare earth nitrate in distilled water, carrying out heat preservation at the temperature of 30-90 DEG C, and stirring for a period of time, washing and drying to obtain the aminated rare earth-doped lanthanum fluoride nanocrystalline with the component of xLn<3+>-(1-x) LaF3, wherein Ln<3+>=Ce<3+>, Yb<3+>, Er<3+>, Tm<3+>, Ho<3+>, Eu<3+>, Gd<3+>, Tb<3+>, Dy<3+>, Sm<3+>, Nd<3+> and Pr<3+>, and x=0-50mol%. The rare earth-doped LaF3 nano fluorescent marker material prepared by the method has the advantages that the size of nanoparticles can be controlled to be about 5nm, water solubility is good and the surface amino can be used to realize the connection with biomolecule. Furthermore, different rare earth ions can be doped into the nanoparticles, so that the specific fluorescence emission can be realized so that the biological connection can be detected sensitively; and the nano fluorescent marker material prepared by the method has the potential in application in the biological marking field.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Method for preparing ultra-hydrophilic zinc oxide/titanium oxide film by using layer-by-layer self-assembling method

The invention relates to a method for preparing an ultra-hydrophilic zinc oxide / titanium oxide film by using a layer-by-layer self-assembling method. The method comprises the following steps that: (1) a substrate is immersed in zinc oxide colloid for 3 to 20 minutes, then is washed or rinsed by deionized water, and is dried, such that a substrate with positive electricity on the surface is obtained; (2) the substrate with positive electricity on the surface is immersed in titanium dioxide colloid for 3 to 20 minutes, then is washed or rinsed by deionized water, and is dried, such that a substrate with negative electricity on the surface is obtained; (3) the step (1) and the step (2) are repeated, and finally the substrate is sintered for 0.5 to 4 hours at a temperature of 400 to 500 DEG C, such that an ultra-hydrophilic zinc oxide / titanium oxide film is obtained. The method has advantages of simple equipment and low cost. The obtained film has good hydrophilic performance, and can be used for the determination of chemical oxygen demand in water quality analysis.
Owner:DONGHUA UNIV
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