25601results about How to "Ease of industrial production" patented technology

The invention discloses a method for preparing ethanol by hydrogenation of acetic ester. The method comprises the following step of: hydrogenating the acetic ester at the reaction temperature of between 180 and 300 DEG C under the reaction pressure of between 1.0 and 5.0 MPa in the presence of a reducing and activating copper-based catalyst to generate the ethanol, wherein the copper-based catalyst takes Cu as an active ingredient, SiO2 as a carrier and at least one of transition metal or / and alkali metal as an aid. The method has high space-time yield, high ethanol selectivity, a simple process and low cost, is environmentally-friendly, and contributes to industrial production.

Disclosed is a titanium carbonitride based metal ceramic material based on a high-entropy alloy binder phase. The binder phase of the titanium carbonitride based metal ceramic material is high-entropy alloy, the hard phase of the titanium carbonitride based metal ceramic material is carbonitride solid solution, the high-entropy alloy binder phase includes at least four of ferrum, cobalt, nickel, chromium, aluminum, vanadium, titanium, copper, zirconium, molybdenum, manganese and rare earth elements, and the molar content ratio of each element ranges from 5% to 35%. In a preparation method, the titanium carbonitride based metal ceramic material based on the high-entropy alloy binder phase comprises raw materials including, in weight percent, 3-30% of the high-entropy alloy binder phase, 0-30% of second carbide powder and the balance carbonitride solid solution powder, the carbonitride solid solution powder includes at least one of Ti (Cx, N1-x), (Ti, M1...) and (Cx, N1-x), the M1 component of the (Ti, M1...) and (Cx, N1-x) includes at least one of W, Mo, Ta, Nb, V, Cr, Zr, Hf, Y and lanthanide, and 0<x<1 in the Ti (Cx, N1-x), (Ti, M1...) and (Cx, N1-x). The preparation method includes the process steps of (1) ball-milling mixing, (2) forming and (3) low-pressure sintering.

A 3D printing modified polylactic acid material comprises, by weight, 70-85 parts of polylactic acid, 1-5 parts of chain extenders, 1-5 parts of cross-linking agents, 0.5-1 part of nucleating agents, 5-10 parts of polymers with low molecular weights, 5-10 parts of flexibilizers, 1-5 parts of fortifiers and 0.3-0.8 part of antioxidants. According to the 3D printing modified polylactic acid material, a low-temperature smashing hybrid reaction technology is utilized, modified processing is carried out on polylactic acid, toughness, impact strength and the heat distortion temperature for the polylactic acid are improved to a large extent, and the polylactic acid can have wider application prospects in 3D printing materials.

The invention discloses a method for extracting cannabidiol from cannabis. The method comprises the following steps: smashing and drying extraction fractions of cannabis to obtain medicine material powder; extracting the medicine material powder with 30% to 100% (V / V) of ethanol to obtain an extracting solution; concentrating the extracting solution to obtain an extract; carrying out water precipitation on the extract, and removing impurities to obtain a water precipitation solution; centrifuging the water precipitation solution and adding 10% to 100% (V / V) of ethanol into an obtained precipitate, and dissolving the precipitate to obtain an alcoholic solution of the precipitate; carrying out column chromatography on the alcoholic solution of the precipitate; eluting an obtained eluant after the concentration column chromatography, and adding ethanol for supersaturated dissolution to obtain a crystal substance; adding the crystal substance into purified water or ethanol for washing to obtain a primary product; blending the primary product with purified water, and drying to obtain the cannabidiol. Only highly safe ethanol is adopted as a solvent, the purity of the cannabidiol in a finished product is improved, and the psychotoxic component of tetrahydrocannabinol is also removed, so that the product safety is improved, and the method is applicable for industrial production.

The present invention discloses lithium iron phosphate material for lithium ion power cell and its preparation process, and dissolves the technological problem of raising the discharge power and safety performance. The lithium iron phosphate material is spherical or spheroid composite particle with one base body of lithium iron phosphate and doping and modifying agent and one coating carbon layer. Its preparation process includes wet ball milling the mixture comprising lithium salt, ferric salt, phosphoric acid, doping and modifying agent and dispersant, spraying to pelletize, heating for pre-treatment, maintaining temperature, cooling, pulverizing and shaping. Compared with available technology, the present invention has the features of high crystallization, single structure, average composite particle size of 5-60 microns, specific surface area of 8.0-15.0 sq m / g, bulk density of 1.4-1.7 g / cu cm, high specific capacity, high safety, etc.

The invention discloses a lithium nickel cobalt manganese positive electrode material. The lithium nickel cobalt manganese positive electrode material comprises a lithium nickel cobalt manganese oxide contained core pure phase layer having a thickness of 5-8mum, a surface coat containing oxides, phosphates or fluorides of coating elements comprising Li, Al, Mg, Ti and Zr and having a thickness of 50-100nm, and a superficial doped transition layer positioned between the core pure phase layer and the surface coat, containing doping elements comprising Al, Mg, Ti and Zr or one of rare earth elements and having a thickness of 1-2mum. The lithium nickel cobalt manganese positive electrode material can inhibit the material dissolving in a cycle process without reducing a specific capacity, and has the characteristics of high capability excellent cycle and rate performances, and excellent thermal stability.

The invention relates to a modified chinlon fiber, a preparation method and application. Even dispersion of graphene particles in a chinlon base material is achieved through a physical method, the process is simple, no dispersing agent is needed, and industrial production is easy. Graphene, especially biomass graphene is introduced into chinlon, so that the modified chinlon fiber has a low-temperature far infrared function, and the far infrared normal emissivity of the modified chinlon fiber is 0.85 or above. The antibacterial property of the modified chinlon fiber is 90% or above, and the mechanical strength and breathability are excellent.

The invention provides a graphene / polysiloxane composite coating material and a preparation method thereof. The method comprises the following steps: modifying the graphene surface with active groups by a chemical modification technique to obtain modified graphene, mixing the modified graphene with a silane compound, a dispersion medium, a non-essential comonomer and a non-essential accelerator, and carrying out hydrolytic condensation or hydrolytic condensation-free radical polymerization to generate a graphene / polysiloxane composite resin in situ; and mixing the resin with a non-essential blend resin, a non-essential curing agent, a non-essential solvent, a non-essential pigment and filler and a non-essential aid, and carrying out physical blending, amino epoxy addition reaction, Michael addition reaction and the like to form a film, thereby obtaining the graphene / polysiloxane composite coating material. The uniformly dispersed graphene lamellae and polysiloxane have strong interface effects, also have the gas / liquid barrier and heat shielding effects, and endow the coating with excellent corrosion resistance, flame retardancy and the like, thereby greatly enhancing the mechanical properties, corrosion resistance, scratch resistance, wear resistance and the like of the coating.

The invention relates to a cobalt-intercalated molybdenum sulfide secondary battery material and a preparation method and an application thereof. A three-dimensional cobalt-intercalated molybdenum sulfide multi-level structure is prepared by adopting a chemical solution method; firstly, a cobalt salt, a molybdenum salt and a sulfur source are dispersed into a solvent to prepare a reaction liquid; and then the prepared reaction liquid is subjected to solvent thermal treatment to obtain the three-dimensional cobalt-uniformly-intercalated molybdenum sulfide multi-level structure which is self-assembled by graphene-like ultra-thin nanosheets, wherein the size of the multi-level structure is about 100nm. The invention also discloses a preparation method for the multi-level structure. The secondary battery material prepared by the method is stable in nanomaterial performance, and long in cycle life when the secondary battery material is used as a negative electrode material of a lithium ion battery and an electrode material of a supercapacitor.

The invention discloses environmentally-friendly acrylic ester coating printing adhesive emulsion and a preparation method. An emulsion polymerization process is adopted. The emulsion comprises the following raw materials in part by weight: 50 to 90 parts of soft monomer, 10 to 20 parts of hard monomer, 2 to 10 parts of functional monomer, 2 to 5 parts of emulsifying agent, 0.2 to 0.5 part of initiator, 0.2 to 0.5 part of pH buffer, 80 to 120 parts of deionized water and a proper amount of pH adjustor, wherein the total amount of the soft monomer, the hard monomer and the functional monomer is 100 parts by weight. The three monomers are cooperatively used as functional monomers for generating carboxyl crosslinking, hydroxy crosslinking, epoxy crosslinking and the like so that the obtained printing adhesive emulsion has excellent water tolerance and mechanical property. The crosslinking monomers and the emulsifying agent do not contain the components such as N-methylol acrylamide, APEO and the like, so the emulsion does not release formaldehyde during baking and using and is suitable for high-grade environmentally-friendly printing adhesive.

The invention discloses a mud resisting and slump retaining type polycarboxylic acids water reducer and a preparation method thereof. The mud resisting and slump retaining type polycarboxylic acids water reducer comprises, by weight, unsaturated polyoxyethylene ether 32.5% to 33.6%, unsaturated carboxylic acid 1.7% to 2.5%, functional monomer 3.25% to 3.36%, cross-linking agent 0.08% to 0.13%, oxidizing agent 0.12% to 0.32%, reducing agent 0.09% to 0.17%, chain transferring agent 0.03% to 0.06%, alkalinity modifier 0.86% to 1.22%, and water 60%. The water reducer in the invention has quite strong adaptability for sandstone with high silt content, good effect on mud resisting, large initial dispersibility, low cost and good slump retaining performance. Moreover, the preparation method in the invention reacts at normal temperature; has short reaction time, low energy consumption, low cost, high security coefficient, and no need to control the temperature in the whole production process; and is simple, without pollution, and suitable for commercial production.

The invention relates to method for preparing taurine, comprising the following steps: (1) reacting epoxy ethane with sodium sulfite under 0.05 to 0.1MPa, with pH value of 6.5 to 7.5 and at temperature between 75 and 85 DEG C to obtain hydroxyethyl sodium sulfonate; (2) carrying out ammonolysis reaction on the hydroxyethyl sodium sulfonate and liquid ammonia under 14 to 21MPa and at temperature between 160 and 280 DEG C to obtain ammonolysis solution containing sodium taurate; (3) introducing the ammonolysis solution into a single flash evaporator for primary flash evaporating at a temperature between 160 and 200 DEG C and under 1.3 to 2.0MPa; introducing the flash evaporated liquid into a secondary flash evaporating and falling film evaporator, using the primary flash vapor as a heating medium to carry out flash evaporating and falling film evaporating on the primary flash evaporated liquid in the secondary flash evaporating and falling film evaporator at a temperature between 110 and 140 DEG C and at 0.1 to 0.6MPa; evaporating and concentrating the flash evaporated liquid subjected to secondary flash evaporating and falling film evaporating with flash vapor and steam as heating media in a multi-effect flash evaporating and falling film evaporator; and (4) neutralizing the sodium taurate by sulphuric acid to obtain the taurine. The method for preparing the taurine has the advantages of short time, high yield and low cost, and is easy for industrialized production. In addition, by primary flash evaporating and secondary flash evaporating processes, almost all the ammonia and 40% to 60% of water in the flash evaporated liquid can be removed, thus having double effects of removing ammonia and condensing.