575 results about "Methyl oleate" patented technology

A pharmaceutical composition contains cyclosporine as the active ingredient. More specifically, the composition is an orally administered pharmaceutical formulation in the form of a spontaneous emulsion comprising cyclosporine, ethanol ethyl oleate and polyoxyethylene glycerol trioleate. A method for preparing an orally administered pharmaceutical composition involves first dissolving cyclosporine in ethanol. Polyoxyethylene glycerol trioleate and an oil component are then added, mixed and diluted in an aqueous media to form a spontaneous emulsion.

The invention provides a pesticide oil suspension agent and a preparation method thereof; the pesticide oil suspension agent contains a pesticide active component, emulsifier, defoamer and a dispersion medium; and the dispersion medium is methyl oleate or the mixture of oil methyl ester and vegetable oil. The method for preparing the pesticide oil suspension agent comprises the following steps that: the dispersion medium and the emulsifier are mixed and emulsified; other components are added in to be mixed into pulp; and the pulp is ground by a grinder to prepare the oil suspension agent. Thepesticide oil suspension agent of the invention has small average grain size and high dispersion stability, has good extendibility and permeability on plant leaves, and improves the medicine effect of the product; and the preparation method of the pesticide oil suspension agent has simple process and low cost, facilitates industrial production, and has wide production application prospect.

The invention discloses a highly-efficient lubricant for a drilling fluid. The highly-efficient lubricant comprises the following components in percentage by weight: 10 to 40 percent of white oil, 30 to 70 percent of fatty acid methyl ester or methyl oleate, 5 to 20 percent of polyester, 2 to 8 percent of organic phosphate, 1 to 6 percent of oilness extreme-pressure additive, 0.5 to 2 percent of emulsifier OP-10 and 0.5 to 2 percent of span-80. The invention also discloses a method and steps for preparing the highly-efficient lubricant for the drilling fluid. The highly-efficient lubricant can enhance the lubricating property of the drilling fluid and increase an extreme pressure value of the drilling fluid, and is suitable for the demand of ordinary drilling and use in a high-difficulty highly deviated directional well and a horizontal well.

The present invention relates to an injectable, pharmaceutical composition comprising a C_1-6 alkyl ester of a C_10-20 fatty acid. In an embodiment, the fatty acid is ethyl oleate, isopropyl oleate, ethyl myristate, or isopropyl myristate. These compositions are useful for the delivery of anti-psychotic drugs.

This invention relates to a Group 8 catalyst compound for the metathesis of

This invention also relates to process to make alphaolefins comprising contacting an olefin, such as ethylene, with a feed oil containing a triacylglyceride (typically a fatty acid ester (such as methyl oleate)) with a Group 8 catalyst compound. The fatty acid ester may be a fatty acid methyl ester derived from biodiesel.

This invention relates to a catalyst compound for the metathesis of olefins represented by the formula:

This invention also relates to process to make alphaolefins comprising contacting an olefin, such as ethylene, with a feed oil containing a triacylglyceride (typically a fatty acid ester (such as methyl oleate)) with the catalyst compound described above. The fatty acid ester may be a fatty acid methyl ester derived from biodiesel.

The invention relates to an icariin microemulsion which takes icariin as active ingredient; the icariin is dissolved in oil and then added with emulsifying agent, assistant emulsifier and water to prepare microemulsion with the micro emulsion grain diameter of 10-100nm, wherein, the oil can be one or more in oleic acid, ethyl oleate, isopropyl myristate or castor oil; the icariin microemulsion has the components with the mass percent: 0.66-6.02% of saturated solution of oil of icariin, 10-50% of emulsifying agent, 10-38% of assistant emulsifier and the balance water, Hank's balanced salt solution (HBSS), PBS buffer solution or normal saline. The icariin microemulsion can be kept clear, transparent, stable and uniform when being placed at room temperature for a year, thus good stability is verified evidently. The experiments of cells and animals prove that the icariin microemulsion can strengthen the icariin to penetrate cell layers, promote the medicine to be ingested and absorbed and enhance the healing effect of the medicine. The invention also discloses a preparation method of the icariin microemulsion.

The invention discloses a preparation method for a polyvinyl alcohol/attapulgite-polyion liquid catalytic esterification composite membrane. The preparation method comprises the following steps: adding an attapulgite clay/polyion liquid composite catalyst (ATP-PILs) immobilized with a high-density acidic site into a polyvinyl alcohol (PVA) solution for alloying to form a membrane casting solution, and stewing for defoaming; then coating a smooth and clean glass plate or a microhole basement membrane with the defoamed membrane casting solution; then performing drying, heating and crosslinking after-treatment to form a per-vaporized compact catalytic esterification membrane with a catalysis function. The PVA dense membrane is filled with attapulgite immobilized with the high-density acidic site, so that the mechanical strength and the thermal and chemical stability of the membrane are improved; furthermore, the surface of the catalysis membrane has the high-density acidic catalysis site, and an efficient integrated membrane reaction-separator is constructed; in the catalytic esterification reaction of oleic acid and methyl alcohol, the oleic acid methyl alcohol conversion rate is up to about 90 percent; after the polyvinyl alcohol/attapulgite-polyion liquid catalytic esterification composite membrane is repeatedly used for 4 times, the oleic acid methyl alcohol conversion rate is reduced by about 5 percent or less.

The present invention relates to preparation process of iodized vegetable oil ethyl ester. Iodized vegetable oil is first produced with vegetable oil and hydrogen iodide gas through addition reaction, and iodized vegetable oil and ethanol then produce ester exchange reaction under the action of alkali catalyst to produce iodized vegetable oil ethyl ester, with the hydrogen iodide gas being produced through reaction of iodine, red phosphorus and water. The present invention has facile cheap materials and high conversion rate of ester exchange reaction, and the product has low viscosity.

The invention discloses a process for synthesizing sucrose polyester, particularly a process for synthesizing sucrose polyester by using a rotating film transesterification flow reactor. The process comprises the following steps: methyl oleate, sucrose powder, potassium stearate and potassium carbonate are added into a mixing kettle, and heated while stirring; the materials enter the rotating film transesterification flow reactor to react; the crude fatty acid sucrose polyester product obtained after the reaction enters a product storage tank, and the reaction product methanol enters a methanol receiver after being cooled by a condenser; and the crude product in the product storage tank is neutralized with acetic acid, washed and dried to obtain the sucrose polyester product. The low-boiling-point substances generated in the process provided by the invention are quickly removed out of the reaction system, thereby being beneficial to the generation of the product, greatly increasing the reaction speed and enhancing the product quality. The process can be used for continuous-feeding production, is beneficial to large-scale production, enhances the production efficiency, has the advantages of high yield and simple process, lowers the production cost and raises the resource utilization ratio.

The invention discloses a method for synthesizing methyl oleate and epoxy methyl oleate in ionic liquid medium, which pertains to the technical field of fine chemical synthesis. The invention adopts N-methylimidazole positive ion or ionic liquid composed of N-methyl-2-ketopyrrolidine positive ion liquid and inorganic anions as the catalyst and the medium for reaction; under normal atmosphere, oleic acid and methanol are catalyzed to react for generating methyl oleate; and the invention also adopts 1-methyl-3-n-butylimidazolium chloride ionic liquid as the reaction medium and [Bmim]W10O23 as the catalyst, and under normal atmosphere, uses the synthesized methyl oleate to carry out epoxidation reaction by being dropped with oxyful of 30 percent, thus generating the epoxy methyl oleate. Compared with the traditional catalyzing method, the invention has the advantages that: 1. the reaction temperature is low, the reaction time is short and the energy consumption is low without pollution; 2. the separation process is easier; and 3. the ionic liquid medium used in the reaction can be reused after being simply processed.

The invention relates to biodiesel prepared by non-edible vegetable oil and a method thereof, which belong to the biodiesel field. By-product milk thistle oil produced during the production process of Silibinin serves as a raw material for preparing the biodiesel. The biodiesel is obtained by transesterification of the milk thistle oil and methyl alcohol under the condition of a catalyst. Gas chromatography-mass spectrometry analysis results show that main components of the biodiesel prepared by the milk thistle oil serving as the raw material are methyl oleate and methyl linoleate. The biodiesel is high in cetane number, excellent in performance and capable of meeting China current biodiesel standard. In addition, the biodiesel is simple in process, mild in reaction condition, low in cost and capable of achieving large-scale production.

Methods are provided for purification of epothilone D and epothilone D analogs from epothilone producing cells such as, for example, Sorangium cellulosum and Myxococcus xanthus (recombinant). Epothilone can be purified from fermentation broth, for example by using resins, chromatography, and crystallization. Epothilone D can be crystallized from a binary solvent system in which water is the forcing solvent.

The invention discloses a method for epoxidating methyl oleate, which comprises the following steps of: adding the methyl oleate into a reactor, adding a catalyst and an organic solvent, heating the mixture to the required reaction temperature of 50 to 70 DEG C, keeping constant the temperature, adding dropwise hydrogen peroxide with the concentration of 30 weight percent according to the mass ratio of the hydrogen peroxide to the methyl oleate of 1-2:1 in a way of ensuring that the dropwise addition of the hydrogen peroxide is finished within 2 to 2.5 hours, and continuing to preserve the heat for 2 to 6 hours after the dropwise addition is finished, wherein the mass ratio of the organic solvent to the methyl oleate is 2.0-5.0:1, and the mass ratio of the catalyst to the methyl oleate is 5-25:1,000; standing the reacted mixed solution in an environment of 5 to 10 DEG C for 3 to 5 hours to slowly separate the catalyst out and filtering the mixed solution to remove the catalyst; and standing and demixing filtrate, and distilling an organic layer under reduced pressure to remove the organic solvent to obtain the product epoxy methyl oleate. The method has the advantages of easy post-treatment, no environmental pollution, and high percent conversion and selectivity.