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362results about How to "Control mechanical properties" patented technology

Method for preparing complexly shaped biomedical porous titanium molybdenum alloy implant body

The invention provides a method for preparing a complexly shaped biomedical porous titanium molybdenum alloy implant body and belongs to the technical field of biomedical porous metallic material preparation. The method comprises the following steps of: taking a mixture of titanium and molybdenum metallic element powder and organic polymer powder as raw materials, and then preparing the biomedical porous titanium molybdenum alloy implant body by adopting the processes, such as three-dimensional modeling, selective laser-firing rapid forming, thermal de-greasing, vacuum sintering, and the like. The processing steps are simple, the period is short, the use ratio of materials is high, the cost is low, any complexly shaped porous titanium alloy implant body can be conveniently manufactured, and the method has efficiency and economic advantages in individual design and rapid manufacturing of the implant body. A titanium molybdenum alloy material prepared by using the method has the advantages that pore space is uniform, adjustment scopes of porosity, aperture ratio and aperture are wide, elasticity modulus and compression strength are in close proximity to natural bone, and the demand on biomechanical compatibility required by a biomedical material is met.
Owner:UNIV OF SCI & TECH BEIJING

High-entropy alloy with dispersion nano-sized precipitate strengthening effect and preparing method thereof

The invention discloses high-entropy alloy with the dispersion nano-sized precipitate strengthening effect and a preparing method thereof. The method comprises the steps of removing oxidized skin of a metal material, and then conducting weighing and burdening accurately according to a ratio; conducing smelting in an electric-arc furnace in an argon shield atmosphere of titanium absorbed oxygen to obtain an initial high-entropy alloy ingot, and conducting cold rolling, wherein rolling reduction is 20-50%; placing the ingot in a heat treatment furnace with a temperature ranging from 900 DEG C to 1000 DEG C for heat preservation for 0.5-2 hours, and conducting quenching; placing the ingot in a heat treatment furnace with a temperature ranging from 700 DEG C to 800 DEG C for heat preservation for 2-18 hours, and conducting quenching. By means of precipitation strength, on the premise that high plasticity is kept, yield strength and tensile strength are improved greatly. The room-temperature tensile strength of (FeCoNiCr)94Ti2Al4 in the final state reaches 1094 MPa, plastic elongation is 35%, work hardening effect is remarkable, comprehensive room-temperature mechanical property is prominent, high-temperature tensile strength can reach 400 MPa at the temperature of 800 DEG C and strain rate of 10<-3>, steady creep rate is smaller than or equal to 10<-8> under the stress of 100 MPa and at the temperature of 750 DEG C, and high-temperature tensile strength and creep mechanical property are excellent.
Owner:UNIV OF SCI & TECH BEIJING

Selective laser melting forming molten bath real-time monitoring device and monitoring method

The invention relates to a selective laser melting forming molten bath real-time monitoring device and a monitoring method, and belongs to the technical field of 3D printing additive manufacturing. The selective laser melting forming molten bath real-time monitoring device and the monitoring method can monitor the molten bath temperature, the shape and the area in the SLM forming process in real time, conduct online assessment on the forming precision and the laser power and feed back the result. According to the adopted technical scheme, a melting forming laser system and a pulsed laser are arranged on the top of a forming cavity, a piece of transparent glass is arranged in the center of the top of the forming cavity, a laser lens tube is arranged above the transparent glass, and the pulsed laser is connected with the laser lens tube through an optical fiber. A lifting frame is arranged in the forming cavity, lifting mechanisms are arranged on the two sides of the lifting frame, and cameras are arranged at the bottom of the lifting frame in the mode of different angles. The melting forming laser system, the pulsed laser, the lifting mechanisms and the cameras are connected with a master control system. The selective laser melting forming molten bath real-time monitoring device and the monitoring method are widely used for real-time monitoring of a selective laser melting forming molten bath.
Owner:山西阳宸中北科技有限公司

High-strength small-bore metal bone trabecula and preparation method of same

The invention provides a high-strength small-bore metal bone trabecula and a preparation method of the same. The high-strength small-bore metal bone trabecula is made through overlapping of a plurality of basic units, wherein the basic unit has seamed edges and is solid, other parts have a hollow polyhedral structure, one face of one basic unit coincides with one face of an adjacent basic unit, and reinforced bars are disposed inside the basic unit. The invention also provides a method to prepare the metal bone trabecula, which comprises the steps: 1. modeling is completed; 2. sectioning is completed; 3. a base plate is pre-heated; 4. powder is pre-heated; 5. areas are selected for melting and scanning; 6. the fourth and the fifth steps are repeated to obtain a 3D printing part; 7. residual powder is removed; and 8. electrochemical corrosion is carried out to obtain the high-strength small-bore metal bone trabecula. The high-strength small-bore metal bone trabecula provided by the invention has compression strength of 60 MPa-90 MPa, and effective aperture of 100 mum-150 mum, wherein the aperture is reduced by over 50% and the compression strength increases by over 20% in comparison with those of a conventional 3D printing porous material. The high-strength small-bore metal bone trabecula provided by the invention is more beneficial for bone in-growth and cell growth.
Owner:西安赛隆增材技术股份有限公司

Girth welding method of duplex stainless steel bimetal composite pipe

InactiveCN101362249ASimple welding processExcellent weld mechanical properties and corrosion resistanceArc welding apparatusWelding/soldering/cutting articlesCarbon steelDouble phase
The invention discloses a method for girth welding for double-phase stainless steel bimetal composite tubes. The method comprises the following steps of: firstly, groove processing: the double-phase stainless steel bimetal composite tube consists of a double-phase stainless steel lining tube and a carbon steel base tube, the welding surface of the base tube is processed into a V-shaped groove at an angle of 45-55 degree, and the lining tube is 2-3 mm longer than the base tube; secondly, caulk welding: the connection ports between the base tube and the lining tube are welded through argon tungsten-arc welding, double-phase stainless steel welding wires are adopted, and the welding current is 65-80 A; thirdly, backing welding: the connection ports of lining tube are welded through argon tungsten-arc welding, double-phase stainless steel welding wires are adopted, and the welding current is 60-90 A; fourthly, base tube welding: the connection ports of the base tube are welded through arc welding, and double-phase stainless steel welding wires are adopted. The procedures and the steps are simple, the used welding material is in a small amount, the welding qualification rate is high, the welding defect can be reduced or avoided, and the production efficiency can be greatly improved.
Owner:XIAN SUNWARD AEROSPACE MATERIAL

Medical degradable and absorbable Mg-Sr system magnesium alloy implant and preparation method thereof

The invention relates to a medical degradable and absorbable Mg-Sr system magnesium alloy implant and a preparation method thereof. The medical implant is made of Mg-Sr system alloy, and the Mg-Sr system alloy comprises the following elements in percentage by weight: 0 to 5 percent of strontium (except for 0 percent), a small amount of trace elements, namely one or more of manganese, zirconium, stannum, rare earth and yttrium and the balance of magnesium, wherein the total content of the trace elements is less than 3 percent. In-vivo and in-vitro experiments prove that the Mg-Sr system magnesium alloy implant does not have toxicity, has high histocompatibility, and is a reliable biological medical implant material.
Owner:浙江海圣医疗器械股份有限公司

Microbolometer and preparation method thereof

The invention relates to a microbolometer, which comprises a microbridge structure, wherein a thermosensitive resistance material and an infrared absorption material layer in the microbridge structure are of a carbon nanometer tube-amorphous silicon composite film, the carbon nano tube-amorphous silicon composite film is formed by compounding an one-dimension carbon nano-tube and a two-dimensional amorphous silicon film, and the microbridge structure is of a three-layer sandwich structure; the most bottom layer is of a amorphous silicon nitride film which is used as a supporting and insulation material of the microbridge; the intermediate layer is of one layer or multiple layers of carbon nano-tube-amorphous composite film, the stress is opposite to the nature of the bottom layer silicon nitride film, and the carbon nano-tube-amorphous composite film is used as the thermosensitive layer and the infrared absorption layer of the microbolometer; and the surface layer is of an amorphous silicon nitride film, the stress of the amorphous silicon nitride film is opposite to the nature of the intermediate carbon nano-tube-amorphous composite film, and the amorphous silicon nitride film is used as a passivation layer of the inforared sensing film and a control layer of the stress. The microbolometer and the preparation method can overcome the weaknesses of the prior art, improves the working performance of the part, reduces the cost of the raw material and are applicable to the industrialized mass production.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Sodium alginate-chitosan double-layer edible membrane as well as preparation method and application thereof

The invention discloses a sodium alginate-chitosan double-layer edible membrane as well as a preparation method and an application thereof. The sodium alginate-chitosan double-layer edible membrane isprepared from a sodium alginate membrane and a chitosan membrane through cross-linking compounding. The sodium alginate-chitosan double-layer edible membrane is prepared from a safe and non-toxic material, wide in raw material source, low in production cost and good in membrane forming property, the eating security of an edible inner packaging membrane is improved, through synergetic promotion ofthe components, the air permeability of the membrane is remarkably degraded, the oxygen permeation rate of the membrane is remarkably reduced, the tension property and the transparency of the membrane are remarkably improved, and the membrane is easy to degrade; due to addition of a natural antibacterial agent, microorganism pollution can be very well prevented; the thickness of the membrane canbe controlled by changing the proportioning of the sodium alginate to the chitosan, and then the mechanical properties, the dissolution degree and the antibacterial agent release speed of the membraneare controlled; and the membrane is simple in preparation step, and by adopting the preservative membrane made from the membrane disclosed by the invention, moisture loss and microorganism pollutionin the transportation, storage and processing process of fruits and vegetables can be reduced.
Owner:HAINAN NORMAL UNIVERSITY

Submerged arc welding method for K-shaped groove of 80mm extra-thick steel plate with excellent plate shape after welding

The invention discloses a submerged arc welding method for a K-shaped groove of an 80mm extra-thick steel plate with an excellent plate shape after welding. The method comprises the following steps of: taking a K-shaped symmetrical groove machined by machinery as the groove type, wherein a truncated edge is not remained at the root, and the assembling clearance of the groove is 2-3mm; performing backing welding on a front root weld pass of a K-shaped groove test plate by adopting a solid gas shield welding wire during backing welding, so that partial weld metal penetrates through the reverse side of the groove after the root weld pass is penetrated, the backing welding is finished, and employing mixed gas protection of argon and carbon dioxide during welding; performing positive submerged arc welding after backing welding is finished, turning over and performing back chipping while welding to 2 / 3 depth of the groove, performing reverse submerged arc welding until the reverse welding line is totally filled, and finishing welding of the residual 1 / 3 depth on the positive side after the welding on the reverse side is completely finished. The method is easy and convenient to operate, the turn-over frequency is reduced, the labor intensity is reduced, the working efficiency is improved, the residual deformation of a soldering block is small, and the welding quality is high.
Owner:NANJING IRON & STEEL CO LTD

Method for preparing conductive composite nanofiber nervous tissue engineering scaffold based on graphene

The invention provides a method for preparing a conductive composite nanofiber nervous tissue engineering scaffold based on graphene. The method includes the following steps: a step 1, dissolving tussur silk fibroin and poly (lactic acid)-poly caprolactone in a solvent with stirring till complete dissolution of the tussur silk fibroin and the poly (lactic acid)-poly caprolactone so as to acquiring a spinning solution; a step 2, performing electrostatic spinning on the spinning solution obtained from the step 1 so as to acquire a nanofiber membrane, performing steam fumigation treatment by using ethyl alcohol, and performing drying so as to acquire tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofibers; and a step 3, dipping the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material obtained from the step 2 in a graphene oxide dispersion liquid, taking out the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material, cleaning the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material, soaking the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material in an ascorbic acid solution, taking out the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material, and cleaning the tussur silk fibroin/ poly (lactic acid)-poly caprolactone composite nanofiber scaffold material so as to acquiring the conductive composite nanofiber nervous tissue engineering scaffold based on the graphene. The method is simple to operate, is excellent in repeatability, and can provide a new thought for nerve defect repairing.
Owner:DONGHUA UNIV

Flexible conductive fiber with sheath-core structure and preparation method thereof

The invention belongs to the technical field of flexible conductive fibers for wearable electronic devices and preparation thereof, specifically relates to a conductive coaxial nanofiber with a sheath-core structure of an aramid fiber or a polyamide fiber coating a reduced graphene oxide and a preparation method thereof, and provides a preparation method of a conductive fiber with a sheath-core structure. The preparation method of the conductive fiber with the sheath-core structure comprises the steps that (1), a core layer spinning solution is prepared; (2) a sheath layer spinning solution isprepared; (3) a coaxial fiber is prepared; and (4), high-temperature thermal reduction is conducted, specifically, the coaxial fiber obtained in the step (3) is subjected to the high-temperature thermal reduction to obtain a conductive coaxial nanofiber, that is, the conductive fiber with the sheath-core structure. According to the preparation method of the conductive fiber with the sheath-core structure, graphene oxide is used as the core layer material, and the high temperature resistant wet spinning polymer is used as the sheath layer material, thus reduction of the core layer graphene oxide through the high temperature thermal reduction can be realized, so that the obtained fiber has flexibility and also has the excellent electrical and mechanical properties.
Owner:SICHUAN UNIV

Biodegradable magnesium alloy blood vessel rack

ActiveCN1887360AImprove the overall functionGrain refinementStentsSurgeryHalf-lifeRenal tubule
The biodegradable magnesium alloy blood vessel rack consists of magnesium in 60-95 wt% and other metals, including RE, for the rest. Metal magnesium as the basic material has excellent tissue compatibility and blood compatibility, and the added other metal, including RE, elements raise and improve the comprehensive performance, especially mechanical strength, plasticity, degradability and biocompatibility. The magnesium alloy blood vessel rack has tensile strength of 200-300 MPa, elastic module of 10-50 GPa, elongation at break of 2-10%and degrading half life of 6-18 weeks. Most of the degraded metal ions are drained through renal tubules while small part being utilized by human body.
Owner:LIAONING YINYI BIOTECH CO LTD

Regenerative implant of cruciate ligament and preparation method and application thereof

ActiveCN107510520AMaintain joint functionPromote degradationLigamentsMusclesCruciate ligamentTibia
The invention relates to a regenerative implant of a cruciate ligament and a preparation method and application thereof. A surgical suture-shaped structure made of a degradable high molecule polymerization material is used as an initial mechanical support structure; a membrane-shaped structure made of a composite electrostatic spinning timbering material is used as a core structure for tissue remodeling and regeneration to be tightly wrapped in a winding mode on the initial mechanical support structure so as to form ligament regeneration elements; the multiple ligament regeneration elements form a ligament regeneration element set which is the regenerative implant of the ligament. The results of a goat animal experiment confirms that the implant is completely degraded within 52 weeks after being implanted to an organism, is induced to form an autogenous ligament tissue in the cavity of a knee joint, and induces the bone tunnel interface of a tibia and a femur to form tendon-bone healing; the maximum pulling force of the regenerated ligament is 20-60% that of a normal ligament tissue within 12 months after the implant is implanted to the organism.
Owner:SHANGHAI P & P BIOTECH

Preparation of acrylic ester mixed polymer urea slow release coating agent

ActiveCN101353283AImprove film forming performanceImprove membrane stabilityFertilizer mixturesWater soluble polymersUrea
The invention discloses a preparation method of a urea slow-release film coating agent of an acrylic ester mixed polymer, which comprises the following steps: the preparation of the acrylic ester mixed polymer, the preparation of water-soluble polymer water solution and the preparation of the slow-release film coating agent of the acrylic ester mixed polymer. The preparation method takes water as a polymerization medium, polymer emulsion prepared by segmentation emulsion polymerization effectively controls water resistance and mechanical properties of slow-release materials, and the polymer emulsion is added with the water-soluble polymer material to improve the film forming capacity of the emulsion and the stability of the film material. The method has the advantages that no organic solvent is adopted during the production process, no waste gas and waste liquid is produced, and the slow-release film coating material obtained has good film forming effect, excellent slow-release function and good water solubility, therefore, the slow-release film coating agent is an ideal environment-friendly film coating material.
Owner:CNOOC FUDAO
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