Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

99results about How to "Solve segregation" patented technology

Technological process for producing super-thick plate

The invention relates to a process for producing an ultra-thick plate and belongs to the field of rolling and producing an ultra-thick steel plate in the metallurgical industry. The invention mainly overcome the defect of producing the ultra-thick steel plate by a traditional model casting manufacturing blank and an electro-slag remelting manufacturing blank. The method comprises the following steps: cutting and fixing lengths of the blanks, mechanically conditioning the blanks (eliminating, leveling and cleaning a single-surface oxide layer of a casting blank with a milling machine, a planer or a shot blast); clamping an assembly (relatively superposing the cleaning surfaces of the two blanks after processing, placing the two blanks oppositely and clamping the blanks); mounting the blanks in a vacuum chamber of an electronic beam welding machine for purpose of vacuuming; sewing the assembly on the electronic beam welding seal edge, heating the assembly in a furnace and rolling the assembly through temperature control; and then producing the ultra-thick steel plate. Compared with the traditional electro-slag remelting production process, the process has the advantages of high production efficiency, reduced electric power consumption, less investment of production devices and low production cost. Compared with the traditional die casting production process, the process solves the problem of segregation and looseness of a large-scale die casting ingot center part; the finished product ratio is high; and the finished product ratio of blank assembly is over 90 %.
Owner:SHANDONG IRON & STEEL CO LTD

Preparation method of high-voltage lithium cobalt oxide cathode material

The invention discloses a preparation method of a high-voltage lithium cobalt oxide cathode material which comprises the steps: (1) mixing cobaltosic oxide containing doped element M, a lithium source, oxide containing doped element M', a grain refiner and a fluxing agent to obtain a primary mixture; (2) sintering and smashing the primary mixture to obtain primary sintered powder; (3) mixing the primary sintered powder with a coating material to obtain a secondary mixture; (4) sintering and smashing the secondary mixture to obtain the lithium cobalt oxide cathode material. According to the preparation method disclosed by the invention, the problem of microscale segregation of distribution of doped elements in the product is solved by two modes of doped element premixing and dry-method mixing; a coulter type mixing technology is utilized to solve the problem of segregation of different matters in material mixing; the grain refiner and the fluxing agent are combined for use to synthesizea material in a mixed morphology; technologies such as dual effects of doped element surface crystallization catalysis and the coating material and the like are utilized; thus, performance of the high-voltage lithium cobalt oxide is obviously improved.
Owner:HUNAN CHANGYUAN LICO CO LTD

Preparation method of small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide

The invention relates to a preparation method of a lithium ion battery positive electrode material precursor, in particular to a preparation method of small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide. The preparation method includes following steps: 1, adding soluble aluminum salt and EDTA disodium into a cobalt salt solution to prepare a cobalt-aluminum mixed salt complexsolution; 2, injecting pure water into a reaction kettle to serve as base liquid, blowing in air, adding a small amount of sodium hydroxide solution to adjust pH, and rising temperature; 3, adding the cobalt-aluminum mixed salt complex solution and the sodium hydroxide solution into the reaction kettle for settling reaction while stirring; 4, sampling every 2h to measure granularity till reaching2-5um after more than 40h of reaction, and filtering and washing a material after the granularity reaches a target value; 5, thermally decomposing aluminum-doped hydroxyl cobalt after being washed sectionally to finally obtain small-particle-size uniform-aluminum-doped spherical tricobalt tetraoxide with uniform distribution of aluminum from inside to outside, tricobalt tetraoxide is compact andadhesion-free spherical particles in morphology, tap density is 2.0-2.7g / cm3, and laser granularity distribution is narrow.
Owner:취저우화여우코발트뉴머터리얼컴퍼니리미티드 +1

Method for preparing copper-lead alloy/steel bimetal laminated composite material

The invention discloses a method for preparing a copper-lead alloy / steel bimetal laminated composite material, which comprises the following steps of: treating a steel plate and preheating to the temperature of between 150 and 200 DEG C in a resistance furnace; coating saturated ZnCl2 solution on the surface of the steel plate and preheating to the temperature of between 200 and 600 DEG C; smelting copper-lead alloy liquid in a medium-frequency induction furnace, namely putting charcoal and electrolytic copper into the medium-frequency induction furnace in turn, adding tin and lead after the electrolytic copper is melted, uniformly mixing and deoxidizing to obtain the copper-lead alloy liquid; and preheating a graphite mold to the temperature of 600 DEG C in a box-type resistance furnace, putting a steel substrate into the graphite mold, casting the copper-lead alloy liquid at the temperature of between 950 and 1,100 DEG C, opening the mold to take the composite material out after the temperature of the alloy is reduced to 300 DEG C, and performing air cooling. The method has the advantages of simple process and low cost; and the composite material has the advantages of high interface bonding strength, good alloy structure, and capability of meeting the operational performance of the copper-lead alloy.
Owner:XIAN UNIV OF TECH

GH4738 nickel base superalloy casting ingot homogenization treatment method

The invention provides a nickel base superalloy casting ingot homogenization treatment method, and relates to a GH4738 superalloy casting ingot homogenization treatment process. In the existing GH4738 casting ingot, a large amount of casting state dendrite structures exist, homogenization can cause a large size of the grain, and other problems exist, such that the subsequent cogging forging forming is not easily achieved. A purpose of the present invention is to solve the problems in the prior art. The homogenization treatment method is carrying out an annealing treatment in an annealing furnace, wherein an annealing treatment temperature is 1160-1200 DEG C, and an annealing time is 20-50 h. With the technical scheme of the present invention, problems of element segregation, existing of a large amount of dendrites, large grain and the like can be effectively solved, and an alloy segregation degree can be improved at a maximum so as to establish a foundation for the subsequent cogging forging forming. The nickel base superalloy casting ingot homogenization treatment method can be used for homogenization treatments of GH4738 nickel base superalloys with different casting ingot sizes.
Owner:BC P INC CHINA NAT PETROLEUM CORP +2

Preparation method of high-elasticity corrosion-resistant and wear-resistant Cu-Ni-Sn alloy

The invention relates to a preparation method of a high-elasticity corrosion-resistant and wear-resistant Cu-Ni-Sn alloy. The preparation method comprises the following steps: vacuum induction melting or covering protection type non vacuum melting of a Cu-Ni-Sn ternary alloy, application of electromagnetic stirring until alloy melt is solidified completely in the subsequent solidification process, and homogenization annealing-water cooling-solid solution-cold deformation-aging treatment of as-cast alloy. Through use of the preparation method of a high-elasticity corrosion-resistant and wear-resistant Cu-Ni-Sn alloy, crystal grains can be refined, dendrite spacing can be reduced, macrosegregation and microsegregation of the series of alloy can be eliminated, aging strengthening effect is excellent, plastic processing property of the series of alloy can be improved, the service life of the alloy can be improved, by the application of electromagnetic stirring in the solidification process, the segregation degree of the obtained as-cast structure is small, the segregation is easy to remove, and the method has the advantages of saving energy, improving production efficiency and reducing production cost.
Owner:JIANGYIN SANLING METAL PROD

Preparation method of ultra-coarse tungsten carbide powder

InactiveCN102249234AHigh combined carbon contentTotal Carbon UniformTungsten/molybdenum carbideTube furnaceCarbonization
The invention discloses a preparation method of ultra-coarse tungsten carbide powder. The preparation method comprises the following steps: evenly mixing LiOH solution or Na<2>CO<3>solution with tungsten trioxide in an atomized doping mode; adding the mixed raw material to a four-tube reduction furnace for slow-push reduction, and sieving with a 80-mesh sieve to obtain ultra-coarse tungsten powder with Fisher particle size of 30-40mum; crushing conventional carbon black to obtain fine carbon powder, mixing the fine carbon powder with the tungsten powder in a mixer for 50-70 minutes, and carrying out ball-milling on the mixed powder in a ball mill for 50-70 minutes by utilizing 60kg of a stainless steel ball to obtain evenly mixed W+C powder; adding the evenly mixed W+C powder to a high-temperature carbon tube furnace for high-temperature carbonization to obtain block tungsten carbide; and ball-milling and crushing the obtained block tungsten carbide, and then sieving with a 120 mesh sieve to finally obtain ultra-coarse tungsten carbide particles with particle size of 30-40mum. The ultra-coarse tungsten carbide powder obtained by the method has the advantages of high combined carbon content, good total carbon uniformity, high supply-state and grinding-state Fisher particle size and high primary qualification rate.
Owner:GUANGDONG XIANGLU TUNGSTEN

Neodymium, praseodymium, dysprosium and yttrium multi-element rare earth alloy permanent magnet material and preparation method

The formula of a neodymium, praseodymium, dysprosium and yttrium multi-element rare earth alloy permanent magnet material is Re alpha Re' beta Re'' eta B delta Cu zeta Al epsilon Fe gamma. The neodymium, praseodymium, dysprosium and yttrium multi-element rare earth alloy permanent magnet material is characterized in that Re represents Nd and Pr, Re' represents Dy, Re'' represents Y, Fe represents Fe and inevitable impurities, alpha, beta, eta, delta, zeta, epsilon and gamma represent mass percent contents of the elements respectively, the sum of alpha, beta and eta is larger than or equal to 30 and smaller than or equal to 32, the sum of beta and eta is larger than or equal to 5 and smaller than or equal to 12, eta is larger than or equal to 3 and smaller than or equal to 7, delta is larger than or equal to 1.02 and smaller than or equal to 1.09, zeta is larger than or equal to 0 and smaller than or equal to 0.24, epsilon is larger than or equal to 0.33 and smaller than or equal to 0.67, and 100 minus alpha, beta, delta, zeta and epsilon equals to gamma. According to the neodymium, praseodymium, dysprosium and yttrium multi-element rare earth alloy permanent magnet material, the problem that segregation happens to alloy ingots obtained through melting due to element melting point difference and manual operation factors in the traditional melting process is effectively solved, actual coercive force of the alloy ingots is easily improved due to addition of Dy, Y can partly replace Nd and Pr, and production cost is reduced for enterprises; in addition, alpha-Fe influencing performance of the permanent magnetic material can be effectively avoided, and performance of the alloy ingot material is improved.
Owner:GANZHOU JIATON ADVANCED MATERIALS

Anisotropically bonded magnet and fabricating method, magnetic path thereof

This invention relates to a fabricating method for anisotropically bonded magnet including: step S1 for adjusting the first mixture and the second mixture, where: the first mixture comprises the first magnetic powder, of which the grain size is in the range of 20-150mum, thermosetting resin of 2.0 wt%being added into the anisotropically bonded magnet, the first additive; the second mixture comprises the second magnetic powder, of which the grain size is in the range of 1-20mum, the second additive; step S2 for adjusting the first mixture and the second mixture; step S3 for making the magnetic intensity of the end part of the shaping metal die be under the 0.8T, the magnetic intensity of the central part of the shaping metal die is 5% higher than that of the said end part of the shaping metal die after said mixed compounds being filled into the metal die; step S4 for heating said mixed compounds at the atmosphere of inert gases or nitrogen gases so as to harden compounds.
Owner:SEIKO INSTR INC

Preparation method and mold for microdefect high-utilization rate high-quality static ingot

The invention relates to the field of static ingot preparation, in particular to a preparation method and a mold for a microdefect high-utilization rate high-quality static ingot. The invention is applied to preparing carbon steel, alloy steel and nonferrous metals under vacuum and non-vacuum conditions and has an effect of inhibiting defects, such as shrinkage cavity and porosity, segregation and deposit cone in ingots of various materials. Through adopting a big end down mold design, microzone triggered nucleation is performed by adopting a vibration device to refine grains; a dead head is heated by adopting plasma submerged arc heating; the ingot is demolded by adopting the high-temperature demolding process; thermal insulation is performed on a demolded ingot by adopting a thermal insulation material, and therefore, the thermal stress of the center of the ingot is reduced, and the shrinkage cavity and porosity defect in the ingot is eliminated by adopting an ingot self-feeding mechanism. According to the preparation method and the mold for the microdefect high-utilization rate high-quality static ingot, the problem of the shrinkage cavity and porosity defect in the ingot is effectively solved, the dimension of the dead head is reduced, and the utilization rate and the production efficiency of the ingot are greatly improved.
Owner:中科西王特钢有限公司

Technique method for improving density of injection molding high-speed steel columnar deposition blank

The invention relates to a technique method used for raising the density of a steel-column shaped sediment blank of a spray-forming high-speed tool and belongs to the technical field of material processing. The invention thoroughly combines the theory idea and the technical advantage of spray-forming and heat-control concretion. In an early phase of the spray sediment process, the advantages of the spray-forming that an equiaxed grain (less than 20Mum) having no segregation but a uniform and thin structure can be manufactured in a short process can be performed, and then the manufactured high-speed steel sediment blank has high strength, better plasticity and easy-forging capability. In a later phase of the sediment process, i.e. after the spray-forming is finished, the structure of a main body of equipment (such as a tundish and an atomizing sprayer, etc.) is adopted to control output and radiation of the heat. The invention enhances solidification of easy-loosening part of the high-speed steel sediment blank, so as to manufacture high quality and high density sediment blank. The technique not only can solve the segregation of the high-speed steel but also further enhance the density of the sediment blank to guarantee a following smooth process of fine-forging, etc.
Owner:BEIJING AVIATION MATERIAL INST NO 1 GRP CORP CHINA AVIATION IND

High modulus, ultrahigh strength TiB2 particle reinforced Al-Zn-Mg-CU composite material and preparation method thereof

InactiveCN106834833AThe particle distribution area is wide and uniformSolve segregationMaterial DesignSynthesis methods
The invention discloses a high modulus, ultrahigh strength TiB2 particle reinforced Al-Zn-Mg-CU composite material and a preparation method thereof and belongs to the field of composite materials. TiB2 with a high zinc Al-Zn-Mg-CU-Zr alloy serving as a matrix, the mass fraction being 6.0%-10.0% and the average size being smaller than 1 [mu]m serves as a reinforcement particle; an Al-TiB2 intermediate alloy is prepared through a melt self-propagating direct synthesis method, dosing and melting are conducted according to composite material design compositions, the Al-TiB2 intermediate alloy serves as a matrix, pure aluminum ingots, pure zinc ingots, pure magnesium ingots and an Al-Cu and Al-Zr intermediate alloy are added, stirring and standing are conducted, and then casting is conducted; after homogenization treatment at the temperature of 420-470 DEG C for 25-45 h, casting ingots are squeezed at the temperature of 330-430 DEG C with the squeezing ratio being (15-20):1; and a squeezed material is subjected to T6 artificial aging treatment, the strength of the matrix alloy is significantly improved, and compared with the matrix alloy, the elastic modulus of the composite material is improved by 45%.
Owner:BEIJING UNIV OF TECH

Preparation method for power NCM523 material capable of improving high-and-low-temperature performance

The invention relates to a preparation method for a power NCM523 material capable of improving high-and-low-temperature performance, and belongs to the technical field of a positive electrode material of a lithium ion battery. The preparation method comprises the following steps of 1, preparation of an NCM523 precursor, including the sub steps of 1) solution preparation: preparing a mixed solution of Ni, Co, Mn and Y salt; preparing an NaOH alkali solution, adding Al(NO<3>)<3>.9H<2>O, and adding ammonium hydroxide to form an aluminum-containing ammonia alkali solution; 2) parallel flow reaction: performing a parallel flow reaction on the Ni, Co, Mn and Y salt solution and the aluminum-containing ammonia alkali solution in a reaction kettle to form a sky blue turbid liquid; 3) aging: regulating the ph value of the solution to perform aging and crystal type transformation; 4) performing pressing and filtering, washing and drying; and 5) performing demagnetizing; 2, lithium preparing and sintering: enabling a lithium salt to be mixed with a precursor material, and performing sintering and smashing on the mixture to obtain the positive electrode material; and 3, performing liquid phase coating of a lithium rapid ion conductor: enabling Li<3>PO<4>-Al(OH)<3> to be mixed with the positive electrode material, and performing spraying and drying, and sintering. The preparation method has the advantages of simple process, convenient operation, and capability of remarkably improving the high-and-low-temperature performance, and the like.
Owner:CHINA ELECTRONIC TECH GRP CORP NO 18 RES INST

Homogenization treatment process for high-temperature alloyed steel ingot

InactiveCN101311277ASolve segregationImprove the degree of segregationHeat treatment process controlIngotSuperalloy
A homogenizing treatment method for high-temperature alloy ingots is annealing treatment in an annealing furnace. The method is characterized in that the temperature of the annealing treatment is between the temperature of 1180 to 1230 DEG C and the annealing lasts for twenty hours. The method of the invention adopts the technical proposal, so the method can effectively solve the problem of segregation between the phase Laves and the phase delta and improves the alloy segregation degree to the utmost extent.
Owner:JIANGSU TOLAND ALLOY

Method for producing pre-reducing composite sinter

The invention relates to a production method of pre-reductional composite sinter. The method mixes two kinds of charging high alkalinity sinter and acid pellet together and adds coal dust to the material for acid pellet. Then the uniform mixture of high alkalinity sinter and acid pellet is sintered in sintering machine to produce charging for pre-reduction blast furnace. The produced charging of the invention has higher grade and concise blast furnace operation.
Owner:ANGANG STEEL CO LTD

Secondary-cooling reduction convex foot roll structure for bloom and reduction technology

The invention discloses a secondary-cooling reduction convex foot roll structure for bloom and a reduction technology, and particularly relates to a secondary-cooling reduction convex foot roll structure for bloom and a reduction technology in the technical field of iron and steel metallurgy. The secondary-cooling reduction convex foot roll structure for the bloom comprises reduction-area upper foot rolls and reduction-area lower foot rolls, the reduction-area lower foot rolls are located under the reduction-area upper foot rolls, a boss is arranged in the middle of each reduction-area upper foot roll, a boss is arranged in the middle of each reduction-area lower foot roll, and the bosses of the reduction-area lower foot rolls are longer than the bosses of the reduction-area upper foot rolls. According to the secondary-cooling reduction-area reduction technology for the bloom, multiple groups of reduction-area upper foot rolls and reduction-area lower foot rolls are arranged, and the reduction quantity of the reduction-area upper foot rolls is gradually increased in the blank drawing direction. Therefore, the center segregation and center porosity problems of a continuous casting blank of the bloom can be effectively solved.
Owner:PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP

Steel with high low temperature fracture toughness and used for ocean engineering and manufacturing method thereof

ActiveCN108728743ASolve segregationImprove low temperature fracture toughnessReduction rateUltimate tensile strength
The invention discloses steel with high low temperature fracture toughness and used for ocean engineering and a manufacturing method thereof. The steel comprises the following components: 0.05%-0.10%of C, 0.2%-0.5% of Si, 1.0%-1.5% of Mn, 0.20%-0.50% of Cu, 1.00%-1.50% of Cr, 1.6%-1.8% of Ni, equal to or less than 0.01% of P, equal to or less than 0.01% of S, 0.01%-0.05% of Als, 0.02%-0.04% of Nb, 0.01%-0.02% of Ti, 0.05%-0.07% of V and the balance of Fe and unavoidable impurities. Rolling is controlled by adopting two phases, at the first phase, the rolling temperature is 950-1050 DEG C, andthe single-pass reduction rate is equal to or greater than 15%; at the second phase, the rolling temperature is 840-880 DEG C, and the single-pass reduction rate is greater than 10%; the average cooling rate is greater than 3 DEG C / s, and the self-tempering temperature is 500-600 DEG C; thermal treatment adopts twice quenching and tempering; the yield strength of a steel plate is equal to or greater than 620 MPa, the thickness of the steel plate is 60-100 mm, and the low temperature fracture toughness is high.
Owner:ANGANG STEEL CO LTD

Valve retainer

The invention discloses a valve retainer, which is made of a powdered metal material that comprises the following components in percentage by weight: 0.8 to 1.3 percent of C, 2.0 to 4.0 percent of Cr, 1.0 to 3.0 percent of Mo, 3.0 to 6.5 percent of Co, 0.5 to 2.0 percent of Ni, 0.8 to 1.5 percent of Mns, 0.05 to 0.1 percent of P, 0.2 to 0.5 percent of V, less than or equal to 3 percent of other elements and the balance of Fe. A prevention segregation agent is added into the powdered metal material which can make valve retainer. The valve retainer disclosed by the invention can resist high temperature and wear, and resist the high temperature of over 800 DEG C. In a bench test of more than 300 hours, the valve retainer does not generate segregation, which is favorable for cutting and ensuring the size precision and surface roughness of a cut face.
Owner:CHANGSHU SHUANGYUE MACHINERY

Laser selective melting forming method of copper-chromium alloy part

The invention discloses a laser selective melting forming method of a copper-chromium alloy part. The laser selective melting forming method specifically comprises the following steps of preprocessingCu-Cr alloy powder, preparing a program file and a SLM device, finally melting the selective laser to form a copper-chromium alloy part. The laser selective melting technology can directly form complex parts, shorten the production period and improve the forming efficiency, and the method has a great production application value; in addition, the cooling rate can reach 106 orders of magnitude, asmaller molten pool range and a molten pool can be rapidly cooled, and the liquid phase layering phenomenon in the traditional process is overcome.
Owner:XIAN BRIGHT ADDTIVE TECH CO LTD

Preparation method of high-elasticity, corrosion-resistant and wear-resistant Cu-Ni-Sn alloy

InactiveCN110629070AGuaranteed AM DecompositionReduce segregationWear resistantSolid solution
The invention relates to a preparation method of high-elasticity, corrosion-resistant and wear-resistant Cu-Ni-Sn alloy. The Cu-Ni-Sn multi-element alloy is obtained through vacuum induction melting or covering protection type non-vacuum smelting. In the casting forming process, electromagnetic stirring is applied until alloy liquid is complete solidified, and then the as-cast alloy is subjected to homogenization annealing, hot rolling and cogging, solid solution treatment, cold deformation, spinodal decomposition and other processes. The preparation method of the Cu-Ni-Sn alloy is capable ofrefining crystalline grains, reducing dendritic spacing and eliminating alloy microscopic and macroscopic structure and component segregation, provides implementation conditions for follow-up alloy plastic processing, spinodal decomposition and other processes, and has the beneficial effects that energy is saved, the production efficiency is improved, the service life of the alloy is prolonged, and the production cost is reduced.
Owner:JIANGYIN SANLING METAL PROD

Plastic processing method for powder metallurgy high-speed steel

The invention relates to a plastic processing method for powder metallurgy high-speed steel. The plastic processing method comprises the following steps of: firstly compression-molding water-atomized high-speed steel powder by adopting a pressure of 800-1000MPa; putting a cold-pressed blank in a vacuum sintering furnace, and sintering the cold-pressed blank in vacuum, wherein the vacuum degree is10<-3> Pa, and the sintering temperature is 1100 DEG C to 1300 DEG C; insulating the heat for 2 hours; cooling the cold-pressed blank to room temperature together with the furnace; heating the sintered blank to 900-1100 DEG C; insulating the heat for 30 minutes; preheating an extruding die to 400 DEG C; putting the blank into the extruding die; and extruding the blank under the conditions that the extruding ratio is 8-27 and the speed of a punch of the extruding die is 20-30 mm.S<-1>. Products produced in the invention can obtain tiny and uniform microscopic structures, and carbide and nonmetallic impurities are distributed in a dispersive manner in the sintering process. Extruded materials have higher hardness and bending resistance, and the hardness of the extruded materials can reach more than 66.8HRC without any heat treatment.
Owner:HARBIN INST OF TECH AT WEIHAI

Cement admixture used for building ready-mixed dry mixed mortar and application method thereof

The invention discloses a cement admixture used for building ready-mixed dry mixed mortar and an application method thereof. The cement admixture comprises the following components: 45-98% of cement, 0-40% of mineral admixture, 0-15% of lime or gypsum and 0.1-5% of additive. 10-50% of cement mixture and 50-90% of sand are mixed, water with 10-20% weight of solid matter is added, stirring to be uniform is carried out, and the cement admixture is used for building construction. Dry ready-mixed mortar is divided into two parts, one part is the cement admixture, and the other part is baked sand. The two parts are separately stored and transported, quantitative cement is added in the scene, and mixing is carried out to obtain the mortar for building. Equipment investment and floor area of a ready-mixed mortar factory are greatly reduced, even the cement admixture is produced by a cement factory without requiring the read-mixed mortar factory, and social investment can be greatly saved.
Owner:盛富春

Preparation method for TiAl-Ni alloy plate with high strength and toughness and high stability

ActiveCN110643853AEasy to handleImprove thermal deformation abilityMetal rolling arrangementsIngotUltimate tensile strength
The invention relates to the field of preparation of alloy materials, in particular to a preparation method for a TiAl-Ni alloy plate with high strength and toughness and high stability. The preparation method aims to solve the problems of uneven structure and poor mechanical properties caused by excessive grain growth and process heredity of a TiAl alloy plate material prepared through existing ingot metallurgy and powder metallurgy methods, especially the problems of low strength and plasticity. The preparation method comprises the following steps of 1, weighing raw materials; 2, smelting acast ingot; 3, carrying out primary pretreatment on a blank; 4, carrying out secondary pretreatment on the blank; 5, carrying out jacketing and hot rolling; 6, carrying out stabilizing treatment; and7, removing a jacket so as to obtain the TiAl alloy plate. The plate obtained through the preparation method has the advantages of being good in surface quality, fine and uniform in structure, good inmechanical property and high in repeatability.
Owner:TAIYUAN UNIV OF TECH

Nickel-molybdenum intermediate alloy preparation method for smelting TA10 cast ingot

The invention provides a nickel-molybdenum intermediate alloy preparation method for smelting a TA10 cast ingot. The nickel-molybdenum intermediate alloy preparation method comprises the following steps: respectively turning a pure nickel rod and a molybdenum rod into scrap materials, and heating and drying the scrap materials; adding dried master batch nickel scraps into a crucible of a medium-frequency induction furnace; meanwhile, adding molybdenum scraps into a secondary charging hopper in the medium-frequency induction furnace; vacuumizing the medium-frequency induction furnace to 0.6Pa-0.1Pa and starting to heat and smelt; raising the temperature to 1800-1900 DEG C and keeping the heat for 15-20 minutes; observing that when the smelting rate of the master batch nickel scraps is more than 45%, starting to add the molybdenum scraps; inflating argon to carry out gas protection; continually raising the temperature to guarantee that the temperature reaches 1900 DEG C and keeping the temperature for 20-30 minutes to sufficiently float impurities in smelting liquid up to the surface of a smelting tank; and finally, pouring the smelting liquid into a fixed die and cooling to the room temperature to obtain the product. According to the nickel-molybdenum intermediate alloy preparation method, pure nickel and pure molybdenum are directly prepared into an intermediate alloy; the smelting point of the nickel-molybdenum alloy is reduced and various disadvantages of a traditional manner of adding the intermediate alloy in the process of smelting the TA10 cast ingot are made up.
Owner:CHEN YAN BAOJI METAL MATERIALS

Aluminum tin 40 copper-steel metal bearing material and production method thereof

The invention discloses an aluminum tin 40 copper-steel metal bearing material and a production method thereof. The production method comprises that (1) aluminum tin 40 copper alloy ingots of which two surfaces are roughened and a pure aluminum layer are subjected to the dual-surface composite rolling, the cold rolling is conducted sequentially till the target thickness is reached, the aluminum tin 40 copper alloy ingots are obtained through horizontal continuous casting, the processing rate of the dual-surface composite rolling is more than 50% and the processing rate per cold rolling is in a range from 20% to 35%; and (2) steel plates of which two surfaces are roughened and the aluminum tin 40 copper alloy after being burnished in the (1) are subjected to the composite rolling and the annealing is conducted for 8-10 hours at the temperature of 280 DEG C+ / -10 DEG C. The material has good seizure resistance, adaptability and high-temperature properties and is suitable to diesel engine bearing of medium and low speed ships.
Owner:SHANGHAI HEWEI IND

Ultra-high-strength and ultra-fine-grain TiB2 reinforced Al-Zn-Mg-Cu composite material and preparation method thereof

InactiveCN111500908AEvenly dispersedEnhanced particle sizeMass fractionZr alloy
The invention discloses an ultra-high-strength and ultra-fine-grain TiB2 reinforced Al-Zn-Mg-Cu composite material and a preparation method thereof, and belongs to the field of composite materials. The ultra-high-strength and ultra-fine grain TiB2 reinforced Al-Zn-Mg-Cu composite material is characterized in that an Al-Zn-Mg-Cu-Zr alloy is used as a matrix, TiB2 with the average size less than 1 micron is used as reinforcing particles, and the composite material comprises the following components of, in percentage by mass, 8%-12% of Zn, 1.0%-2.0% of Mg, 1.0%-1.5% of Cu, 0.05%-0.15% of Zr, 1%-5% of TiB2 and the balance Al. A two-step method is adopted to prepare the composite material, the mass fraction of the TiB2 particles is adjusted, and crystal grains are refined through a rapid solidification process, so that the matrix forms a large solid solution state, and the structure is more uniform.
Owner:WEIHAI WANFENG MAGNESIUM IND DEV +1

Rare-earth alloy permanent magnet material preparation device and technique

A rare-earth alloy permanent magnet material preparation device comprises a raw material treatment portion, a precipitation tank, an electrolytic furnace, a grinding mechanism, a stamping mechanism and a vacuum sintering furnace. The raw material treatment portion comprises a rare-earth metal treatment tank and a blending tank, a delivery pipe connected with the blending tank is arranged on the rear-earth metal treatment tank, the blending tank is connected with the precipitation tank through a complexing solution delivery pipe, the precipitation tank is connected with the electrolytic furnace, a feed inlet is arranged on one side of the electrolytic furnace, a casting chamber is arranged at the tail end of the electrolytic furnace and connected with a cooling chamber, the cooling chamber is connected with the grinding mechanism through a discharge pipe, and the grinding mechanism is connected with the stamping mechanism which is connected with the vacuum sintering furnace. The problem of segregation of alloy ingots is solved effectively, high temperature strength, structural stability, welding performance and corrosion resistance of the alloy ingots are improved beneficially due to addition of Sc, and the common electrolytic furnace can be used for smelting the alloy ingots by adopting mixture after Nd, Pr, Dy and Sc complexing.
Owner:南京萨伯工业设计研究院有限公司

Double-scanning spray forming preparation method of high-carbon wear resisting tool and mold steel

The invention belongs to the field of processing and manufacturing of advanced materials, and relates to a double-scanning spray forming preparation method of high-carbon wear resisting tool and mold steel. The method fully uses advantages of a double-scanning spray forming process, and proposes a double-scanning spray forming preparation process of high-carbon wear resisting tool and mold steel. Compared with a single-nozzle spray forming process, the double-scanning spray forming has the following advantages: (1) the material structure is more uniform; the performance is higher; and the mass and heat distribution of alloy atomization molten drips of double-nozzle spray is more uniform; (2) a deposition blank is more regular in shape; and in two scanning nozzles, one nozzle is used for forming a cylindrical blank, and the other nozzle is mainly used for filling and feeding the middle mass of the blank; and (3) the cost is lower; and as the material yield of double-scanning spray forming is higher, the double-scanning spray forming is lower in cost compared with single-nozzle spray forming.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products