The invention discloses a preparation method for hyperpure sulphuric acid, and fuming sulphuric acid is taken as raw materials. The preparation method comprises the following steps of 1 distilling; 2 purifying and filtering; 3
sulfur trioxide liquid separating; 4 evaporating; 5 multi-stage absorbing; 6 gas stripping
tower impurity removing; 7 finished product obtaining. In the hyperpure sulphuric acid, the concentration of particles with the particle size larger than or equal to 0.5
micrometer is smaller than 5 p / ml, the concentration of particles with the particle size larger than or equal to 0.2
micrometer is smaller than 100 p / ml, the content of single
metal ions is smaller than 0.1 ppb, and the content of
sulfur dioxide is smaller than 3 ppm. According to the preparation method for hyperpure sulphuric acid, the technology is simple, the
energy consumption is low, purified
sulfur trioxide gas is firstly obtained through a reasonable purifying and
impurity removing technology, then ppt-grade hyperpure sulphuric acid is obtained through multi-stage absorbing and gas stripping, the content of trace
sulfur dioxide impurities in hyperpure sulphuric acid is effectively controlled, and a foundation is laid for production of a new generation of hyperpure sulphuric acid.