33results about How to "High active oxygen content" patented technology

The invention provides a preparation method of an oxygen-containing washing agent. The preparation method comprises the following steps of: A, adding 1-10 parts by weight of surfactant, 10-70 parts by weight of sodium carbonate, 1-40 parts by weight of sodium sulfate and a raw material combination containing or not containing additional assistant into a reactor, wherein the additional assistant contains 0-20 parts by weight of sodium bicarbonate, 0-30 parts by weight of silicious sodium salt and 0-10 parts by weight of an anti-dirt redeposition agent; and B, adding an aqueous hydrogen peroxide solution in the reactor, controlling the reaction temperature of the reactor to be 0-60 DEG C, shaping and drying after reaction to obtain 100 parts by weight of the oxygen-containing washing agent the active oxygen content of which is 1-12.33%. The invention also provides the oxygen-containing washing agent prepared by using the preparation method. The preparation method provided by the invention is safe and environment-friendly, and can prepare the oxygen-containing washing agent which has the advantages of uniform component distribution, variable active oxygen content, stable performance,and excellent washing effect.

A chemical to enrich oxygen, and disinfect and clean water for culturing aquatic products is a coated three-element addition of sodium sulfate, hydrogen peroxide and sodium chloride. Its preparing process features that the stabilizer is added in its synthesizing procedure for preventing the decomposition of hydrogen peroxide and product, and increasing the output rate and the content of active oxygen.

The invention discloses a production method of polypropylene cooling masterbatch, including the following steps: (1) mixing: the following components by parts by weight are mixed for 10-20 minutes: 50-90 parts of polypropylene resin, 0.5-9.5 parts of dispersing agent, 0.1-0.6 part of surface modifier, 0.1-2.7 parts of lubricant and 0.2-0.8 part of liquidity regulator, and then the following components by parts by weight are sequentially added: 0.1-0.9 part of light stabilizer, 0.1-1.6 parts of antioxidant and 0.2-7 parts of molecular weight regulator, and mixing is carried out for 5-15 minutes; (2) pelletizing: the mixed material is subject to melt extrusion at 130-230 DEG C and then grain-sized dicing is carried out. The invention adopts compound peroxide as molecular weight regulator and adopts compound antioxidant, compound dispersing agent, compound light stabilizer and compound lubricant, and the produced polypropylene cooling masterbatch has the advantages of high initiator content, good dispersity and obvious cooling effect and modification effect.

The invention discloses a method for preparing canthaxanthin through oxidation.The method includes the steps that beta-carotene serves as the raw material, sulfur oxide urea or urea peroxide serves as an oxidizing agent, an oxidizing reaction is conducted, and the canthaxanthin is obtained.The method has the advantages that operation is simple, the reaction is stable, and the trigger condition is mild; the oxidizing agents including sulfur oxide urea and urea peroxide can be decomposed into H2O2 and elemental oxygen in solvent, O2 is released slowly, the content of active oxygen is high, stability is high, the utility of time is long, no side effect exists, no toxin or public hazard exists, and it is beneficial to achieve industrialized clean production.

The invention discloses a device for preparing plasma activated oil. The device comprises a discharge module and an annular grounding device which are oppositely arranged in the axial direction from the top to the bottom. A gap is arranged between the discharge module and the annular grounding device. The annular grounding device is internally provided with a cavity for storing the oil liquid. Thegap is communicated with the cavity. The discharge module comprises a metal base, multiple current limiting resistors and multiple corresponding metal needle electrodes from the top to the bottom. The first ends of the current limiting resistors are arranged on the bottom surface of the metal base, and the second ends are connected with the rear ends of the metal needle electrodes. The front endsof the metal needle electrodes are opposite to the annular grounding device. The device can produce low temperature plasma at the atmospheric pressure, and the plasma can directly process the activated oil so that the required time is shorter, the power consumption is lower and the device more environment-friendly.

The invention relates to oxygen-containing concentrated laundry powder. The oxygen-containing concentrated laundry powder comprises the following components by weight percent: 5-35% of percarbamide, 5-20% of sodium fatty alcohol-polyxyethylene ether sulfate, 1-8% of sodium dodecyl sulfate, 10-30% of alpha alkene sodium sulfonate, 0.5-5% of sodium fatty acid methyl ester sulfonate, 4-12% of fatty alcohol-polyethylene ether, 0.5-15% of fatty acid sodium and the balance of detergent additive. According to the oxygen-containing concentrated laundry powder provided by the invention, the defects of high energy consumption, poor dissolubility, high alkalinity and high transportation cost of common laundry powder are overcome, and the oxygen-containing concentrated laundry powder has the effects of high concentration, sterilization and bleaching and water conservation, is neutral, mild, bleachable and environmentally-friendly, and the like; and after the laundry powder is used, a white coat is more white, and a color coat is bright.

A method and apparatus for production of a high-concentration H2SO5 solution is presented. This high-concentration H2SO5 solution is useful for producing a stable, non-hygroscopic triple salt. The invention includes a single-stage reactor that includes a reservoir for holding an oxyacid solution and an inlet to the reservoir for receiving a peroxide solution. The peroxide solution is added such that a gradient of peroxide concentration forms in the oxyacid solution as a function of distance from the inlet, and less than all of the oxyacid solution reacts with the peroxide solution at a given time. A stirring mechanism slowly dissipates the gradient, so that any H2SO5 formed as a result of reaction between the peroxide and the oxyacid is stirred away from the high-peroxide concentration zone, thereby preventing the decomposition of H2SO5 by an equilibrium reaction. The temperature of the reservoir is maintained at less than or equal to 20 ° C.

The present invention relates to a preparation of percarbonate. Sodium carbonate solution and hydrogen peroxide solution are added dropwise simultaneously into reactor to prepare sodium percarbonate.The process features the addition of silicate to sodium carbonate solution, the addition of one or more of soluble magnesium salt, organic phosphonic acid, ethylenediamine tetraacetic acid and their salt to hydrogen peroxide solution, and the molar ratio between sodium carbonate and hydrogen peroxide of 0.5-1. The improved wet process of preparing sodium percarbonate has high reaction stability, increased active oxygen content in sodium percarbonate, and improved wet and hot stability.

The invention discloses a peracetic acid solid generating agent as well as a preparation method and an application thereof. The peracetic acid solid generating agent consists of tetra acetyl ethylene diamine, anion active agents and antiseptic agents. A reagent kit used for preparing the peracetic acid consists of peracetic acid solid generating agents and sodium percarbonate. The mol ratio of tetra acetyl ethylene diamine to sodium percarbonate to anion active agents to antiseptic agents is 1 / (0.5 to 2) / (0.2 to 0.5) / (0 to 0.5). The peracetic acid solid generating agent can accelerate the preparation speed of the peracetic acid and is favorable for maintaining effective ingredients of solution, and simultaneously, the washing and cleaning effect of the solution can also be enhanced. The antiseptic agents are added into the system, the corrosion effect of the peracetic acid on various kinds of metals can be reduced, and the stability of the solution is enhanced.

The water dispenser with GAC-O3-UV integrated treatment is aimed at completely eliminating micropollution in the drinking water, and is characterized by that the drying chamber, air pump, ozonizer, GAC-sand filter water injector, water pump, water tank, porous diffuser, fluidic device, spray header, UV254 lamp, GAC exhaust tube, GAC filtration tank, heating and refrigerating machine and accessories are connected together and packaged in same medicine shell. Said water dispenser can implement the disinfection process of drinking water in 20 min-30 min.

This invention relates to a fine chemical product of percarbonamide, a crystal addition compound of hydrogen peroxide and urea, the outlook of which is white crystal powder , the theory active oxygen is 17.02%, and easy to be solved in water and the solution has the performance of hydrogen peroxide and urea liquor having good stability, slow releasing of oxygen and is effective for a long time.

The invention provides a preparation method of a composite potassium monopersulfate disinfectant and antibacterial application thereof in water treatment. The preparation method comprises the steps ofsynthesizing monopersulfuric acid with 30% by mass of hydrogen peroxide and 98% by mass of sulfuric acid, and adding potassium carbonate into the monopersulfuric acid in batch manner to obtain the composite potassium monopersulfate. The composite potassium monopersulfate has excellent performance, with active oxygen content of 3.2-3.4%, monthly average active oxygen loss rate of 0.4% and below, and water content of less than 0.08%; the prepared composite potassium monopersulfate has a wide range of antimicrobial effects, features stability, high efficiency and safety and helps environmentallysolve the problem of disinfection and purification in water treatment.

The invention provides application of Nifeviroc in preparing an antitumor drug, and provides an antitumor drug containing Nifeviroc. As is proved by cell experiments, after Nifeviroc acts on tumor cells, the cell cycle progress can be interfered, and the cell growth is inhibited, so that the cell cycle is stagnant at the G0-G1 stage; meanwhile, cell apoptosis can also be induced by increasing theactive oxygen content in the cells and lowering the mitochondrial membrane potential; meanwhile, Nifeviroc has an obvious effect of inhibiting invasion and metastasis of the tumor cells, by inhibitingadhesive power of the tumor cells to an extracellular matrix, the directed migration capability, the non-targeted migration capability and the in-vitro invasion capability of the cells are lowered, and the increase in size of the tumors in vivo can also be inhibited. As can be seen, Nifeviroc has a good effect of resisting the activity of the tumor, can be used for preparing the antitumor drug, does not have an obvious side effect, and has a good application prospect.

The invention belongs to the technical field of design, research and development of veterinary health preparations, and particularly discloses a formula of a cow hoof bath lotion. The formula comprises the following components in parts by weight: 1.5-25 parts of a bactericide, 0.5-30 parts of polyvinylpyrrolidone, 0.5-15 parts of polyethylene glycol, and 60-90 parts of deionized water. The preparation method comprises: mixing polyvinylpyrrolidone, polyethylene glycol and water, stirring slowly and uniformly for 5-20 minutes, then adding the bactericide, and carrying out stirring for 10-20 minutes to obtain cow hoof bath lotion. A use method comprises using the bath lotion according to a dosage ratio of the bath lotion to water of (10-100):(0-90). The cow hoof bath lotion does not contain heavy metal ions, glutaraldehyde and the like, is easy to degrade, can avoid irritation and carcinogenicity to human beings and animals, and can also avoid continuous damages of broad-spectrum and long-acting bactericides to environmental micro-ecology.

The invention relates to an oligosaccharide preservative for inhibiting fruit softening and reducing mechanical damage harm. The oligosaccharide preservative is prepared by the following steps of inducing one kind or a plurality of kinds of microbes by a 25-percent (w / w) apple pomace composite culture medium to produce a fruit cell wall polysaccharide hydrolase composition through fermentation; treating specific apple pomace wastes by the hydrolase composition under the condition of 10 to 50 DEG C; then, adding 95-percent ethyl alcohol; performing overnight aging under the condition of 4 DEG C; and performing distillation rotation or vacuum freezing concentration after centrifugation to obtain a target preservative. The mass concentration of a product is not lower than 4 percent. After thepreservative is used, the fruit softening can be obviously inhibited. The inhibition rate of the tomato fruit softening reaches 65 percent. Meanwhile, the formation of soluble solids is retarded. Theretarding efficiency is 15 percent to 35 percent according to different storage periods. In addition, after the preservative is used, the self healing capability of the wound of the fruit can be accelerated; the fruit mechanical damage is directly or indirectly reduced; and the shelf life of the fruit is prolonged.

The invention discloses a plasma activated oil treatment device. The plasma activated oil treatment device comprises a plurality of metal needle electrodes, a turbine, a vessel and a plurality of discharge electrodes, the turbine is fixed in the vessel, the center of the turbine is grounded, and a plurality of discharge electrodes are fixedly placed on the surfaces of turbine blades; the vessel isused for containing liquid oil to be activated; the vessel is arranged right below the metal needle-shaped electrode; the metal needle electrode is driven by a power supply to act with the pluralityof discharge electrodes to discharge and generate plasmas; the plasmas are mixed with liquid oil to activate the plasmas to obtain activated oil; when the turbine rotates, the streamer-shaped discharge area between the metal needle-shaped electrode and the discharge electrode is lengthened along with the change of the rotating position of the turbine blade, so that the volume of the plasma is increased; along with the change of the rotating position of the turbine blade, the turbine blade stirs the liquid oil, so that the liquid oil is in more uniform contact with the plasma discharge area, and the plasma concentration in the activated oil is improved. According to the invention, the content of active particles in the plasma activated oil can be greatly improved.

A crystallizing modifier of sodium percarbonate is prepared through dissolving phosphate in water, adding Na2EDTA, hydroxyethylene diphosphonic acid, ethyldiamine tetramethylene phosphonic acid and sodium polyacrylate, and stirring.

The invention provides a composite catalyst for performing catalytic combustion on acetic ether. According to the catalyst, Al2O3 is taken as a carrier; metal Pd is taken as an active component; the mass of metal Pd is 0.1 to 0.5 percent of that of Al2O3; composite non-noble metal oxide is taken as an assistant and is formed by compounding CeO2 and SnO2, with a structural formula being CeO2-SnO2;the mass of CeO2 is 0.5 percent of that of Al2O3; the mass SnO2 is 4 to 20 percent of that of Al2O3. The invention further provides a method for preparing the catalyst and a method for performing catalytic combustion on acetic ether through the catalyst. The catalyst takes non-noble metal oxide as an assistant, and the assistant can increase the content of active oxygen on the surface of the catalyst and improve the activity of the catalytic, has high heat stability, and can rapidly and efficiently eliminate acetic ether in industrial tail gas.

The invention relates to a jet flame and hydrocarbon flame resistant medium-voltage cable for an offshore oil platform and a manufacturing method thereof. A semi-conductive conductor shielding layer,an insulating layer and a semi-conductive insulating shielding layer wrap the periphery of a stranded tin-plated annealed copper conductor from inside to outside in a three-layer co-extrusion mode; atinned copper wire shielding layer is woven on the periphery of a semi-conductive insulation shielding layer to form a shielding wire core, a plurality of shielding wire cores are twisted to form a cable core, an inner silicone oil layer is extruded on the periphery of the cable core, an inner lining layer is extruded on the periphery of the inner silicone oil layer, a fireproof wrapping tape is wrapped on the periphery of the inner lining layer, and an armor layer is wrapped on the periphery of the fireproof wrapping tape; the periphery of the armor layer is extruded with an outer silicone oil layer, the periphery of the outer silicone oil layer is extruded with a jet flame and hydrocarbon flame resistant inner sheath, and the periphery of the jet flame and hydrocarbon flame resistant inner sheath is extruded with a slurry resistant cross-linked polyolefin outer sheath. The cable adopts a double-layer composite sheath, can bear high-temperature flame of 1300 DEG C for 120 minutes under rated voltage, and does not have a grounding fault or a short circuit.

The invention discloses an application of a wild soybean NADPH (Nicotinamide Adenine Dinucleotide Phosphate) oxidase gene GsRbohA1. The invention relates to an application of a wild soybean NADPH oxidase gene GsRbohA1 as shown in SEQ ID NO.1 in gene engineering modification of the resistance of soybeans to prodenia litura. The active oxygen content of the soybean hairy roots over-expressed with the GsRbohA1 is increased, and the resistance to prodenia litura is increased. The soybean hairy roots for inhibiting the expression of the gene have no significant change in resistance to prodenia litura. The wild soybean resistance haplotype GsRbohA1A transcripts more GsRbohA1, accumulates more ROS (reactive oxygen species), and has stronger resistance to prodenia litura. According to the present invention, the wild soybean NADPH oxidase gene GsRbohA1 has the potential of introducing the wild soybean resistance haplotype GsRbohA1A into the cultivated soybean so as to improve the resistance of the soybean to the prodenia litura;

The invention discloses a method for preparing bicalutamide from N-(4-cyano-3-trifluoromethylphenyl)-3-(4-fluorophenylsulfenyl)-2-hydroxy-2-methyl-propanamide. The method adopts N-(4-cyano-3-trifluoromethylphenyl)-3-(4-fluorophenylsulfenyl)-2-hydroxy-2-methyl-propanamide as a raw material, and comprises the following step that bicalutamide is obtained by an oxidation reaction in a solvent in the presence of an oxidizing agent. The method is characterized in that the oxidizing agent is a hydrogen peroxide aqueous solution and the solvent is added with sodium bicarbonate as a catalyst. Compared with the prior art, the method has the advantages that the oxidizing agent and the catalyst all have abundant sources in the market, are cheap and easily available and have low costs; reaction conditions are mild and waste capable of polluting the environment is not produced; and a heavy metal catalyst is not needed so that environmental pollution is reduced and environmental protection requirements are satisfied.

The invention discloses an active oxygen antibacterial and anti-dandruff hair washing gel. The hair washing gel is prepared from, part by weight, 10-16% of an active oxygen coating, 5-10% of cocamidopropyl betaine, 1-3% of cocamide, 0.05-0.2% of climbazole, 0.3-1.6% of guar hydroxypropyltrimonium chloride, 0.02-0.1% of hydantoin, 1-2% of menthol, 0.5-2% of sodium hyaluronate, 1-3% of imidazoline quaternary ammonium salt, 0.6-1% of zinc pyrithione, 1-2.5% of triethanolamine, 0.6-1% of carbomer, 0.1-0.3% of benzophenone, 1-3% of essence and the balance being deionized water. The active oxygen coating is prepared from percarbamide and olive oil, wherein the ratio of the percarbamide to the olive oil is 10:1. The hair washing gel can have sterilization, dirt removal and moisturizing effects through the cooperative use of the components, and the system is stable and synergistic through the compounded combination of the olive oil and the percarbamide.

The invention discloses an active oxygen preparation and fine control integrated device for upgrading and reforming a sewage treatment plant. The integrated device comprises a DC power source 1, an ammeter 2, an oxygen valve 3, an air intake pipe 4, an oxygen pump 5, a water inlet flow meter 6, a water inlet valve 7, a water inlet pipe 8, a water inlet pipe pump 9, a water inlet storage tank 10, an electrolytic tank 11, a Naflon separator 12, a modified negative electrode plate 13 for preparing active oxygen, an active oxygen outlet pipe 14, an active oxygen outlet valve 15, an active oxygen storage tank 16, a modified positive electrode plate17 for preparing the active oxygen, an electrolyte flowmeter 18, an electrolyte inlet valve 19, an electrolyte inlet pipe 20, an electrolyte pipe pump 21, an electrolyte feed storage tank 22, an electrolyte outlet valve 23, an electrolyte outlet pipe 24 and an electrolyte outlet storage tank 25. The beneficial effects of the active oxygen preparation and fine control integrated device are that an aqueous solution having a high active oxygen content and a long stabilization time can be prepared by using the integrated device.

A chemical to enrich oxygen, and disinfect and clean water for culturing aquatic products is a coated three-element addition of sodium sulfate, hydrogen peroxide and sodium chloride. Its preparing process features that the stabilizer is added in its synthesizing procedure for preventing the decomposition of hydrogen peroxide and product, and increasing the output rate and the content of active oxygen.

The invention belongs to the field of organic synthesis and discloses a preparation method of 3,6,9-triethyl-3,6,9-trimethyl-1,4,7-triperoxynonane. The preparation method mainly comprises peroxidatic reaction, condensation polymerization reaction and a blending refining process and particularly comprises the following steps of: stirring concentrated sulfuric acid used as a catalyst as well as hydrogen peroxide and methyl ethyl ketone used as raw materials at the temperature condition of 10-50 DEG C for reacting for 0.5-6.0h, then cooling to 20 DEG C, standing for layering, and retaining an organic layer, wherein the molar ratio of the methyl ethyl ketone to the hydrogen peroxide to the concentrated sulfuric acid is 3:(1-6):(0.3-3); neutralizing the reaction solution with aqueous alkali with the concentration of 10-50% in the organic layer, carrying out washing refining, removing byproducts, after the reaction, standing, cooling, separating the solution, drying, and filtering to obtain a pure target product; and adding a diluent to obtain a finished product. The preparation method disclosed by the invention is simple in reaction process, higher in yield, safe and environment-friendly.

The invention discloses a production method of polypropylene cooling masterbatch, including the following steps: (1) mixing: the following components by parts by weight are mixed for 10-20 minutes: 50-90 parts of polypropylene resin, 0.5-9.5 parts of dispersing agent, 0.1-0.6 part of surface modifier, 0.1-2.7 parts of lubricant and 0.2-0.8 part of liquidity regulator, and then the following components by parts by weight are sequentially added: 0.1-0.9 part of light stabilizer, 0.1-1.6 parts of antioxidant and 0.2-7 parts of molecular weight regulator, and mixing is carried out for 5-15 minutes; (2) pelletizing: the mixed material is subject to melt extrusion at 130-230 DEG C and then grain-sized dicing is carried out. The invention adopts compound peroxide as molecular weight regulator and adopts compound antioxidant, compound dispersing agent, compound light stabilizer and compound lubricant, and the produced polypropylene cooling masterbatch has the advantages of high initiator content, good dispersity and obvious cooling effect and modification effect.

The invention discloses a device and a method for producing potassium peroxymonosulfate composite salt based on a jet reactor, and belongs to the technical field of chemical engineering. The device comprises a jet pipe type oxidation reactor, a jet supplement oxidation reactor, an acid gas absorption tower, a mixing tank, a jet neutralization reactor, a crystallizer I, a crystallizer II, a crystal slurry tank, a horizontal double-drum centrifuge and a fluidized bed dryer. During production, secondary jet oxidation is carried out, and heat transfer and mass transfer are enhanced by the jet tubular oxidation reactor, the jet supplementary oxidation reactor and the jet neutralization reactor; mother liquor and steam condensate are subjected to flash evaporation to recover secondary water vapor to provide an auxiliary heat source for the fluidized bed dryer, and the mother liquor is recycled; and the quality of the prepared potassium peroxymonosulfate composite salt is higher than the national standard of industrial products. The technology is mature, continuous in operation, high in automation degree, capable of recycling resources and environmentally friendly, the device comprehensively saves energy by 10%, and the content of active oxygen is increased by 1%-2%.

The invention provides a composite catalyst for performing catalytic combustion on acetic ether. According to the catalyst, Al2O3 is taken as a carrier; metal Pd is taken as an active component; the mass of metal Pd is 0.1 to 0.5 percent of that of Al2O3; composite non-noble metal oxide is taken as an assistant and is formed by compounding CeO2 and SnO2, with a structural formula being CeO2-SnO2;the mass of CeO2 is 0.5 percent of that of Al2O3; the mass SnO2 is 4 to 20 percent of that of Al2O3. The invention further provides a method for preparing the catalyst and a method for performing catalytic combustion on acetic ether through the catalyst. The catalyst takes non-noble metal oxide as an assistant, and the assistant can increase the content of active oxygen on the surface of the catalyst and improve the activity of the catalytic, has high heat stability, and can rapidly and efficiently eliminate acetic ether in industrial tail gas.

The invention discloses a peracetic acid solid generating agent as well as a preparation method and an application thereof. The peracetic acid solid generating agent consists of tetra acetyl ethylene diamine, anion active agents and antiseptic agents. A reagent kit used for preparing the peracetic acid consists of peracetic acid solid generating agents and sodium percarbonate. The mol ratio of tetra acetyl ethylene diamine to sodium percarbonate to anion active agents to antiseptic agents is 1 / (0.5 to 2) / (0.2 to 0.5) / (0 to 0.5). The peracetic acid solid generating agent can accelerate the preparation speed of the peracetic acid and is favorable for maintaining effective ingredients of solution, and simultaneously, the washing and cleaning effect of the solution can also be enhanced. The antiseptic agents are added into the system, the corrosion effect of the peracetic acid on various kinds of metals can be reduced, and the stability of the solution is enhanced.