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155 results about "Isooctanes" patented technology

Aviation gasoline for aircraft piston engines, preparation process thereof

The subject of the present disclosure is an aviation gasoline composition that is lead-free and free of oxygenated compounds meeting the specifications of the ASTM standard comprising isopentane, isooctane, and (alkyl)aromatics. The aviation gasoline composition according to the disclosure may be obtained simply and economically from a mixture of hydrocarbon bases usually available in a refinery.
Owner:TOTAL MARKETING SERVICES

Method for quickly preparing high-content zanthoxylum unsaturated amide components

The invention discloses a method for quickly preparing high-content zanthoxylum unsaturated amide components. The method comprises the following steps: (1) adding a low-polar solvent into zanthoxylum oleoresin serving as a raw materials, stirring and filtering to obtain solid residues; (2) adding one or more of hexane, cyclohexane and isooctane into the solid residues, heating, performing reflux extraction, and filtering; (3) freezing and crystallizing the filtrate at minus 10- minus 20 DEG C; (4) washing and filtering the crystal, purging and drying in high-purity nitrogen at negative 5-5 DEG C to obtain high-content zanthoxylum unsaturated amide components. According to the method, application of column chromatography in the prior art can be avoided, the high-content unsaturated amide components can be quickly and effectively prepared, and the method is simple and reliable at low cost. Mass spectrum identifies that the prepared crystal sanshool and isomerides, the content detected by high-performance liquid chromatography is over 95 percent, and the crystal can meet basic requirements for reference substance application in the aspects of content detection, quality evaluation and the like.
Owner:NANJING INST FOR THE COMPREHENSIVE UTILIZATION OF WILD PLANTS CHINA COOP

Preparation method of bombyx mori silk fibroin monoclonal antibody

The invention relates to the field of archaeological detection and discloses a preparation method of a bombyx mori silk fibroin monoclonal antibody. The preparation method comprises the following steps: extracting bombyx mori silk fibroin by adopting an isooctane, n-octyl alcohol, bi(2-ethylhexyl) sodium sulfosuccinate and polyvinyl pyridine quaternary ammonium salt mixed system, injecting the bombyx mori silk fibroin serving as a complete antigen into the bodies of rabbits, selecting the rabbits with high immunizing potency, fusing splenic lymphocytes and myeloma cells, cultivating the obtained hybridoma cells, selecting strains with positive secretory antibodies, high secretion ability and good cell growth state by an indirect ELISA method, cloning by a limited dilution method until the antibody secretion positive rate of hybridoma cell growth is 100 percent, performing big turn production on the screened cells, and purifying the obtained monoclonal antibody by a chromatographic column. The antibody prepared by the method has high specificity, and is simple and rapid in operation during the application process and high in detection accuracy.
Owner:ZHEJIANG SCI-TECH UNIV

Extraction tower and process for removing methanol from residual C4 of etherification reaction

The invention relates to an extraction tower and a process for removing methanol from residual C4 of an etherification reaction. The extraction tower comprises a tower body which is internally provided with a plurality of supporting beams; each group of supporting beams corresponds to one layer of tower plate in parallel; a plurality of grooves are formed in each supporting beam at intervals; liquid flow holes communicated with the adjacent lower layer of tower plate are formed in the bottom surfaces of the grooves; each layer of tower plate is formed by splicing a plurality of secondary tower plate pieces; the supporting beams in each two adjacent groups are arranged in a staggered manner; a washing liquid inlet is formed in the upper part of the tower body and a C4 inlet is formed in the lower part of the tower body; a gas-phase outlet is formed in the tower top, and a liquid-phase outlet is formed in the tower bottom. Desalted water which is taken from the outside and has the temperature of 35-45 DEG C enters the tower body from the washing liquid inlet through a desalted water pump, residual C4 of the etherification reaction, which has the temperature of 35-45 DEG C, enters the tower body from the C4 inlet, and the flow ratio of the washing liquid to residual C4 of the etherification reaction is 1 to (20-25). Methanol in mixed C4 with the low methanol content can be removed and the content of methanol in processed mixed C4 is not more than 50ppm so that the consumption amount of a sulfuric acid catalyst in an isooctane device, the energy consumption of the device and the amount of waste acids can be reduced.
Owner:NINGBO HAIYUE NEW MATERIAL

Super-hydrophilic/underwater super-oleophobic copper net and preparation method thereof, and application of super-hydrophilic/underwater super-oleophobic copper net in separation of emulsified oil-in-water

The invention discloses a super-hydrophilic / underwater super-oleophobic copper net and a preparation method thereof, and application of the super-hydrophilic / underwater super-oleophobic copper net inseparation of emulsified oil-in-water. The preparation method comprises the following steps: ultrasonically cleaning a copper net with acetone, ethyl alcohol and deionized water separately, and then drying the copper net; preparing a composite dip-coating solution of polydopamine, polyethyleneimine and aminated carbon nanotubes; immersing the whole pre-cleaned copper net into the dip-coating solution; then putting the whole dip-coating solution system including the copper net on a shaking table for horizontal-rotary coating operation; and taking out the copper net, cleaning the copper net withdeionized water, and drying the copper net. The preparation method has the advantages of simple preparation technology, low raw material consumption, mild reaction conditions and harmlessness to theenvironment, and the obtained super-hydrophilic / underwater super-oleophobic copper net is resistant to physical wear and chemical corrosion and has the function of quickly and efficiently separating various emulsified oil-in-water such as methylbenzene, petroleum ether, isooctane and 1,2-dichloroethane.
Owner:SOUTH CHINA UNIV OF TECH

Method of rapidly and quantitatively analyzing 48 amino acids

The invention discloses a method of rapidly and quantitatively analyzing 48 amino acids. A derivatization reagent combination for quantitatively analyzing and detecting an amino acid content by a derivatization HPLC-MS / MS method is provided, and comprises a derivatization reagent A and a derivatization reagent B; the derivatization reagent A is a mixed solution of n-propanol and 3-methylpyridine;and the derivatization reagent B is a mixed solution of dichloromethane, chloroformyl propyl ester and isooctane. Furthermore, a stable isotope internal standard solution combination, a sample pretreatment method and a liquid chromatography-tandem mass spectrometry method based on the derivatization method are established. The derivatization reagent proposed by the invention has high derivatization efficiency and low toxicity; the method requires fewer samples, the processing is simple and quick, the repeatability is good, and the detection cost is low; absolute quantitative analysis on 48 amino acids is realized by only 22 minutes, the analysis time is greatly shortened, and the detection throughput is improved; and great promotion and application value are achieved.
Owner:GUANGZHOU WOMEN AND CHILDRENS MEDICAL CENTER

Primary oil aid, and primary oil and preparation method thereof

The invention belongs to the field of petrochemical industry, and particularly relates to a primary oil aid, and primary oil and a preparation method thereof, wherein the primary oil aid comprises anantioxidant, a corrosion inhibitor, a detergent dispersant and a cosolvent, has good corrosion resistance, can be adsorbed on the inner surface of an engine so as to prevent the corrosive components in an oil product from corroding the engine, protect the engine and prolong the service life of the engine, and has good oxidation resistance. According to the invention, by combining the primary oil aid, isopentane, isohexane, isooctane, alkylated gasoline, methyl tert-butyl ether, raffinate oil and toluene to obtain primary oil, the primary oil aid can react with the unstable free radicals in theprimary oil to terminate the chain reaction in the fuel oxidation process and eliminate the free radicals, so that the primary oil is in a stable state, the storage time of the engine and the oil product is prolonged, and the good cold starting performance, the combustion performance and the power performance are achieved; and after the primary oil is combusted, the combustion efficiency of the engine is high, the oil consumption is low, and the tail gas emission is little.
Owner:SHANDONG EFIRM BIOCHEMISTRY & ENVIRONMENTAL PROTECTION CO LTD

Rice bran protein porous material and application thereof

The invention belongs to the field of porous polymer materials, and particularly relates to a rice bran protein porous material with strong adsorption performance. The porous material is prepared by the following steps: adding rice bran protein into a solution to form a rice bran protein solution, performing modification treatment, conducting stirring, foaming, freezing, plasticizing, and freeze-drying to obtain the rice bran protein intercommunication porous material with high adsorption of organic solvents and grease, light weight, high porosity, degradability, greenness and environment-friendliness. The organic solvents comprise one or more of acetonitrile, methanol, ethyl acetate, isooctane, petroleum ether, cyclohexane and glycerol; The grease comprises one or more of rice bran oil, soybean oil, sunflower oil or medium-chain triglyceride. The preparation method provided by the invention is simple in process, easy to operate and suitable for large-scale production in factories, theraw materials are from natural products, and thus the prepared porous material is safe and non-toxic, has good biocompatibility, and can be widely applied to the fields of food, organic solvent wasteliquid transportation, biomedical materials and the like.
Owner:SOUTH CHINA AGRI UNIV

Super-hydrophobic manganese dioxide coating on metallic material surfaces and preparation method thereof

The present invention discloses a durable super-hydrophobic manganese dioxide coating and a preparation method thereof, belonging to the field of metallic material surface treatment. In the method, by using manganese sulfate as a raw material, based on the property of interface reaction, a manganese dioxide coating is synthesized on the metallic material surface by simple and convenient solution impregnation, and then processed by hydrophobization with stearic acid to obtain a super-hydrophobic manganese dioxide coating. This coating has excellent chemical stability to organic solvents such as n-hexane, isooctane, dodecane, tetradecane, and acids, alkali and salt solutions at different pH values, and exhibits great resistance against dynamic water shear and good durability, with broad application prospect.
Owner:EAST CHINA JIAOTONG UNIVERSITY

Producing a Trimethylpentanoic Acid Using Hybrid Polyketide Synthases

The present invention provides for a polyketide synthase (PKS) capable of synthesizing trimethylpentanoic acid. The present invention also provides for a host cell comprising the PKS and when cultured produces the trimethylpentanoic acid. The present invention also provides for a method of producing the trimethylpentanoic acid, comprising: providing a host cell of the present invention, and culturing said host cell in a suitable culture medium such that the trimethylpentanoic acid is produced, optionally isolating the trimethylpentanoic acid, and optionally, reducing the isolated trimethylpentanoic acid into a trimethylpentanol or an iso-octane.
Owner:RGT UNIV OF CALIFORNIA

Superposition oil hydrogenation device and method capable of producing isooctane

The invention discloses a superposition oil hydrogenation device and method capable of producing isooctane, and belongs to the technical field of petrochemical engineering. The device comprises a catalytic distillation hydrogenation column, a condenser, a reflux tank, a reboiler, a first compressor and a hydrogenation reactor; the top of the catalytic distillation hydrogenation column is connectedwith the condenser, the condenser is connected with one inlet of the reflux tank, one outlet of the reflux tank is connected with the first compressor, and the other outlet of the reflux tank is connected with the catalytic distillation hydrogenation column; the reboiler is arranged at the bottom of the catalytic distillation column; and the bottom of the hydrogenation reactor is connected with the catalytic distillation hydrogenation column. According to the superposition oil hydrogenation device and method capable of producing the isooctane, olefin in superimposed oil can be saturated, requirements of the superposition oil as a vehicle gasoline blending component are met and the isooctane is produced as needed, a hydrogenation reaction is separately carried out on different components in the superimposed oil through the catalytic distillation column and the hydrogenation reactor, the equipment and operation costs can be reduced, and the purpose of energy saving and flexible operation is achieved.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Chromatographic method for determining content of EPA, DHA and total w-3 acids in fish oil

The invention discloses a chromatographic method for determining the content of EPA, DHA and total w-3 acids in fish oil. The method comprises the following steps: 1, esterifying; 2, preparing a sample solution; 3, preparing a standard substance solution; 4, setting chromatographic conditions; 5, sequentially introducing samples; and 6, comparing the relation between the retention time and the peak area of a sample to be determined with that of a standard substance to determine the content in the sample. In the w-3 fatty acid-containing fish oil sample treatment process, unsaturated fatty acids is saponified, saponified unsaturated fatty acids and a methanol solution of boron trifluoride directly undergo an ester formation reaction, and unsaturated fatty acid esters are directly extracted by a BHT-containing isooctane solution to obtain a solution used as the sample to be determined. The method adopting the appropriate ester formation process and the sample post-treatment process has the advantages of short test operation cycle, effective avoiding of volatilization and other problems in the operation, and accurate and reliable determination result, and is especially suitable for industrial production and other occasions needing large scale determination.
Owner:JIANGSU ALAND NOURISHMENT

Application of reverse micelle system in catalysis of lignin peroxidase for esterification reaction of oleic acid

The invention discloses an application of a reverse micelle system in the catalysis of lignin peroxidase for an esterification reaction of an oleic acid. The reverse micelle system consists of rhamnoilpid, iso-octane and n-hexanol, wherein the ratio of the iso-octane to the n-hexanol is 1:(1-3); the clinical micelle of the reverse micelle system is 20 to 100 CMC. The application comprises the following steps of mixing crude enzyme of the lignin peroxidase and the reverse micelle system to form a reverse micelle enzyme system, adding the oleic acid and C1-C10 organic alcohol, and performing water bath shaking to obtain an esterification product, wherein the crude enzyme of the lignin peroxidase consists of lignin peroxidase and a buffer solution. The application of the reverse micelle system in the catalysis of the lignin peroxidase for the esterification reaction of the oleic acid is environment-friendly, safe, convenient to operate, low in cost and high in efficiency and yield.
Owner:HUNAN UNIV

Production method for generating isooctene by utilizing acetic acid and mixed C4 and producing high-purity isooctane by hydrogenating

The invention discloses a production method for generating isooctene by utilizing acetic acid and mixed C4 and producing high-purity isooctane by hydrogenating. The production method is characterizedby comprising the following steps: step 1, carrying out esterification; enabling acetic acid and isobutene in the mixed C4 to be subjected to esterification reaction, so as to generate tert-butyl acetate; step, carrying out polymerization; decomposing tert-butyl acetate into isobutene and synchronously carrying out dimerization reaction to generate isooctene; then carrying out steam stripping separation; carrying out distillation separation on a liquid-phase material to obtain isooctene; carrying out third-step recycling reaction on a gas phase; step 3, carrying out recycling and esterification on isobutene; step 4, hydrogenating and desulfurizing isooctene to obtain the high-purity isooctane and hydrogen sulfide. The method disclosed by the invention is green and environmentally friendly,high dimerization selectivity and high product purity; an intermediate product and acetic acid can be circularly utilized and requirements on large-scale and continuous production can be met; an MTBE(Methyl Tert-butyl Ether) device can be replaced after ethanol gasoline of China is implemented.
Owner:YUEYANG FUHE TECH

D-A-D type organic photo-thermal small molecular material and preparation method thereof

The invention provides a D-A-D type organic photo-thermal small molecular material and a preparation method thereof. The D-A-D type organic photo-thermal small molecular material contains an electronwithdrawing group 2,1,3-benzothiadiazole and an electron donating group 3,6-di(thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c] pyrrole-1,4-dione. The preparation method comprises the steps: substituting H ona thiophene ring of bromo-isooctane substituted 3,6-di(thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione with N-bromo-succinimide, and carrying out a reaction with 2,1,3-benzothiadiazole-4,7-bis(pinacol borate) through Suzuki reaction to obtain the target product. With the introduction of an alkyl chain on the side chain of the electron donating group, the solubility of the organic photo-thermal material in the organic solvent is improved, the problem of poor solubility of the organic polymer is overcome, and favorable light stability is achieved.
Owner:SHANXI UNIV

Isooctane production line

The invention discloses an isooctane production line. The isooctane production line comprises a coolant pump (10), a raw material buffer tank (11), a depropanization tower (12), a return tank (13), a dehydrater (20), a reactor (21), a flash tank (22), a pickling settling chamber (23), an alkali wash settling chamber (24), a deisobutanizer (25) and an n-butane removal tower (26), wherein the raw material buffer tank (11) comprises a tank shell (15) and a group of separators (16). The isooctane production line disclosed by the invention has the advantages that due to the group of separators in the buffer tank, the gas flow time in the buffer tank is increased, and the liquefaction efficiency is improved; the tank body is separated into an upper part and a lower part by a spherical separator, so that the contact area between mixed gases and condensing agents is enlarged by the spherical separator, and the cooling effect is improved; the flash effect is improved by changing the contact area and time between liquid in the flash tank and air; and the whole production line is reasonable in structure and high in efficiency.
Owner:荆门市渝楚化工有限公司

High-octane-value oil product composition, primary oil and preparation method of primary oil

The invention relates to the field of petroleum products, and specifically discloses a high-octane-value oil product composition, primary oil and a preparation method of the primary oil. The oil product composition is prepared from the following raw materials in parts by weight: 62-86 parts of isooctane, 12-21 parts of methyl tert-butyl ether and 2-17 parts of benzene-making raffinate oil, the research octane number of the oil product composition is greater than or equal to 97.6, and the motor octane number of the oil product composition is not greater than 91.0; the invention further discloses the primary oil, which comprises the high-octane-value oil product composition and further comprises 0.0002-0.002 part by weight of an antistatic agent. The preparation method of the primary oil comprises the following steps: uniformly mixing the raw materials according to the proportion to obtain the primary oil. The oil product composition and the primary oil prepared in the invention have thecharacteristics of high octane number, especially high motor octane number, stable quality and clean combustion, and meet the use requirements of a high compression ratio engine, and the preparationmethod has the characteristics of simple and convenient operation and stable finished product.
Owner:北京中燕恒成能源有限公司
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