66results about How to "Easy to form large-scale production" patented technology

The invention provides a continuous blowing and casting method of oxygen-free copper ingots, which pertains to the metal smelting and casting technical field and is carried out according to the technical steps as follows: A. cathode copper is firstly melted in a smelting furnace, and melted copper liquid enters a deoxidation furnace through a bottom blowing chute; B. carbon monoxide gas or the mixed gas of carbon monoxide and nitrogen enters the copper liquid in the bottom blowing chute through the bottom blowing chute and enters the deoxidation furnace with the copper liquid to realize the deoxidation and the degassing of a first stage; C. when passing through a diversion trench arranged in a bottom blowing furnace end, the carbon monoxide gas or the mixed gas of carbon monoxide and nitrogen enters the copper liquid in the diversion trench for realizing the deoxidation and the degassing of a second stage to the copper liquid in the diversion trench; D. the copper liquid after the second stage of deoxidation and degassing enters a crystallizer through a casting gate arranged in the bottom blowing furnace end. The oxygen content of an oxygen-free copper ingot base produced by the method of the invention can stably reach not only less than 5ppm, but also less than 3ppm.

The invention provides a continuous blowing and casting furnace of oxygen-free copper ingots, which pertains to the technical field of manufacturing metal smelting and casting equipment. The furnace essentially comprises a furnace shell (3) which is externally coated with refractory bricks (1), a smelting furnace (4) and a deoxidation furnace (10) which are provided with an electric inductive heater (17) at the bottom and arranged in the furnace shell (3) in parallel, a bottom blowing chute (19) which is provided with gas permeable bricks (22) at the bottom and arranged between the smelting furnace (4) and the deoxidation furnace (10), a bottom blowing furnace end (11) which is provided with a casting gate (20) and bottom blowing bricks (12) at the bottom and connected with the deoxidation furnace (10), a diversion trench (21) which is distributed in an 'S' shape and arranged in the bottom blowing furnace end (11), a smelting furnace cover (5) arranged at the upper part of the smelting furnace (4) and a deoxidation furnace cover (9) which is provided with a vent (8) and arranged at the upper part of the deoxidation furnace (10), etc. The whole structure of the furnace has reasonable design, convenient operation, low cost, being stable and reliable and can effectively reduce the oxygen content and the casting cost of oxygen-free copper, thereby being easy to form mass production.

The invention discloses a preparation method of silicon dioxide@ quantum dot composite nanoparticles. The method comprises steps as follows: thiolation silicon dioxide nanoparticles are prepared firstly, and the silicon dioxide@ quantum dot composite nanoparticles are prepared with a hydrothermal method. The preparation method is simple and easy to implement, high in yield and efficiency and beneficial to large-scale production. The prepared silicon dioxide@ quantum dot composite nanoparticles comprise silicon dioxide balls with particle sizes of 50-800 nm and quantum dot particles loaded on the silicon dioxide balls. The excellent fluorescence property of quantum dots is preserved, centrifugal separation of the particles is facilitated due to the fact that the quantum dots are loaded on silicon dioxide, the aftertreatment steps during use of the quantum dots are greatly optimized and simplified, and the preparation method has a broad application prospect.

The invention relates to a method for preparing 1,2-cyclohexanediol through carrying out catalytic oxidation on cyclohexene by using a phase transfer catalyst. 1,2-cyclohexanediol is prepared through carrying out catalytic oxidation on cyclohexene by taking quaternary ammonium decatungstate as the phase transfer catalyst, phosphoric acid as a catalyst promoter and hydrogen peroxide as an oxidizing agent. The method has the advantages that toxic and harmful organic solvents such as acetonitrile, methylbenzene and methanoic acid are not used as reaction media, the environment pollution is reduced, the risk of combustion explosion generated in the reaction process is reduced, and large-scale production is easy to realize; the used catalyst, i.e., quaternary ammonium decatungstate, has high catalytic activity; and 1,2-cyclohexanediol is simple in preparation process, convenient to separate and recycle and favorable in application prospect.

Method for removing environmental pollutant ethylene bisphenol A is carried out by dripping carbonate solution into ethylene bisphenol A, Ni-Al alloy and solution while agitating and heating, reacting Ni-Al alloy with carbonate solution to produce hydrogen, reducing and debrominating ethylene bisphenol A into reactive product bisphenol A. It is simple and convenient, has higher reutilization and no environmental pollution.