The invention relates to a preparation method of
nickel-coated
alumina oxide powder, in particular to the preparation method of
nickel-coated aluminum
oxide powder for
thermal spraying in
aviation,
aerospace and military fields. The invention is characterized in that: a suspension is made from a mixing liquid of nano-aluminum
oxide and dispersant, stirred and added with
nickel salt solution at the same time, and the obtained mixture liquid is dropped with
ammonium water after being fully stirred, added with
distilled water, when dark blue mixing solution C of nickel
ammonia complex ([Ni (NH3)) 2+and
alumina oxide is obtained; the mixing solution C is aged by water, filtered, washed and dried, and a green middle coated product is obtained; the green middle coated product is further reduced and roasted, finally, black nickel-coated aluminum oxide
powder is prepared. The nickel-coated aluminum oxide powder prepared through the invention has uniform
granularity, with
average size less than or equal to 1.0Mum, and can enhance the application performance of nano-
alumina and expand the application of nano-aluminum oxide; the product is mainly used for
aviation,
aerospace and military materials and other high-tech fields. The method of the invention is simple, reproducible and easy to be industrialized.