The invention discloses a general synthesis method of a three-dimensional
compound structure based on three-dimensional MXene, and belongs to the field of nano materials. The three-dimensional
compound structure is composed of a three-dimensional MXene load inorganic nano structure and is of a flower-like
hierarchical porous structure. The method comprises the steps that an
ultrasonic atomizer isadopted for atomizing mixed suspension liquid of three-dimensional MXene particles,
metal salt and an auxiliary into
aerosol micro-droplets, and under
inert or reactive
atmosphere, high-temperature fast
drying is conducted to obtain the three-dimensional
compound structure with controllable structure and size; or the three-dimensional MXene particles and
metal salt or a nonmetallic compound are evenly mixed in
solvent or in a
solid-phase mode to obtain a mixture, and high-temperature
calcination is conducted under the
inert or reactive
atmosphere to obtain the three-dimensional compound structure with controllable structure and size. By means of the three-dimensional compound
structure based on the three-dimensional MXene, the problems of inorganic nano material
particle aggregation, poorconductivity and two-dimensional MXene stacking can be solved, and thus a foundation is laid for preparation,
processing and various aspects of application of a MXene-based high-performance functionalmaterial.