The invention discloses a method for recycling walnut
polyphenol and flavone in walnut kernel peeling
wastewater through
macroporous resin. The method comprises the operating steps of pretreatment of the walnut kernel peeling
wastewater, separation, purification and regeneration of the macroporous adsorption resin, concentration and
drying. The concentration of the walnut flavone in the pretreated walnut kernel peeling
wastewater is reduced to 0.34mg / mL-0.67mg / mL through
dilution, the pH value is adjusted to be 7-9 through concentrated
hydrochloric acid, a solution is poured into an adsorption tank filled with the
macroporous resin to be adsorbed, the adsorption time is more than 4 hours, after adsorption is finished,
desorption is conducted through 60%-80% ethyl
alcohol to obtain an ethyl
alcohol walnut flavone solution, the solution is processed through
vacuum evaporation, concentration and
drying, the ethyl
alcohol is recycled, and finally fine walnut flavone extract is obtained. The recycling rate of the walnut flavone is more than 70%, and the purity of the walnut flavone is more than 50%. The technological process is simple, the cost is low, the benefit is high, the
macroporous resin can be regenerated and recycled, and the method is suitable for industrial recycling of walnut flavone compounds in the walnut kernel peeling wastewater.