A synthesis method of order mesoporous
metal oxide with high specific surface area by hard template agent belongs to the filed of the preparation of
solid mesoporous materials. The prior art is difficult to control the problems of the
hydrolysis rate of
metal salt, easy collapse and the poor universality of channels when templates are removed by
calcination, etc. In the invention, firstly, hard template agent cubic-phase mesoporous
silicon oxide powder is synthetized; the
silicon oxide powder is added into 50 to 95wt percent of ethyl
alcohol solution of
metal salt with the concentration of 0.12 to 0.40 mol / L to form
mixed solution; after 90 to 120 min of
ultrasonic dispersion, the product is mixed again, vaporized under the temperature of 40 DEG C to 50 DEG C and dried; and then the product is heated to 400 DEG C to 850 DEG C in
atmosphere at 1 DEG C / min, and kept for 4 hours under the temperature to obtain the mesoporous oxide precursor
powder; the mol ratio of the cubic-phase mesoporous
silicon oxide powder and the metal salt is 7-14; 10wt percent of HF solution is used to wash, so as to remove the cubic-phase mesoporous
silicon oxide template agent, and the product is dried under 60 DEG C to 70 DEG C for 20 to 24 hours. The mesoporous metal oxide of the invention is suitable to be adsorbent, catalyst, carrier, etc., and is applicable to dyes, magnetic, photoelectric materials, etc.