Method for regenerating normalization spandex fibre from dry spinning spandex waste silk
A technology of spandex waste and spandex yarn is applied in the field of spandex yarn, which can solve the problems of inability to complete the regeneration of dry-spun spandex waste yarn, unable to remanufacture spandex yarn, etc., and achieves the effects of less investment, great economic benefit, and simple operation process.
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Embodiment 1
[0021] The present invention regenerates dry-spinning spandex waste into normal spandex, comprising the following steps:
[0022] (1) Use a low-temperature pulverizer below -30°C to change spandex waste from filaments to short fibers;
[0023] (2) Remove the oil on the surface of the spandex waste silk with water and detergent;
[0024] (3), remove the moisture on the spandex waste silk with drying method;
[0025] (4), put the spandex waste silk after degreasing and drying into the reactor, and add organic solvent dimethylacetamide (DMAC), reaction terminator, anti-aging agent, fiber forming agent, spandex waste silk and organic The mass ratio of the solvent is 1:1, according to the mass percentage of spandex waste silk, the reaction termination dose is 0.01%, the antiaging agent is 0.2%, and the fiber forming agent is 0.2%. Stir at 45°C-100°C for 6-12 hours to obtain a suitable Viscosity spinning dope;
[0026] (5) Remove the air bubbles in the spinning dope;
[0027] (6...
Embodiment 2
[0029] The difference between a method of regenerating dry-spinning spandex waste silk into normal spandex silk and embodiment 1 of the present invention is:
[0030] The organic solvent is dimethylformamide (DMF), and the mass ratio of spandex waste silk to organic solvent is 1:2. According to the mass percentage of spandex waste silk, the reaction terminator is 0.5%, the antiaging agent is 0.01%, and the fiber forming agent 0.3%.
Embodiment 3
[0032] The difference between a method of regenerating dry-spinning spandex waste silk into normal spandex silk and embodiment 1 of the present invention is:
[0033] Organic solvent is dimethylformamide (DMF), spandex waste silk and organic solvent mass ratio are 1: 3, according to the mass percentage of spandex waste silk, reaction terminator is 0.2%, anti-aging agent 0.3%, fiber forming agent 0.01%.
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