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47 results about "Benzyl peroxide" patented technology

Preparation method of phosphorus-containing flame-retardant polymethyl methacrylate resin

InactiveCN105384858ABenzenePhosphate
The invention relates to a preparation method of phosphorus-containing flame-retardant polymethyl methacrylate resin. A formula for preparing the phosphorus-containing flame-retardant polymethyl methacrylate resin comprises the following components by weight percent: 17.92 to 22.65 percent of tri((6-oxo-6H-dibenz [c,e][1,2] oxaphosphorin-6-yl)methyl) phosphate, 78.16 to 82.39 percent of methyl methacrylate and 0.16 to 0.76 percent of benzoperoxide. The preparation method comprises the following steps: adding a formula amount of methyl methacrylate, tri((6-oxo-6H-dibenz [c,e][1,2] oxaphosphorin-6-yl)methyl) phosphate and initiator benzoperoxide into a reaction container, stirring about 52 min at 85.2 DEG C, allowing the system to be viscous, then pouring a prepolymer into a mold, cooling to about 40 DEG C, performing the heat insulation for 6h, then heating to 80 DEG C, and performing the heat insulation for 12h to obtain the flame-retardant polymethyl methacrylate resin.
Owner:LANZHOU UNIVERSITY OF TECHNOLOGY

Lithium anode-protecting polymer layer for a lithium metal secondary battery and manufacturing method

Provided is lithium secondary battery comprising a cathode, an anode, and an electrolyte or separator-electrolyte assembly disposed between the cathode and the anode, wherein the anode comprises: (a)a foil or coating of lithium or lithium alloy; and (b) a thin layer of a high-elasticity polymer disposed between the foil / coating and the electrolyte (or separator-electrolyte assembly), having a recoverable tensile strain no less than 2%, a lithium ion conductivity no less than 10-6 S / cm at room temperature, and a thickness from 1 nm to 10 [mu]m, wherein the high-elasticity polymer contains a cross-linked network of polymer chains having an ether linkage, nitrile-derived linkage, benzo peroxide-derived linkage, ethylene oxide linkage, propylene oxide linkage, vinyl alcohol linkage, cyano-resin linkage, triacrylate monomer-derived linkage, tetraacrylate monomer-derived linkage, or a combination thereof in the cross-linked network of polymer chains.
Owner:NANOTEK INSTR

Thermoplastic-elastomer-modified polymethyl methacrylate color antiskid paint

The invention provides a thermoplastic-elastomer-modified polymethyl methacrylate color antiskid paint. The paint is of a three-component reaction type and comprises a component A, a component B and a component C, wherein the ratio of the component A to the component B to the component C is 100 to (50-200) to (5-30); and the paint is formed by mixing the three components. The component A is MMA resin liquid modified by thermoplastic elastomer and tackifying resin, the component B is graded waste tire rubber particles, and the component C is formed by mixing and dissolving 2 to 3 parts of benz peroxide and 10 to 30 parts of dibutyl phthalate. The thermoplastic-elastomer-modified polymethyl methacrylate color antiskid paint has beneficial effects that an energy-saving, high-efficient and durable color antiskid paint for roads and bridges is provided, the cost can be reduced, the energy consumption can be reduced, the economic benefit and social benefit can be improved, and various technical indexes of the paint can reach or exceed that of the color antiskid paint sold in the market.
Owner:广东立得新材料科技有限公司

Polyphenyl thioether composite material for 3D printing and preparation method thereof

The invention provides a polyphenyl thioether composite material for 3D printing and a preparation method thereof. The preparation method comprises the following steps: dissolving N-vinyl-2-pyrrolidone in ethanol, adding benzoperoxide, standing at room temperature, sequentially adding terephthalic acid and ethyl alpha-cyanoacrylate, stirring at room temperature, adding polyphenyl thioether particles, heating while stirring, and cooling to room temperature, thereby obtaining the polyphenyl thioether composite material for 3D printing. The polyphenyl thioether composite material can be used for 3D printing within the temperature range of 40-70 DEG C, can not block the 3D printer injector, and overcomes the defect that the polyphenyl thioether consumable 3D printing needs to melt the high-molecular polymers under high-temperature conditions; and the preparation method has the advantages of simple technique and low production cost, is convenient for popularization and application, and enriches the varieties of the 3D printing consumables.
Owner:TAICANG BIQI NEW MATERIAL RES & DEV

Preparation method of ethylenediamine modified maleic anhydride polylactide-glycolide polymer

ActiveCN104177553AImprove hydrophilicityAlleviate acid build-upEthylenediamineBiocompatibility Testing
The invention provides a preparation method of an ethylenediamine modified maleic anhydride polylactide-glycolide polymer disclosed as Formula (I), which comprises the following steps: by using D,L-lactide, glycolide and maleic anhydride as raw materials, stannous octanoate as a catalyst and benzoperoxide as an initiator, carrying out polymerization in an ampoule bottle under high-vacuum conditions to prepare maleic anhydride polylactide-glycolide (MPLGA), adding a trichloromethane solution of ethylenediamine into a trichloromethane solution of the MPLGA while stirring, keeping the temperature at lower than 10 DEG C for 5-10 minutes, reacting at room temperature for 30-60 minutes, dropwisely adding the product into excessive solvent, precipitating, washing with deionized water to a neutral state, and carrying out vacuum drying to constant weight, thereby obtaining the ethylenediamine modified maleic anhydride polylactide-glycolide polymer solid. The product has higher hydrophilicity and biocompatibility.
Owner:HUNAN UNIV OF SCI & TECH

Formula and use method of lens anti-fog wet tissue

The invention discloses a formula and a use method of a lens anti-fog wet tissue. According to the formula and the use method of the lens anti-fog wet tissue, the lens anti-fog wet tissue is preparedfrom the following raw materials: 1-3 parts of acrylic acid, 8-10 parts of methyl methacrylate, 2-5 parts of ethyl methacrylate, 8-10 parts of butyl methacrylate, 60-80 parts of butanone, 2-5 parts ofbenzoyl peroxide, 10-20 parts of a silver ion antibacterial agent, 30-50 parts of ethanol and 1-3 parts of fatty alcohol-polyoxyethylene ether sodium sulfate. Ethyl methacrylate mixed with fatty alcohol-polyoxyethylene ether sodium sulfate can be effectively attached to the surfaces of the lenses to prevent the lenses from fogging to influence the sight of people, so that the personal safety of people wearing the lenses is improved; silver ion disinfection powder is added into the anti-fog wet tissue, so that the surface of the lens is sterilized and disinfected while the lens is placed in the anti-fog agent and fogged, the face of a human body is prevented from being in contact with infectious microbes, the personal safety of people during use is guaranteed, and the product characteristics of the anti-fog wet tissue are improved.
Owner:南昌迈进科技有限公司

Two-component adhesive for bonding artificial teeth to a denture base

A mixture containing at least one first component A and at least one second component B, characterized in that said at least one first component A comprises a methyl methacrylate, a copolymer of methyl methacrylate dissolved in excess methyl methacrylate, optionally comprising, additionally dissolved therein, atleast one polyfunctional (meth)acrylate, especially ethylene glycol dimethacrylate, butanediol dimethacrylate, hexanediol dimethacrylate, triethylene glycol dimethacrylate (TEGDMA), tetraethylene glycol dimethacrylate, diurethane dimeth- acrylate, bis(hydroxymethacryloyloxypropoxy)phenylpropane (bis-GMA), polyethylene glycol dimethacrylate, trimethylolpropane trimethacrylate, ditrimethylol- propane tetraacrylate;and a peroxide-based free-radical initiator, wherein said copolymer of methyl methacrylate is present in an amount of 30-50 parts by weight dissolved in a solution of 65-85 parts by weight of monomeric methyl methacrylate and 3-15 parts by weight of the polyfunctional (meth)acrylate, especially the triethylene glycol dimethacrylate (TEGDMA), mixed with a solution of 0.5 to 3 parts by weight of said peroxide-based free-radical initiator, especially dibenzoyl peroxide, in 70-90 parts by weight of monomeric methyl methacrylate, and said at least one second component B comprises methyl methacrylate and a tertiary amine.
Owner:VITA ZAHNFABRIK H RAUTER GMBH & CO KG

CPE (Chlorinated polyethylene) coated quartz sand modified low-density polyethylene foam material and preparation method thereof

The invention discloses a CPE (chlorinated polyethylene) coated quartz sand modified low-density polyethylene foam material. The low-density polyethylene foam material is prepared from the following raw materials in parts by weight: 60-100 parts of LDPE (low-density polyethylene), 0-40 parts of LLDPE (linear low-density polyethylene), 30-40 parts of CPE, 10-20 parts of quartz sand, 2-3 parts of vinyl tris(beta-methoxyethoxy) silane, 5-10 parts of triphenyl phosphate, 4-6 parts of 4,4'-oxydibenzenesulfonyl hydrazide, 2-3 parts of ammonium bicarbonate, 5-8 parts of n-butyl methacrylate, 1-1.5 parts of 2,4-dichlorobenzoyl peroxide, 2-3 parts of zinc stearate, 1-2 parts of calcium stearate, 1-2 parts of lead sulfate tribasic, 2-3 parts of polyethylene wax, 3-5 parts of modified tree ash, 1-2 parts of ultraviolet light absorber THUV-328 and 2-3 parts of antioxidant 264. The CPE-coated quartz sand modified low-density polyethylene foam material disclosed by the invention is light in weight, soft, high in strength and good in rebound resilience, the foaming effect is ideal, and bubble holes are uniform, small and dense, so that the CPE-coated quartz sand modified low-density polyethylene foam material is good in fire resistance, resistant to chemical corrosion and ageing and is durable in use.
Owner:重庆锋胜包装材料有限公司

Water-glass-containing compression-resistant impervious wear-resistant reinforced concrete drainage pipe and preparation method thereof

The invention discloses a water-glass-containing compression-resistant impervious wear-resistant reinforced concrete drainage pipe and a preparation method thereof. The invention is characterized in that the drainage pipe is prepared from fly ash, mineral slag powder, metakaolin, gypsum, sodium sulfate, a naphthalene high efficiency water reducing agent, sand, gravel, a bisphenol A epoxy resin E-44, benzoperoxide, acrylic acid, N,N-dimethylethanolamine, organic montmorillonite, cement, steel fibers, calcined diatomite, steel bars, urea, sodium methylsiliconate, potassium dichromate, water glass and the like. The water-based epoxy resin is prepared by graft copolymerization, thereby obtaining the polymer-cement base material interpenetrating-network structure. The organic montmorillonite used as the filler is added into the water-based epoxy resin matrix by high-polymer solution intercalation to prepare the water-based epoxy resin / montmorillonite nano composite material. The uniform intense magnetic field is applied to the steel fiber reinforced concrete mixture to prepare the one-way-distributed steel fiber reinforced concrete, so the fibers have high utilization ratio and favorable reinforcement effect.
Owner:阜阳市华顺水泥制品有限公司

A kind of method that benzyl peroxide is prepared by toluene liquid-phase air oxidation method

The invention discloses a method for preparing benzyl peroxide by adopting a toluene liquid-phase air oxidation method. Under the synergistic effect of a catalyst, an initiator and an assistant, toluene and oxygen in the air perform oxidizing reaction to generate the benzyl peroxide, the balance of reaction temperature is ensured by adopting an external circulated cooling mode, pressure balance in a toluene oxidation reactor is controlled according to the discharge amount of high-temperature compressed tail gas or nitrogen or reaction tail gas led from the upper portion of the reactor, the reaction process is full-automatically controlled, and safe, stable and continuous reaction is ensured. The oxygen content in the reaction tail gas is ensured by controlling the high-temperature compressed tail gas or nitrogen led from the lower portion of the reactor and reaction conditions, and higher toluene conversion rate is ensured. The product benzyl peroxide can serve as a raw production material of benzene-alcohol, aromatic aldehyde, aromatic acid and benzyl ester, and the method is a green and environment-friendly no-chloride involved process.
Owner:湖北科林博伦新材料有限公司
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