2744results about How to "Thorough response" patented technology

The invention provides a ceramsite water permeable brick, which comprises the following components by weight: 80-100 parts of ceramsite, 10-15 parts of silicon sand, 20-40 parts of cement, a setting accelerator accounting for 2-4% of the weight of the ceramsite, and a water reducing agent accounting for 2-4% of the weight of the ceramsite. According to the invention, silicon sand dust made ceramsite is combined with a small quantity of cement, the setting accelerator, the water reducing agent and a silicon sand fabric to manufacture the ceramsite water permeable brick. One the one hand, the water permeable brick has a beautiful appearance, and on the other hand it combines the lightweight and high strength characteristics of ceramsite. At the same time, ceramsite is round stone rather than polygonal, and usually the gap between round objects is larger than that between polygonal objects, so that the prepared water permeable brick has good permeability effect. The water permeable brick prepared by the method has compressive strength of greater than or equal to 30Mpa and a permeability coefficient of greater than or equal to 0.05cm/s, and the other properties of the brick meet the JCT945-2005 industrial standard.

The invention provides a hydrolyzing and separation device of methyl acetate and a technique method thereof, which more particularly relates to a novel technique to catalyze and hydrolyze methyl acetate by a reaction bulkhead distillation tower, which can organically combine reaction process, product separation and recovery of no reactant into the tower. A separator extending from the upper part of the tower to the lower part of the tower is arranged on the vertical direction in the conventional distillation tower, the upper part of one side of which is covered and the other side of which is filled with a catalyst; therefore, the inner space of the reaction bulkhead distillation tower is divided into five regions with different functions. The hydrolyzing and separation device of methyl acetate can fully unleash the advantage of bulkhead tower and reaction distillation, and can cause hydrolysis reaction, product separation and recovery of non reactant to be realized in the same tower. The device provided by the invention and the technique process thereof can obtain the methyl acetate with 60 percent to 99.99 percent hydrolysis rate and products with high purity, restrain side effect effectively, reduce the volume of equipment markedly, simplify process, and reduce energy consumption and operation cost.

The invention relates to a method for recycling metals from a waste catalyst containing molybdenum and nickel, which comprises the following steps of: roasting and smashing the waste catalyst containing the molybdenum and nickel; mixing with an alkaline substance and roasting; leaching by using a mixed acid liquid; depositing by using an alkaline solution, wherein molybdenum is deposited out in the form of ammonium molybdate; further dissolving the ammonium molybdate by using ammonia water; regulating a pH value to obtain ammonium molybdate deposition; and drying to obtain an ammonium molybdate product. The method is particularly suitable for extracting high-purity ammonium molybdate from the aluminum-based waste catalyst containing the molybdenume, and has the advantages of simple process, strong operability, low energy consumption, and stable produced product quality.

The invention discloses salt-spray-resistant and anti-aging water-based paint and a preparation method thereof. The salt-spray-resistant and anti-aging water-based paint is prepared from components in percentage by weight as follows: 40%-60% of a water-based epoxy ester emulsion, 8%-20% of an anti-rust pigment, 1%-5% of a coalescing agent, 4%-20% of filler, 0.5%-2% of a dispersant, 0.5%-2% of a defoaming agent, 0.3%-0.6% of an anti-settling agent, 0.1%-2% of an anti-rust agent, 0.5%-2% of a flash-rust inhibitor, 0.1%-2% of a wetting agent, 0.1%-0.5% of a mildew preventive, 0.1%-2% of a thickening agent, 0.1%-0.3% of a pH conditioning agent and 1%-20% of deionized water. The water-based paint can resist neutral salt spray for 550 H and resist QUV aging for 600 H, has the advantages of high water resistance, good storage stability, contamination resistance, fast drying, safety, environment-friendliness, simple preparation process and the like, is environment-friendly, accords with the environmental protection development trend and is suitable for industrial production.

The invention discloses a high effect formaldehyde dispelling agent. The formaldehyde dispelling agent of the invention comprises formaldehyde dispelling factors, a stabilizing agent, a synergistic agent, surfactants and water, etc. The product is nonpoisonous and tasteless, safe and environmental friendly, which can quickly and thoroughly dispel free formaldehyde in air, waste water and various boards and furniture, and a dense protecting film is formed on the surface of solid, working for a long time. The method of the invention is characterized by simple production technique and devices, no three wastes pollution and low production cost.

The invention provides a preparation method of graphene oxide. The method comprises the following steps: firstly, mixing graphite, an intercalator and an oxidizing agent under an airtight condition and then carrying out a reaction to obtain a reaction mixture; separating the reaction mixture obtained in the previous step to obtain a reaction product; finally, stripping the reaction product, obtained in the previous step, in a dispersing agent to obtain graphene oxide dispersion liquid. According to the preparation method, the intercalator is inserted into the parts among graphene sheet layers under the action of pressure and under the airtight condition, so that the acting force among layers is reduced, and the distances among the layers are increased; then, the oxidizing agent enters the parts among the graphene sheet layers and has an oxidation reaction, so that the graphene oxide is formed; due to the action of the pressure, the intercalator and the oxidizing agent are enabled to enter the parts among graphene layers more rapidly, and the reaction is promoted to be completed within a short time, so that first-order intercalating for the graphite is realized; furthermore, the preparation method is less in energy consumption in a reaction process, environmentally-friendly, convenient and fast to operate as well as safe and controllable, thus being more suitable for industrial mass production.

The invention discloses a preparation method of high-reinforcement modified anhydrous calcium sulfate crystal whiskers. The method comprises the following steps that: firstly, limestone powder is added into stirred water to be prepared into calcium salt aqueous emulsion; then, sulfuric acid and crystal modifiers are sequentially added into the stirred water to be prepared into sulfuric acid water solution; next, the calcium salt aqueous emulsion containing 1 mol part of Ca<2+> is added into the sulfuric acid water solution containing 2 mol parts of SO4<2-> with the temperature reaching 100 to 110 DEG C, then, morphology control agents are added, the materials are subjected to stirring and aging for 2 to 3.5 hours under the temperature condition being 110 to 120 DEG C, leaching and washing are carried out, and calcium sulfate hemihydrate crystal whisker wet products are obtained; the calcination drying finally is carried out under the temperature condition higher than 200 DEG C to obtain the anhydrous calcium sulfate crystal whiskers; and then, the surface modification treatment is carried out to finally obtain the high-reinforcement modified anhydrous calcium sulfate crystal whiskers. The preparation method has the advantages that the product quality is high, the cost is low, the preparation process is short, the reaction condition is mild, and in addition, green and environmental-friendly effects can be realized.

The invention relates to superfine Kaolin calcining process and device, the prodn, method includes; preheating kaolin raw powder material, then putting it in fluidization calcining furnace from the bottom, at same time, sending fuel into the furnace, preheated primary air is sent from plenum under the furnace burns with the fuel and to form a reducibility atmosphere calcining area in the lower section, the volume content of CO+H2 in reduction area is 0-10 percent, secondary air is sent from top of the reduction area to burn residual CO+H2 completely, airflow speed is 1-6m/s in the furnace, raw powder material is in fluidization, kaolin is circularly burned for 0.3-3 hours in temp. 700-1100 deg.C, then is sent into cyclone cooling system to be cooled to obtain superfine kaolin by mixer-grinding and depolymerizing.

The invention discloses a method for preparing crystal II-type ammonium polyphosphate with distribution of high polymerization degree and narrow molecular weight. The method comprises the following steps: putting phosphorus pentoxide and diammonium phosphate which have equal molar ratio into a malaxator which can accurately control a temperature and heated by conducting oil for mixing; under the protection of inert gas, heating the materials in the malaxator to between 100 and 250 DEG C through the circulatory conducting oil; stopping introducing the inert gas; performing ammonification on the materials and heating the materials under an atmosphere of ammonia gas till the materials are totally molten down; stopping introducing the ammonia gas; after homogenization, introducing the ammonia gas again and heating the materials; throwing a surface treating agent into the malaxator; after material throwing is completed, continuously introducing the ammonia gas, keeping warm and mixing the materials; after reaction is finished, transferring the materials to a closed vessel and reducing the temperature; simultaneously, continuously introducing the ammonia gas till the temperature of the materials is below 100 DEG C; and obtaining a finished product. The method can prepare the crystal II -type ammonium polyphosphate with the distribution of the high polymerization degree and the narrow molecular weight; and the product has the characteristics of uniform granularity shape, small water-solubility, good heat resistance, high polymerization degree, narrow distribution of molecular weight and high crystal II-type purity.

The invention provides a steel slag treating method comprising the following steps of: directly mixing thermal-state revolving furnace steel slag with blast furnace slag in an arc furnace in proportion, adjusting the molten slag in the furnace into a proper temperature by virtue of the arcing of the arc furnace, and stirring the molten slag by virtue of arc disturbance, so that acidic oxide and basic oxide in the molten slag are sufficiently reacted with each other; reacting free calcium oxide and free magnesium oxide in the raw steel slag with silicon dioxide component and low-calcium calcium silicate in the blast furnace slag to generate safe calcium silicate and magnesium silicate, quenching the molten slag to form glass-state solid slag which is higher in hydration reactivity and free of short-term or long-term inflation harm, and further finely grinding the solid slag into slag powder which can be safely used for related building material as the blast furnace slag. According to the method, the damage caused by the free calcium oxide and free magnesium oxide in the steel slag can be removed, and a basis is provided for the whole use of the steel slag. The heat energy of the thermal-state molten slag can be sufficiently used, so that the energy source can be saved, the energy consumption can be reduced, the cost can be reduced, and the discharge of CO2 can be reduced, and the method is extremely high in social meaning and economic meaning.

The invention provides a method of degrading dye wastewater by an iron-based amorphous alloy/hydrogen peroxide Fenton-like system. The method is characterized by comprising the following steps: inputting iron-based amorphous alloy ribbon slices and hydrogen peroxide into the dye wastewater; then mixing and stirring, wherein the weight ratio of the dye wastewater and the iron-based amorphous alloy ribbon slices is 100:1, the mass fraction of H2O2 in hydrogen peroxide is 20-30%, and the molar concentration of H2O2 in the dye wastewater is 10-20mmol/L. According to the method of degrading dye wastewater by the iron-based amorphous alloy/hydrogen peroxide Fenton-like system provided by the invention, the dye is initially degraded to Fe<2+> by reducing action of the iron-based amorphous alloy to accelerate growth of OH. free radicals which further oxidize and degrade macromolecules of the dye to micromolecules, and finally, the micromolecules are mineralized to CO2 and H2O. The method is high in degradation rate and thorough in reaction.

The invention discloses a method for harmlessly preparing fertilizer through carcasses. The method comprises the steps that carcass fragments are firstly subjected to heat treatment conversion in an acid environment, the reaction environment is controlled to enable animal fat to be converted into fatty acid, and animal skin, fur and meat are converted into amino acid and humic acid, and animal bones are converted into water-soluble calcium salt and phosphate; the fatty acid is separated, and alkali is added to left amino acid and humic acid mixed liquid for neutralization. Special equipment of the method comprises a carcass crusher, an acidizing reaction kettle, a fatty acid separator and a neutralization reaction kettle which are connected in sequence. The method has the advantages of free of pollution, fast, thorough, efficient, high in quality and the like.

The invention relates to a method for recycling the high purity molybdenum from the molybdenum bearing spent catalyst. The method comprises the steps that the molybdenum bearing spent catalyst is roasted and comminuted, then the molybdenum bearing spent catalyst is leach and filter by adopting alkaline solution bearing ammonia, ammonium bicarbonate and oxyful, and the secondary roasting and leaching are performed to the solids after filtration, the twice leaching solution is acidified and the aluminum is precipitated out, then is acidified continuously to precipitate out the molybdenum in the form of molybdic acid, the molybdic acid is dissolved by using ammonia water further, the pH value is adjusted again to obtain ammonium molybdate deposition, and the ammonium molybdate product is obtained after dryness. The method is particularly suitable for the process for extracting the high purity ammonium molybdate with the aluminum based molybdenum-bearing spent catalyst, the operation is simple, the operability is better, and the quality of the prepared product is stable.