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6999results about How to "Increase reaction rate" patented technology

Device and technique for producing cyclohexane by benzene hydrogenation

The invention discloses a device and technique for producing cyclohexane by benzene hydrogenation. The device for producing cyclohexane by benzene hydrogenation comprises a reactor, a superfine bubble generator and a bubble breaker, wherein the reactor is provided with a first containing cavity; the wall of the first containing cavity is provided with a feed port, a circulation discharge port, a circulation return port and a gas phase outlet; the superfine bubble generator is provided with a second containing cavity; the wall of the second containing cavity is provided with a return port and a gas phase outlet; the return port of the superfine bubble generator communicates with the circulation return port of the reactor; the bubble breaker is arranged in the second containing cavity; the bubble breaker is provided with a gas phase inlet and a liquid phase inlet which communicates with the circulation discharge port of the reactor; and the gas phase inlet of the bubble breaker communicates with the gas phase outlet of the reactor. The device disclosed by the embodiment of the invention has the advantages of high mass transfer efficiency, high reaction rate, short reaction time, low material consumption and energy consumption, simple structure, low manufacturing cost and low maintenance cost.
Owner:NANJING UNIV

Preparation method of dichloro propanol from glycerin

The invention discloses a preparing method of dichlorohydrin from glycerol, which comprises the following steps: adding glycerol and HCl and carboxyl acid activator into mixer; charging into tubular reactor continually to proceed chlorination reaction; reacting through chlorination reaction; transforming glycerol swiftly; entering into HCl bubbling still to react continually; evaporating azeotropic material comprised by water through reaction, dichlorohydrin, HCl and part of activator from the top of bubbling still; recycling product through condensation; separating liquid of bubbling still in the fractionating tower; getting dichlorohydrin from the top of fractionating tower; delivering liquid of fractionating tower to proceed circular response.
Owner:溧阳常大技术转移中心有限公司

Multi-component oxidation micro-electrolytic filler and preparation method thereof

The invention belongs to the technical field of environmental engineering wastewater treatment, and particularly relates to multi-component oxidized micro-electrolysis filler and a preparation method thereof. The multi-component oxidized micro-electrolysis filler is mainly prepared from the following components in percentage by mass: 50-60% of iron, 20-30% of activated carbon, 12-15% of adhesive and 3-5% of catalyst through mixing, wherein iron is iron scrap or iron powder with particle size not more than 80 mesh; and activated carbon is in a powder and has particle size not more than 100 mesh. The preparation method of the multi-component oxidized micro-electrolysis filler comprises uniformly mixing iron, activated carbon, the adhesive and the catalyst according to the ratio, adding water, stirring and aging, then carrying out extrusion molding to obtain molded filler, demolding to obtain a filler blank, after naturally drying, drying, sintering in the absence of air, and cooling thefiller blank to obtain the multi-component oxidized electrolysis filler. According to the invention, the hardening, dead pool, stoppage and other practical problems existing in the use of the traditional micro-electrolysis fillers are solved.
Owner:CHINA COAL TECH & ENG GRP HANGZHOU ENVIRONMENTAL PROTECTION INST

Catalytic module capable of removing formaldehyde at room temperature and preparation method thereof

ActiveCN105289298AImprove catalytic activity and purification efficiencyExcellent low temperature activity and removal efficiencyDispersed particle separationMetal/metal-oxides/metal-hydroxide catalystsChemistryLight source
The invention discloses a catalytic module capable of removing formaldehyde at room temperature and a preparation method thereof. The catalytic module comprises a skeleton carrier, coatings and catalyst layers, the skeleton carrier is a foam ceramic structure with three-dimensional pore channels, and the foam ceramic structure is internally provided with multiple pore channels which are interwoven into a net-shaped structure and arranged in any one of the X direction, the Y direction and the Z direction; the coatings are evenly coated on the surfaces of the pore channels in the foam ceramic structure and the other surface of the foam ceramic structure, and the catalyst layers are highly dispersed on the coatings. By means of the catalytic module capable of removing the formaldehyde at the room temperature and the preparation method thereof, at the room temperature and environment humidity, low-concentration formaldehyde can be oxidized into H2O and CO2, excellent low-temperature activity and removing efficiency are achieved, and the formaldehyde removing efficiency can be kept above 98 percent at the airspeed SV equal to 50,000 h<-1>. The preparation process is simple, the precious metal load is low, and accessory equipment such as light sources and heating are not needed. The catalytic module is suitable for air purification of closed and semi-closed spaces such as living rooms, office buildings, schools, dormitories, shopping malls, furniture markets and automobiles.
Owner:展宗城

Catalyst for normal paraffin hydroisomerization reaction and preparation method as well as application thereof

The invention relates to a catalyst for a normal paraffin hydroisomerization reaction and a preparation method as well as an application thereof. The catalyst has the characteristics that the activity is high in an n-hexane hydroisomerization reaction, and the selectivity and stability are good for a double-branched-chain product. The catalyst comprises modified zeolite molecular sieve ZSM-12 treated by alkaline solution and noble metal of family VIII, wherein the zeolite molecular sieve ZSM-12 adopts zeolite molecular sieve ZSM-12 containing organic amine template. The preparation method of the catalyst comprises the following steps of: desilication of zeolite molecular sieve ZSM-12 containing template after being treated with alkaline solution to obtain zeolite molecular sieve ZSM-12 with high content of mesoporous, and preparing isomerized catalyst by loading Pt. The catalyst is applied in the normal paraffin hydroisomerization reaction, when the catalyst is applied, the n-hexane hydroisomerization reaction is carried out on a fixed bed miniature reactor, the reacting raw material n-hexane is fed into the reactor by a force pump, and is contacted with the catalyst to react in the reactor after being mixed with hydrogen in a mixer.
Owner:ZHEJIANG NORMAL UNIVERSITY

In-situ submarine natural gas hydrate exploiting device and method thereof

The invention relates to an in-situ submarine natural gas hydrate exploiting device and a method thereof, and belongs to the technical field of exploitation of natural gas hydrates. The exploiting device comprises a solar and wind power generating system, a rotary telescopic water gun, an insulating pipeline, a conveying pipeline, a sleeve pipe, an ocean platform, a sea water pump, an electric heater, a CO2 liquid storing tank, a decomposition accelerator storing tank, a high-pressure pump, a pressure gauge, a filtering device, a water storing tank, a gas-liquid separator and a gas recovering device. A thermal activation method and a chemical reagent catalyzing method are utilized to trigger a decomposition reaction of the natural gas hydrate, and then the high-pressure CO2 jetting technology is utilized to enable the natural gas hydrate to be cut while a substitution reaction occurs. According to the invention, the natural gas hydrate is exploited by fully utilizing rich solar power and wind power in ocean areas, so that the effects of cleaning and environmental protection are realized; the thermal activation method and the chemical reagent catalyzing method are matched with the CO2 substitution method, and therefore the exploitation rate is improved, the dosage of a chemical reagent is reduced, the stability of submarine geology is protected effectively, and meanwhile the greenhouse gas is treated to a certain extent.
Owner:SHANGHAI JIAO TONG UNIV

Method for producing cellulose ester acetate by using plant cellulose

This invention relates to a method for preparing cellulose ester acetate from plant cellulose in ionic liquid. The method comprises: (1) utilizing plant cellulose as the raw material; (2) dissolving plant cellulose in ionic liquid; (3) adding acylation agent into the ionic liquid, performing homogeneous acetylation on plant cellulose, washing the intermediate with water and drying; (4) separating and purifying dried intermediate to obtain cellulose ester acetate. This invention provides a method for homogeneously preparing cellulose ester acetate in clean solvent (ionic liquid) by using low quality plant cellulose as the raw material. The method solves the problem of high cost faced by the present methods.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI +1

Three-dimensional interconnected hierarchical-structured zeolite molecular sieve material and preparation method thereof

The invention belongs to the technical field of mesoporous composite materials, and particularly relates to a three-dimensional interconnected hierarchical-structured zeolite molecular sieve material and a preparation method thereof. The method comprises the following steps of: self-assembling anionic and cationic surfactants, serving as primary constitutional units, in solution phase to form a secondary constitutional unit; self-assembling in solution to be compounded into amphipathic block copolymer; then, self-assembling in the solution by taking the amphipathic block copolymer as a template agent and by using a structural guide agent and inorganic silicon to obtain a silicon dioxide/surfactant/template agent composite material; and finally, calcining to remove the surfactant and the template agent to obtain the hierarchical-structured mesoporous zeolite molecular sieve material consisting of interconnected mesopores, micropores and macropores. The material has higher specific surface area and stronger hydrothermal stability, and has a broad application prospect in the aspects of petrochemical industry, heavy oil catalysis cracking, biological separation, adsorption and the like. The material obtained in the invention has the advantages of superior performance, simple synthesis method and readily available raw material and is suitable for industrial production.
Owner:FUDAN UNIV

Assay kit for neutrophil gelatinase-associated lipocalin

The invention relates to an assay kit for neutrophil gelatinase-associated lipocalin (NGAL), in particular to an assay kit for detecting the concentration of the NGAL in human body fluids and a preparation method for the assay kit. The kit comprises a reagent R1, a reagent R2 and a working calibrator, wherein the reagent R1 is a buffer solution which is suitable for antigen-antibody reaction; and the reagent R2 is a solution simultaneously containing nanospheres which have two particle sizes and are combined with an anti-human NGAL antibody, and ensures that the nanospheres are coagulated to cause the change of the turbidity through antigen-antibody specific reaction, and the NGAL can be quantificationally determined by contrasting calibration curves. The kit has relatively high sensitivity when determining low NGAL concentration and has a relatively wide linear range when determining high NGAL concentration, so a prozone phenomenon is avoided. The kit has stable physical and chemical properties, is convenient to use, and has a broad application prospect in clinical laboratory science.
Owner:BEIJING STRONG BIOTECH

Calcium carbide production method

The invention relates to a carbide preparation method belonging to the field of carbide preparation. The conventional carbide preparation technology adopts block materials and electric arc as a heat-supply, while the preparation method according to the invention adopts powdery carbon-containing materials and powdery calcium-containing materials, and the combustion of partial carbon-containing materials and oxygen-containing gas as a heat-supply at 1700-2300 DEG C to prepare carbide, wherein the carbon-containing materials is coal or coke, calcium-containing materials is calcium carbonate, calcium oxide, calcium hydroxide or carbide slag, the granularity of the carbon-containing materials and calcium-containing materials is less than 1mm, and the quality ratio is 0.5-3:1. The oxygen-containing gas for combustion is oxygen, oxygen-enriched air or air. The method solves the problems of high energy consumption and high pollution of the carbide preparation and has advantages of wide choice scope of materials, high energy utilization rate, continuous operation and large production capacity. The technology also couples with the process of carbon-containing materials coking and calcium-containing materials calcining, preheats the materials to 500-1500 DEG C utilizing the combustion of by-products CO of the carbide preparation and the assistant fuel, thereby further reducing the oxygen and energy consumption of the carbide preparation.
Owner:BEIJING UNIV OF CHEM TECH

Preparation method of loading iron based metal organic skeleton out phase Fenton catalyst and application thereof

The invention relates to a preparation method of a loading iron based metal organic skeleton out-phase Fenton catalyst and an application thereof. The preparation method comprises the following steps of by taking MIL-100 (Fe) as a basal body, loading a ferrous component through a hydrothermal method so as to obtain the loading iron based metal organic skeleton out-phase Fenton catalyst, namely Fell@ MIL-100 (Fe). The catalyst is used for degrading an organic pollutant in waste water by using an out-phase Fenton catalyst system. Compared with the prior art, the loading catalyst prepared by the invention fully utilizes the advantages of MIL-100 (Fe) and a ferrous component in an out-phase Fenton reaction, so that the loading catalyst has high porosity, large specific surface area, and is stable in a water phase, catalytic activity sites are uniformly dispersed, the capacity is controllable and the like, meanwhile, the mutual circulation action of the Fe<2+> component in a carrier and a Fe<3+> in the basal body are utilized to further strengthen the Fenton reaction activity, the catalyst is suitable for removing refractory organics in waste water by catalytic oxidation of out-phase Fenton, the operation of the technology is simple, the cost is low, the preparation method is an efficient and energy-saving new technology, and the catalyst has the far-reaching application prospect and wide social and economic benefits.
Owner:TONGJI UNIV

Microbiological fuel cell device and battery and use and water treatment system

A microorganism fuel cell device comprises an outer cover(1) of the fuel cell, an anode chamber(3), an anode(13), a cathode chamber(4), a cathode(16) and a septum(17). Wherein, the anode(13) is positioned inside the anode chamber(3); the septum(17) is positioned between the anode chamber(30) and the cathode chamber(4). The cathode(16) is a slice-shaped cathode, one surface of the slice-shaped cathode and one surface of septum(17) are jointed to form a septum cathode component(10); the surface of slice-shaped cathode not jointing with the septum(17) is positioned at one side of the cathode chamber(4). As the disclosed microorganism fuel cell device forms the septum cathode component by jointing the slice-shaped cathode with the septum, the invention further improves the moving efficiency of the media and also speeds up the cathode reaction, so that the overall reacting speed of the microorganism fuel cell for the device is greatly improved. Therefore, the invention can realize the large scaled successive disposal of the waste water.
Owner:BYD CO LTD
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