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44results about How to "Not hydrolyzed" patented technology

Formula of soles of PU-simulated foaming sneakers through injection and manufacturing method

The invention relates to a formula of soles of PU-simulated foaming sneakers through injection, which comprises the following raw materials in percentage by mass: 40 percent of 21 percent ethylene-vinyl acetate copolymer (EVA 7360), 16.7 percent of styrene butadiene copolymer SBBSJT-83, 12.5 percent of ethylene octylene copolymer POE8130, 8.3 percent of ethylene-propylene-diene copolymer 3745P, 65.9 percent of wear-resisting agent A-18, 8.3 percent of talcpowder, 0.25 percent of stearic acid, 0.42 percent of zinc stearate, 0.9 percent of zinc oxide, 0.08 percent of bridging auxiliary agent ET-102, 0.75 percent of bridging agent DCP, 1.7 percent of high-temperature foaming agent AC-6000H, 2.5 percent of titanium white powder R-103 and 1.7 percent of master batch. The preparation method comprises the steps of banburying, mixing, granulation, injection molding, physical property tests and the like. Thus, in the research and development and application, the PU-simulated foaming soles not only have the physical and chemical properties of no crease marks, high elasticity, low compression and wear resistance of PU soles, and but also have the advantages of low production cost, light specific gravity, good limited-slip properties, no hydrolysis and long service life.
Owner:泰亚投资集团有限公司

Method for extracting chitin from shrimp and crab shells

The invention discloses a method for extracting chitin from shrimp and crab shells. The method comprises the following steps: raw material treatment, ultrasonic treatment, high-pressure treatment, acid treatment, and drying to obtain the product. Compared with the existing acid and alkali treatment, microbiological treatment and the like, the method has the advantages that the time is greatly shortened, and the obtained chitin is high in yield and high in content.
Owner:江苏盐城盐都现代农业产业园发展有限公司

Method for preparing chemically crosslinked photonic crystal hydrogel with adjustable color

The invention relates to a method for preparing chemically crosslinked photonic crystal hydrogel with an adjustable color. The method comprises the following steps: (1) dissolving N-isopropylacrylamide, N-hydroxyethyl acrylamide, a cross-linking agent and an emulsifier into deionized water, stirring, warming and keeping warm under the condition at 20-25 DEG C in a nitrogen condition, and then adding an initiator to continue to react for 1-4 hours, and dialyzing, so as to obtain a colloidal crystal hydrogel solution; (2) concentrating the obtained colloidal crystal hydrogel solution, standing at room temperature, adjusting the pH by adopting an NaOH solution, adding a crosslinking agent, evenly mixing, centrifuging, and standing at room temperature after taking, so as to obtain the chemically crosslinked photonic crystal hydrogel. The method is simple in process and low in cost, and the prepared photonic crystal hydrogel has thermosensibility. In addition, the obtained photonic crystal hydrogel is good in stability, and free of hydrolysis, the problem that nano hydrogel is easily decomposed because of ester hydrolysis in 2-hydroxy ethyl acrylate is solved, and the defects of the photonic crystal hydrogel in application are compensated.
Owner:DONGHUA UNIV

Grafted polymer microspheres for oil displacement modification and preparation method thereof

The invention relates to a profile modifying / water plugging agent for an oil well, in particular to grafted polymer microspheres for oil displacement modification and a preparation method thereof. The grafted polymer microspheres are prepared from etherified starch, acrylamide, N,N-methylene bisacrylamide and ammonium persulfate in the mass ratio of (1-2) to (0.5-1.5) to (0.04-0.2) to (0.1-0.5). The polymer microspheres have the advantages of controllable particle size, high homogeneity, high temperature resistance, high salt resistance, wide raw material source and low manufacturing cost, is not hydrolyzed in a severe saline environment, and is non-degradable; starch microspheres can further go deep into an oil reservoir after being swelled by absorbing water; meanwhile, the polymer microspheres have the rigid characteristic of starch micro molecules and the flexible changeability characteristic of the acrylamide, have high deepening and blocking performance, and are environmentally friendly; by adopting the grafted polymer microspheres, the non-homogeneity of a rock stratum is lowered, and the crude oil recovery factor is increased.
Owner:CNPC GREATWALL DRILLING ENG

Hydrolysis-resistant corrosion-resistant polyurethane synthetic leather

ActiveCN110041498AMake up for water resistanceMake up for the shortcomings of insufficient solvent resistanceTextiles and paperCarbon nanotubeHydrosilylation
The invention discloses hydrolysis-resistant corrosion-resistant polyurethane synthetic leather, which is obtained by infiltrating a modified polyurethane emulsion into a non-woven fabric by a wet manufacturing process; specifically, firstly 2-butene-1,4-diol and heptamethyltrisiloxane are used for a hydrosilylation addition reaction to obtain a silanol compound with the structure shown as the formula A; next, isophorone diisocyanate, polypropylene glycol and the silanol compound A are subjected to block copolymerization to obtain a prepolymer with the structure shown as the formula B; under the action of a chain extender DMPA, further polymerization is performed to obtain a condensate C; organosilicone with low surface energy is embedded in the synthesis of polyurethane; then a carboxylated carbon nanotube is introduced by a hydrogen bonding mode to form a superhydrophobic protective layer, so that the hydrolysis resistance and corrosion resistance of the polyurethane synthetic leather are greatly improved, thereby realizing good application prospects.
Owner:福鼎利都超纤皮革有限公司

Preparation method of triallyl isocyanurate

The invention relates to the synthesis field of triallyl isocyanurate, and specifically provides a method for preparing triallyl isocyanurate by using a catalytic system. The isocyanurate and a catalyst are added into solvent. Chloropropene is dropwise added under the temperature of 70-105 DEG C for reaction. After reacting for 4-8 hours, the reactant is cooled to room temperature and filtered to remove solid phases. The filtrate subjected to solvent recovery is distilled under 113-115 DEG C / 133.3Pa to obtain the triallyl isocyanurate product, wherein the catalyst is the catalytic system of a copper catalyst and a phase transfer catalyst. According to the invention, a solvent method is adopted, and no water is brought in the reaction solution, so that the raw material chloropropene cannot be hydrolysized, the excessive chloropropene can be recycled at the end of the reaction, and the triallyl isocyanurate product obtained by the reaction has good quality.
Owner:江苏科利新材料有限公司

Synthesis method of siloxane-substituted maleimide

InactiveCN104447849AOvercome cumbersomeOvercome the disadvantages of siloxane hydrolysis easily caused by the dehydration processGroup 4/14 element organic compoundsGlass fiberImide
The invention belongs to the field of synthesis of polymer monomers, and specifically relates to a synthesis method of siloxane-substituted maleimide which can be used as an active coupling agent of glass fibers for greatly improving the combination force of the glass fibers and organic resins. The traditional manufacturing method of such coupling agent is a two-step method and comprises the steps of enabling amino alkyl siloxane and maleic anhydride to react to generate maleamic acid alkyl siloxane; synthesizing the siloxane-substituted maleimide through amic acid under the effect of a dehydrating agent. The invention provides a novel synthesis method for preparing a target product through raw materials that are alkali metal salt of maleimide and halogen alkyl siloxane by an one-step mode in the presence of a polar aprotic solvent, aims at overcoming the shortages that the traditional synthesis method is cockamamie in process and the dehydrating easily leads to hydrolyzing of siloxane. The method, by being compared with the traditional synthesis method, has the advantages that the after-treatment is convenient, the siloxane is avoided electrolyzing, and the product is high in purity.
Owner:SHANGHAI AIMO JINSHAN PHARM CO LTD

Pretreatment method for chemical industry wastewater

The invention relates to a pretreatment method for chemical industry wastewater with high salt, high ammonia nitrogen, high organic solvent and high toxicity. According to the technical scheme, the chemical industry wastewater is subjected to coagulating reaction sedimentation treatment, microelectrolysis reaction treatment, Fenton reaction treatment and MVR evaporation treatment in sequence. By means of the pretreatment method, the content of fine suspended matter and low-boiling-point organic matter in the chemical industry wastewater can be effectively reduced, the phenomenon that foam is formed in the operation process of an MVR evaporator is reduced, and thus normal operation of the MVR evaporator is guaranteed; as the chemical industry wastewater is subjected to microelectrolysis reaction treatment and Fenton reaction treatment, organic nitrogen can be converted into ammonia nitrogen before the chemical industry wastewater is subjected to MVR evaporation treatment, the existing form of nitrogen in the wastewater is controlled, most ammonia nitrogen is crystallized out of the system in the form of ammonium chloride, and thus the ammonia nitrogen load in subsequent condensate biochemical treatment is reduced. Compared with a conventional treatment process, the pretreatment method has an unexpected treatment effect on the chemical industry wastewater, and the operation stability of the whole system is guaranteed.
Owner:安徽南风环境工程技术有限公司

Non-ionic emulsifier, epoxy emulsion, preparation method and application thereof

The invention provides a non-ionic epoxy resin emulsifier. The emulsifier has a structure shown as formula ER-1 or ER-2. The invention also provides a preparation method for the non-ionic epoxy resinemulsifier. The invention provides a non-ionic epoxy emulsion, the preparation method and application thereof. The non-ionic epoxy emulsion provided by the invention has small diameter and high stability. A test in the manner of centrifugal separation for 30 minutes at 10000rpm proves that no layering bleeding phenomenon occurs, the change on grain size and epoxide equivalent is small and the protecting property for metal welding area is excellent after the non-ionic epoxy emulsion is stored for 6 months under room temperature.
Owner:BAUHINIA PAINTS SHANGHAI CO LTD

Xanthate cation dual-modified straw fiber printing and dyeing wastewater treatment agent and preparation method thereof

The invention relates to a xanthate cation dual-modified straw fiber printing and dyeing wastewater treatment agent which is prepared by extracting straw fiber by taking straw as a raw material, and sequentially modifying the straw fiber by using an anion esterifying agent and a cationic etherifying agent, wherein the anion esterifying agent is carbon disulfide; the cationic etherifying agent is 3-chlorine-2-hydroxypropyl trimethylammonium chloride. In addition to an excellent decoloration effect, the dual-modified straw fiber in the xanthate cation dual-modified straw fiber printing and dyeing wastewater treatment agent is hard to decompose in a water body, relatively good in water solubility resistance, hard to gelatinize even at 60 DEG C, applicable to certain acid-base environments, hard to hydrolyze and good in stability.
Owner:JIANGYIN POLYTECHNIC COLLEGE

High-hydrolysis-resistant back-adhesion-resistant adhesive used for aluminum plastic composite tag and preparation of adhesive

The invention discloses a high-hydrolysis-resistance anti-sticking backing adhesive used for an aluminum plastic composite tag and preparation of the adhesive. The adhesive comprises a component A anda component B, wherein the component A comprises polyester polyol, modified epoxide resin, hydroxy acrylic resin, a chain extender, a catalyst and a solvent; and the component B comprises an initiator and an isocyanate curing agent. The adhesive disclosed by the invention is particularly applicable to the adhesion of an aluminum foil or an aluminum coating and a PET thin film; the adhesive is high in adhesive strength to an aluminum plastic composite material and has good acid and alkaline resistance and damp-heat aging resistance, and high back adhesion resistance exists between adhesive layers and between an adhesive layer and aluminum respectively when the adhesive disclosed by the invention is applied; and after an etching technology of the aluminum plastic composite tag, the tag cannot be destroyed by back adhesion even if unrolling or rolling.
Owner:SHANGHAI WEIKAI CHEM +2

Measurement method of total saponins in health food using propolis as raw material

The invention relates to a measurement method of total saponins in health food, and particularly relates to a measurement method of total saponins in health food using propolis as a raw material. The measurement method provided by the invention comprises a standard curve making process, a sample treatment process, a test liquid column chromatography isolation process, a color developing process and a total saponins calculating process. In the standard curve making process, a standard curve is obtained by using an absorbance value and a mass of ginsenoside as curves; in the sample treatment process, liquid to be tested is obtained by taking 0.3g of the health food using the propolis as the raw material; in the test liquid column chromatography isolation process, column chromatography isolation is carried out on the liquid to be tested by using a chromatographic column, so as to obtain an evaporation pan with the liquid to be tested which is evaporated to be dry; in the color developing process, the absorbance value of the liquid to be tested is obtained; and in the total saponins calculating process, the content of the total saponins in the health food using the propolis as the raw material can be obtained. The measurement method provided by the invention has the advantages of simple extraction method, high recovery rate, good accuracy, simplicity, convenience and rapidness.
Owner:杭州蜂之语蜂业股份有限公司

Low-carbon, environment-friendly, economical and reasonable water treatment process flow and method for water treatment plant

The invention discloses a low-carbon, environment-friendly, economical and reasonable water treatment process flow and method for a water treatment plant, and belongs to the fields of water resource reasonable utilization technology and environmental protection. The water treatment process flow and method comprises the following steps of: adding a coagulant; adding a disinfectant; purifying water; and utilizing and treating wastewater. The invention has the advantages that: problems of the conventional process are solved; and the water treatment process and method for the water treatment plant is low-carbon, environment-friendly, economical, reasonable, stable and reliable in operation and convenient to manage and maintain, ensures water treatment effect to reduce project investment and daily operating cost.
Owner:姚家泰

Composite water-treatment coagulant prepared from high-iron gibbsite and preparation method thereof

The invention discloses a composite water-treatment coagulant prepared from high-iron gibbsite and a preparation method thereof. The composite water-treatment coagulant is an aluminum chloride molten iron treatment coagulant, aluminum sulfate molten iron treatment coagulant or polyaluminum chloride molten iron treatment coagulant, which is respectively prepared from high-iron gibbsite, technical hydrochloric acid and water, or high-iron gibbsite, technical hydrochloric acid, water and calcium aluminate powder, or high-iron gibbsite, commercial sulfuric acid and water. The invention also discloses a preparation method of the composite water-treatment coagulant prepared from high-iron gibbsite. The composite water-treatment coagulant has the advantages of wide raw material sources, high iron content, high stability, wide water treatment range, favorable turbidity removal effect, simple preparation method, no need of roasting in the production process, no wastewater or waste gas emission and no environmental pollution.
Owner:付春平

Adriamycin nanoparticle with particle size controllable and preparation method thereof

The invention provides an adriamycin nanoparticle with the particle size controllable. The adriamycin nanoparticle is formed by taking polyethylene glycol vitamin E succinate (TPGS) as a core and wrapping the core with polyethylene glycol-adriamycin and poly(isobutene-alt-maleic anhydride)-modified beta-cyclodextrin through self-assembly. The invention further provides a preparation method of the adriamycin nanoparticle. Compared with a traditional nanoparticle prepared through a chemical bond forming and rupturing method, the adriamycin nanoparticle is controllable in particle size, simple in preparation process, mild in reaction condition and capable of easily obtaining the raw materials and has the good biological safety and tissue compatibility.
Owner:INST OF HIGH ENERGY PHYSICS CHINESE ACADEMY OF SCI

Medical cold compress paste

The invention provides a medical cold compress paste. The medical cold compress paste comprises a front face layer and a back lining layer, wherein the front face layer is used for cooling, and mainlyprepared from a cooling substance raw material, and the cooling substance raw material is prepared from, by mass, 50-100 parts of purified water, 20-50 parts of a humectant and 30-60 parts of a thickening agent; the back lining layer is prepared from a non-woven fabric and a polyethylene film, and the non-woven fabric and the polyethylene film are bonded to form the back lining layer; the front face layer is applied on the back lining layer. Further, the cooling substance raw material comprises 10-20 parts of carrageenan. The medical cold compress paste has the advantages that the medical cold compress paste can perform physical pyretolysis, cold compress physiotherapy and specific body surface part cooling to improve the cooling effect, and the preparation of the medical cold compress paste is convenient and low in production cost. The medical cold compress paste also has a good cooling effect on the physical pyretolysis of closed soft tissue of the human body.
Owner:广州赛美药业有限公司

Formula of soles of PU-simulated foaming sneakers through injection and manufacturing method

The invention relates to a formula of soles of PU-simulated foaming sneakers through injection, which comprises the following raw materials in percentage by mass: 40 percent of 21 percent ethylene-vinyl acetate copolymer (EVA 7360), 16.7 percent of styrene butadiene copolymer SBBSJT-83, 12.5 percent of ethylene octylene copolymer POE8130, 8.3 percent of ethylene-propylene-diene copolymer 3745P, 65.9 percent of wear-resisting agent A-18, 8.3 percent of talcpowder, 0.25 percent of stearic acid, 0.42 percent of zinc stearate, 0.9 percent of zinc oxide, 0.08 percent of bridging auxiliary agent ET-102, 0.75 percent of bridging agent DCP, 1.7 percent of high-temperature foaming agent AC-6000H, 2.5 percent of titanium white powder R-103 and 1.7 percent of master batch. The preparation method comprises the steps of banburying, mixing, granulation, injection molding, physical property tests and the like. Thus, in the research and development and application, the PU-simulated foaming soles not only have the physical and chemical properties of no crease marks, high elasticity, low compression and wear resistance of PU soles, and but also have the advantages of low production cost, light specific gravity, good limited-slip properties, no hydrolysis and long service life.
Owner:泰亚投资集团有限公司

Resin composition, prepreg, circuit board and printed circuit board

The invention relates to a resin composition, a prepreg, a circuit board and a printed circuit board. The resin composition comprises carbon-carbon conjugated group-terminated polyphenyl ether resin, carbon-carbon double bond-containing hydrocarbon resin, a polysiloxane curing agent and a solvent, wherein the structure of the polysiloxane curing agent is shown as a formula (I), in the formula (I), m is an integer of 1-20, R1 is a first alkyl group with a carbon chain length of 1-12, R2 is hydrogen or a second alkyl group with a carbon chain length of 1-12, and at least one of R1 or R2 contains an alkenyl active functional group. The polysiloxane curing agent in the resin composition is not easy to volatilize, so that the stable performance of circuit substrates prepared in different batches can be ensured; moreover, the polysiloxane curing agent does not contain hydrophilic groups and cannot be hydrolyzed, so that in the use process of the circuit substrate, the hygroscopicity of the circuit substrate can be effectively reduced, and the dielectric property of the circuit substrate can be prevented from being degraded due to moisture absorption.
Owner:ZHEJIANG WAZAM NEW MATERIAL CO LTD +2

Hemostatic film formula hydrolyzed at high temperature

The invention relates to a hemostatic film formula hydrolyzed at a high temperature. The formula comprises 60-100 parts of polyvinyl alcohol, 5-10 parts of polyethersulfone, 0.5-1 part of ethyl p-hydroxybenzoate, 2-8 parts of betaine polysulfonate, 0.1-0.3 part of ammonium carbonate and 15 parts of dibasic lead stearate 0.5nu. The formula is not hydrolyzed at the room temperature but hydrolyzed atthe temperature of more than 45 DEG C. Hydrolyzed products are harmless to the environment, the formula is simple, the production cost is low, and environment protection and safety are achieved.
Owner:方季群

Organosilicon high boiling mixed liquid directional transformation system

The invention discloses a directional conversion system for organosilicon high-boiling mixed liquid, which comprises a directional oxidation conversion device, a high-temperature oxidation chamber, an oxygen-supplementing air heat exchanger, a high-temperature too-cotton catcher, a waste heat recovery device, and a quenching hydrochloric acid absorption tower arranged in sequence , Hydrogen chloride absorption tower first / secondary, chlorine oxidation tower, alkali washing tower, smoke exhaust fan, activated carbon filter, exhaust pipe. The invention adopts directional oxidation conversion device, high-temperature oxidation chamber, oxygen-supplementing air heat exchanger, high-temperature too-cotton trap, waste heat recovery device, quenching hydrochloric acid absorption tower, hydrogen chloride absorption tower first / secondary, chlorine oxidation tower, alkali washing tower, etc. Gradually carry out directional transformation and treatment of organosilicon high-boiling mixed liquid. The separated silica, hydrochloric acid and other products are all qualified industrial products and can be used industrially. All are advanced, reliable, economical and reasonable, can effectively reduce operating costs, and realize material recycling and energy recovery.
Owner:JIANGSU JINNIU ENVIRONMENTAL ENG EQUIP

An after-treatment fluid for copper surface black oxidation

This invention relates to a kind of processing solution for copper black oxidation. It discloses the water-soluble reducer in the processing solution is tertiary-butyl alkyl borane, trimethyl alkyl borane, ethanol hydrazine or the combination of above compounds. This invention has many water-soluble reducer selections, can reduce the aerugo to copper effectively. The reducer is cheap and will not be hydrolysis. The reduced by-product is water-soluble, will not generate grain on the inner copper. It is good for the adherence of copper and semi-solidified piece.
Owner:GUANGDONG TONESET SCI & TECH

Measurement method of total saponins in health food using propolis as raw material

The invention relates to a measurement method of total saponins in health food, and particularly relates to a measurement method of total saponins in health food using propolis as a raw material. The measurement method provided by the invention comprises a standard curve making process, a sample treatment process, a test liquid column chromatography isolation process, a color developing process and a total saponins calculating process. In the standard curve making process, a standard curve is obtained by using an absorbance value and a mass of ginsenoside as curves; in the sample treatment process, liquid to be tested is obtained by taking 0.3g of the health food using the propolis as the raw material; in the test liquid column chromatography isolation process, column chromatography isolation is carried out on the liquid to be tested by using a chromatographic column, so as to obtain an evaporation pan with the liquid to be tested which is evaporated to be dry; in the color developing process, the absorbance value of the liquid to be tested is obtained; and in the total saponins calculating process, the content of the total saponins in the health food using the propolis as the raw material can be obtained. The measurement method provided by the invention has the advantages of simple extraction method, high recovery rate, good accuracy, simplicity, convenience and rapidness.
Owner:杭州蜂之语蜂业股份有限公司

Digestion method and detection method of vanadium-nitrogen-titanium-iron mixed alloy cored wire

The invention provides a digestion method and a detection method for a vanadium-nitrogen-titanium-iron mixed alloy cored wire. The digestion method comprises the following steps: putting a cored wire into a container, adding a concentrated nitric acid and a concentrated hydrochloric acid to the container; carrying out first time of pre-reaction under an open state; adding a concentrated sulfuric acid and carrying out second time of pre-treatment under the open state; carrying out digestion and complexation reaction by microwave in a closed state, so as to obtain a solution. The detection method comprises the following steps: cooling the solution, diluting and fixing volume to obtain a sample solution; determining the content of elementary compositions in one or more sample solutions by using inductively coupled plasma atomic emission spectrometry, flame atomic absorption spectrometry, titration, spectrophotometry and an electrochemical process. The digestion method and the detection method have the advantages of being safe to operate, simple and rapid, efficient and complete, fewer in man-made factors, and easy to accurately control and repeatedly reappear, and technical indexes such as the accuracy, the precision and the like of an analysis result are improved.
Owner:PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP

Fast leaching method for copper-cobalt alloy

The invention discloses a fast leaching method for a copper-cobalt alloy. The fast leaching method for the copper-cobalt alloy comprises the following steps of (1) preparing a sulfuric acid solution with the concentration being 1 to 6mol / L, and adding ferric sulfate into the sulfuric acid solution until the ferric ion concentration reaches to 25 to 40g / L; (2) adding copper-cobalt alloy powder withthe diameter being 50 to 200mum into a mixed solution in the step (1) according to the liquid-solid ratio being 10 to 15:1, stirring and reacting; (3) when the concentration of Fe3+ in a solution tobe reacted is lower than 8g / L, stopping stirring, standing, guiding the solution separated after standing out into the other container, feeding oxygen into the guided-out solution until the concentration of Fe3+ in the solution reaches to 20 to 25g / l, re-pouring, and then continuously stirring; and (4) repeating the step (3) until the alloy is completely leached. Compared with a traditional technology, the fast leaching method for the copper-cobalt alloy provided by the invention is simple in process, fast in leaching speed, low in cost and free of pollution.
Owner:ZHEJIANG IND & TRADE VACATIONAL COLLEGE
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