Method for extracting chitin from shrimp and crab shells
A technology of chitin and shrimp and crab shells, which is applied in the field of extracting chitin from shrimp and crab shells, can solve the problems of long time and achieve the effects of shortened process time, mature process and mild reaction conditions
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Embodiment 1
[0021] A method for extracting chitin from shrimp and crab shells, comprising the steps of:
[0022] a. Raw material processing: wash 10kg of shrimp head with pure water and mince it;
[0023] b. Ultrasonic treatment: add 10 times the weight of pure water to the crushed raw materials, ultrasonic treatment for 10 minutes, the operating temperature is 25 ° C, and the power is 300 W. After completion, filter and collect the filter residue;
[0024] c. High-pressure treatment: add purified water to the filter residue obtained in step b, maintain high pressure at 121°C for 40 minutes, filter, and collect the filter residue;
[0025] d. Acid treatment: add 1.0 mol / L hydrochloric acid solution equivalent to the same quality of the filter residue to the filter residue obtained in step c, soak for 1 h, wash with water until neutral, centrifuge, and freeze-dry to obtain 1.82 kg of chitin with a content of 98.5%.
Embodiment 2
[0027] A method for extracting chitin from shrimp and crab shells, comprising the steps of:
[0028] a. Raw material processing: wash 10kg of crab shells with pure water and grind them;
[0029] b. Ultrasonic treatment: Add 20 times the weight of pure water to the minced raw materials, ultrasonic treatment for 20 minutes, the action temperature is 45 ° C, and the power is 200 W. After completion, filter and collect the filter residue;
[0030] c. High-pressure treatment: add purified water to the filter residue obtained in step b, maintain high pressure at 121°C for 20 minutes, filter, and collect the filter residue;
[0031] d. Acid treatment: add 3.0 mol / L hydrochloric acid solution equivalent to 3 times the mass of the filter residue to the filter residue obtained in step c, soak for 1 h, wash with water until neutral, centrifuge, and freeze-dry to obtain 1.93 kg of chitin with a content of 98.6%.
Embodiment 3
[0033] A method for extracting chitin from shrimp and crab shells, comprising the steps of:
[0034] a. Raw material processing: Wash 10kg of shrimp heads and crab shells with pure water and mince them;
[0035] b. Ultrasonic treatment: add 15 times the weight of pure water to the crushed raw materials, ultrasonic treatment for 15 minutes, the action temperature is 30 ° C, and the power is 250 W. After completion, filter and collect the filter residue;
[0036] c. High-pressure treatment: add purified water to the filter residue obtained in step b, maintain high pressure at 115°C for 30 minutes, filter, and collect the filter residue;
[0037] d. Acid treatment: add 3.0 mol / L hydrochloric acid solution equivalent to twice the mass of the filter residue to the filter residue obtained in step c, soak for 1 h, wash with water until neutral, centrifuge, and freeze-dry to obtain 1.88 kg of chitin with a content of 99.1%.
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