The invention provides a
fly ash low-temperature wet activating treatment method, comprising the following steps of: (1) mixing the
fly ash with the strong alkali solution of which the concentration is 300-700g / l, to perform activating treatment, wherein the volume-to-
mass ratio of the alkali solution and the
fly ash is (3:1)-(20:1) (ml / g), the activating temperature is 130-180 DEG C, the activating time is 0.5-10 hours, and the activating pressure is normal pressure to 0.5Mpa; performing liquid-
solid separation after activation to get the crude alkali liquor and the activated fly ash; (2) diluting the crude alkali liquor, then, adding
calcium oxide into the diluted crude alkali liquor for purification, performing liquid-
solid separation to get
calcareous residues and strong alkali solution, wherein the
calcareous residues is output to the
system as byproducts, and the strong alkali solution is recycled for fly ash activating treatment. In the method, the alkali solution is NaOH water solution, KOH water solution,
sodium aluminate solution or
potassium aluminate solution, after being activated, the fly ash is dissolved out by diluted acid, and the
dissolution rate of aluminum
oxide is up to 95-99%. In the method, the
activation temperature is low, the activation effect is excellent, the activation process cannot cause secondary
pollution, and essential conditions for follow-up fly ash treatment, especially for extraction of aluminum
oxide,
zeolite preparation, and the like, are created.