3908 results about "Hydration reaction" patented technology

Silicone hydrogels formed from a hydrated polymerization product of a monomer mixture comprising (a) a major amount of a non-silicone-containing hydrophilic monomer; and (b) a minor amount of a silicone-containing monomer, wherein the hydrogel has a water content of greater than 50 weight percent are disclosed.

An integrated process is described for producing biodiesel from oleaginous seeds, preferably castor bean seeds. The inventive process includes a transesterification reaction where the seeds themselves react with anhydrous ethyl alcohol in the presence of an alkaline catalyst. The resulting ethyl esters are then separated by decantation and neutralized and used as fuel for diesel engines, co-solvents for diesel and gasoline mixtures with anhydrous or hydrated ethyl alcohol. The solid fractions may be used as fertilizers, for feeding cattle and as a raw material for producing ethyl alcohol.

This invention relates to an entirely new technology of completely recovering chromium and vanadium from vanadium-chromium miscible liquid. The main procedures include: first a primary-secondary compound amine extracting agent contacts the vanadium-chromium miscible liquid by means of countercurrent contact and extract, so as to extract most of vanadium and a small amount of chromium into a organic phase while most of chromium stays into a aqueous phase; and a reduction reaction is conducted with pH of acid adjustable faffinate (aqueous phase) and a certain amount of a reducing agent; the sodium hydroxide is used for adjusting pH value of the solution and filter, and finally the product is hydrous chromium oxide; at that time, the lye is used as a stripping agent; the vanadium is stripped from the vanadium-rich organic phase into water in the manner of countercurrent contact; and the vanadium is separated from the solution witthe method of ammonium precipitation and in the form of ammonium metavanadate; and finally the supernatant clear solution of the one is processed with deposited vanadium with a high-efficient distillation technology, and the strong aqua ammonia is left in the tower top and deamidization solution is left in the tower bottom until the extraction process is reached. The invention uses the primary-secondary compound amine as the extracting agent, extracts and separates vanadium and chromium selectively at a low temperature. The invention not only has a simple process flow, but also is low-cost, quite applicable in large-scale industrial production. In addition, the invention also provides high-purity ammonium metavanadate and 16 percentage strong aqua ammonia, and makes sure the vanadium and chromium can be completely recovered through re-use of the solution.

Metal catalysts comprising hollow forms or spheres are made of metal alloy and optionally activated. The metal catalysts can be used for the hydrogenation, dehydrogenation, isomerization reductive alkylation, reductive amination, and / or hydration reaction of organic compounds.

The invention relates to a method and system for monitoring and adjusting both air content and rheology (e.g., slump, slump flow) properties of a hydratable concrete mix contained within a concrete mixer. The system simultaneously tracks dosage of both rheology-modifying admixture (e.g., polycarboxylate polymer cement dispersant) and air control agent or “ACA” (e.g., air entraining agent) by reference to at least four nominal dose response (“NDR”) curves or profiles, which at least four NDR profiles are based on the respective behaviors of each of the ACA and rheology-modifying agent on air content and rheology.

The invention discloses a liquid alkali-free chloride-free accelerating agent and methods for preparing and using the same. Raw materials for preparing the accelerating agent include one or a plurality of the following components of aluminum sulfate, magnesium sulfate, hydramine, an early strength agent, a synergist and water. The aluminum sulfate is the purchasable industrial-grade aluminum sulfate hydrate Al2(SO4)3.18H2O and has the solid content of 51%-52%. The magnesium sulfate is MgSO4.7H2O with the solid content of 48%-49%. The hydramine is one or a plurality of mono ethanol amine, diethanolamine, triethanolamine or isopropoxide. The early strength agent is one or a plurality of calcium sulfate, calcium formate or calcium nitrite. The synergist is magnesium fluosilicate and / or magnesium fluoride. The liquid alkali-free chloride-free accelerating agent provided by the invention has the characteristics of good adaptability, low price, low mixing amount, good performance, good stability and the like; and moreover, the liquid alkali-free chloride-free accelerating agent is added into the concrete to be used as sprayed concrete, has the characteristics of low resilience, small dust pollution and the like and can satisfy the requirements of the 'JC477-2005 sprayed concrete accelerating agent' standard.

The invention discloses a reproducible phosphorus-uptake ceramsite and a preparation method thereof. The technical scheme provided by the invention comprises the following steps of: respectively drying 70-85 wt% of fly ash, 10-16 wt% of pore-forming agent and 5-14 wt% of clay powder and uniformly mixing the raw materials; after balling the mixture, baking at a temperature in a range of 950-1100 DEG C for 30-50 min to obtain a baked porous ceramsite; sequentially immersing the baked porous ceramsite with HCl, washing with water and drying; and loading zirconium oxide hydrate to obtain the phosphorus-uptake ceramsite. The phosphorus-uptake ceramsite prepared by the invention can be directly added into or filled as a filtering column to remove phosphorus in the water and the adsorbed phosphorus-uptake ceramsite can be desorbed by a NaOH solution to be reproduced; the saturated adsorption capacity to the phosphorus is 10-11 mg / g and the adaptability to the change of the phosphorus concentration in the water is good; after the treatment, the solid-liquid separation is easy to realize and the water quality of the discharged water is better. The reproducible phosphorus-uptake ceramsite provided by the invention has the advantages of strong phosphorus-uptake capability, easiness of realizing the solid-liquid separation, good cyclic usability and higher cost performance, so that the reproducible phosphorus-uptake ceramsite is applicable to phosphorous removal of various types of wastewater and surface water.

The invention discloses a hydration heat inhibited concrete expanding material as well as a preparation method and applications thereof. The hydration heat inhibited concrete expanding material is implemented by complexly using first two or three of an expanding agent, a hydration heat inhibitor and an inner curing agent. The hydration heat inhibited concrete expanding material disclosed by the invention fully plays the superimposed effect of the three types of materials, so that the dry shrinkage resistance and cold shrinkage resistance of concrete can be maximized. Experiments prove that concrete with the hydration heat inhibited concrete expanding material disclosed by the invention produces a large expansion in the temperature-fall period, thereby considerably improving the temperature shrinkage (caused by hydration heat) resistance of the concrete; the temperature rise of concrete can be effectively reduced; high relative humidity can be kept in the concrete for a long time, thereby providing a good hydration reaction environment for the expanding agent, and reducing dry shrinkage.

The invention relates to a colored aluminum pigment with high color depth and a preparation method thereof. The colored aluminum pigment is obtained by depositing a layer of silicon dioxide on a flaky metallic aluminum sheet substrate and then depositing one or more layers of metal oxide on the surface of the silicon dioxide, and the colored aluminum pigment exists in the form of dry powder. The preparation method comprises the following steps: a. stirring to disperse commercially available aluminum pigment slurry in alcohol, alcohol ether or a ketone solvent; b. regulating the temperature to 30-80 DEG C, respectively adding tetraethoxysilane and aqueous solution to the dispersed aluminum pigment slurry with the mol ratio of the tetraethylorthosilicate to the water ranging from 1:0.5 to 1:20, adding a catalyst such as ethylenediamine solution or aqueous ammonia, and obtaining aqueous aluminum pigment slurry by vacuum filtration and washing after the reaction; and c. cladding the aqueous aluminum pigment slurry obtained in the step b with the hydrated metal oxide on the powdered aluminum surface in a liquid phase. The preparation method help prepare the colored aluminum pigment with diversified colors and high color depth without reducing brightness of the original aluminum pigment slurry.

The present invention discloses an inorganic bone adhesive and its use in human hard tissue repairs. The inorganic bone adhesive comprises basic compound, phosphate, calcium phosphate bone cement and retarder with the characteristics of rapid hydration rate and high early strength. Inorganic Bone adhesive can be widely used in the artificial joints fixation, screw fixation as well as comminuted fracture fixation. It is a kind of safe and effective adhesive material and beneficial for the fast postoperative recovery. The final hydration reaction products contains the composition of magnesium phosphate, bio-mineral containing ammonium and apatite-like materials, which has excellent biocompatibility and can be gradually absorbed by surrounding tissues after being implanted in vivo, which benefits the in-growth of the new bone.

The invention particularly relates to a solid catalyst formed by assembling a racemic Co (salen) metal complex in a nano-reactor and used for the hydration reaction of an epoxy compound to prepare diol. The expression formula of the catalyst is: Co (salen) n / R, wherein R is a nano-reactor with a cage-type pore structure and Co (salen) is a racemic metal complex. A general molecular formula is shown as the following. And n represents the mass percent content of Co in the solid catalyst and ranges from 0. 1% to 1%. The catalyst can be used for a reaction of efficient catalysis of the hydration of an epoxy compound to prepare diol. The catalyst of the invention is characterized by simple preparation method, good reproducibility and easy recycling, thus being able to be used for industrial production.

The invention belongs to the technical field of nanometer materials, and particularly relates to a morphology-controlled carbon quantum dot / nickel cobaltate composite electrode material and a preparation method. The preparation method specifically comprises the following steps of (1) dissolving carbon quantum dot powder, nickel nitrate hexahydrate, cobalt nitrate hexahydrate and urea into a mixed solvent of water and ethanol, mixing, putting into a polytetrafluoroethylene-lined reaction kettle, adding foam nickel, sealing, heating to react, cooling, taking out foam nickel, flushing and drying; (2) performing heat treatment on the dried foam nickel, so as to obtain the carbon quantum dot / nickel cobaltate composite electrode material using the foam nickel as a substrate. The preparation method has the advantages that by adjusting the feeding amount of carbon quantum dots, different morphologies of the composite material, such as urchin shape, corolla shape and waxberry shape are formed on the micro structure; the preparation method is simple, the implementing is easy, and the cost is low; the chemical and physical property of obtained material is stable, and the application prospect is good in the fields of electrochemical energy storage and catalyzing.