The invention discloses a slow-release polycarboxylate
superplasticizer and a preparation method thereof. The preparation method comprises specific steps as follows: firstly, small unsaturated
carboxylic acid monomers and diphenylphosphinyl
chloride are subjected to a partial reaction, and small unsaturated monomers containing
phosphate ester groups are obtained; then 2-phenylethylamine and
phosphate ester groups are added to a
reaction system and subjected to a reaction, and small unsaturated monomers containing
amide groups are obtained; the small unsaturated monomers containing the
amide groups are subjected to an oxidation-reduction free
radical polymerization reaction with unsaturated polyether macromonomers under the action of an initiating agent, a
reducing agent and a
chain transfer agent, and a copolymerization product is obtained; pH value is adjusted to 6-7 after the reaction, water is added, and the polycarboxylate
superplasticizer is obtained. The
amide groups containing
benzene rings are introduced to side chains of the prepared polycarboxylate
superplasticizer, so that the dispersibility of the polycarboxylate superplasticizer for
cement is improved, the polycarboxylate superplasticizer has good
slump retaining performance on the premise of water reduction, and besides, the yield of the polycarboxylate superplasticizer containing the amide groups can reach 94% or higher.