High-voltage working electrolyte and preparation method thereof
An electrolyte, high-voltage technology, applied in the field of electrochemistry, can solve problems such as unfavorable performance of capacitors
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Embodiment 1
[0026] A preparation method of the above-mentioned high-voltage working electrolyte, comprising the following process steps:
[0027] (1) Mix 45g of ethylene glycol and 40g of γ-butyrolactone and heat to 80°C;
[0028] (2) Add 1g of nano silicon dioxide, 0.5g of mannitol and 2.2g of ethylenediaminetetraacetic acid, and mix;
[0029] (3) Heat to 120°C, add 11g of ammonium isosebacate, 0.2g of p-nitrobenzyl alcohol, and 0.1g of ammonium hypophosphite, and keep warm at 120°C until the mixture is completely dissolved;
[0030] (4) cooling to obtain a high-voltage working electrolyte.
Embodiment 2
[0032] A preparation method of the above-mentioned high-voltage working electrolyte, comprising the following process steps:
[0033] (1) Mix 45g of ethylene glycol and 40g of γ-butyrolactone and heat to 100°C;
[0034] (2) Add 2g of nano silicon dioxide, 0.5g of mannitol and 2.0g of ethylenediaminetetraacetic acid, and mix well;
[0035] (3) Heat to 130°C, add 8.6g of ammonium isosebacate, 1g of ammonium 1,10-dodecanoate, 0.5g of p-nitrobenzyl alcohol, 0.4 of ammonium hypophosphite, and keep warm at 130°C until the mixture is completely dissolved;
[0036] (4) cooling to obtain a high-voltage working electrolyte.
Embodiment 3
[0038] A preparation method of the above-mentioned high-voltage working electrolyte, comprising the following process steps:
[0039] (1) Mix 45g of ethylene glycol and 40g of γ-butyrolactone and heat to 80°C;
[0040] (2) Add 2g of nano silicon dioxide, 0.5g of mannitol and 2.2g of ethylenediaminetetraacetic acid, and mix;
[0041] (3) Heat to 130°C, add 10g of ammonium isosebacate, 0.2g of p-nitrobenzyl alcohol, and 0.1g of ammonium hypophosphite, and keep warm at 130°C until the mixture is completely dissolved;
[0042] (4) cooling to obtain a high-voltage working electrolyte.
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