325results about How to "Good solubility" patented technology

The invention relates to a preparation method for a chitosan natural polymer modified crude oil desalting demulsifier. The method comprises the following steps: 1) modifying polyethylene glycol monomethyl ether by halogenating; 2) preparing glycidyl dimethyl alkyl ammonium chloride; 3) preparing quaternized carboxy alkyl chitosan; 4) causing the modified polyethylene glycol monomethyl ether to react with the quaternized carboxy alkyl chitosan, thereby obtaining a target product, polyethylene glycol monomethyl ether grafted quaternized carboxy alkyl chitosan. According to the invention, the chitosan natural high-molecular compound is taken as the raw material and has the advantages of wide resource, naturality, non-toxicity, sustainability, excellent biological compatibility of products, degradability, and the like. The demulsifier prepared according to the invention has excellent demulsification dewatering effect; the molecule of the demulsifier contains a large amount of carboxy alkyl groups and quaternary ammonium salt groups and the electronegative ions, including metal cation, naphthene acid radicals, and surfaces are electronegative grains and have strong combining capacity, so that the demulsifier has the capacities of demulsifying while removing oil-soluble salt.

The invention relates to a preparation method of a polyether-grafted chitosan derivative crude oil desalting demulsifier. The preparation method comprises the following specific steps: firstly, performing formylation modification on polyethylene glycol monoethylether; secondly, preparing glycidyl dimethyl alkyl ammonium chloride; thirdly, preparing quaternarization carboxyalkyl chitosan; fourthly, enabling formylation modified polyethylene glycol monoethylether to react with carboxy alkyl chitosan to obtain the polyether-grafted chitosan derivative crude oil desalting demulsifier. The polyether-grafted chitosan derivative crude oil desalting demulsifier disclosed by the invention is prepared by taking chitosannatural polymeric compounds as raw materials, and has the advantages of wide sources, naturalness, no toxicity, sustainability, good biocompatibility of a product, degradability and the like. The prepared demulsifier is good in demulsifying and dehydrating effect; meanwhile, a demulsifying molecule contains a large amount of carboxyalkyl groups and quaternary ammonium salt groups which have strong combining capacity to metal cation, ions with negative electricity such as naphthenic acid radicals as well as particles of which the surfaces are electronegative, so the polyether-grafted chitosan derivative crude oil desalting demulsifier has capacity of removing oil-soluble salts while demulsifying.

The invention relates to a synthesis method of a crude oil desalting demulsifying agent. The method specifically includes the steps of firstly, conducting p-nitrophenyl ester modification on methoxypolyethylene glycol; secondly, preparing glycidyl dimethyl alkyl ammonium chloride; thirdly, preparing quaternized carboxy alkyl chitosan; fourthly, making the modified methoxypolyethylene glycol react with quaternized carboxy alkyl chitosan to obtain a product, namely polyethylene glycol questin grafted quaternized carboxy alkyl chitosan. A chitosan type natural high-molecular compound serves as the raw material and has the advantages of being wide in resource, natural, free of toxin, sustainable, good in product biocompatibility, degradable and the like; The prepared demulsifying agent is good in demulsifying dewatering effect; meanwhile, due to the fact that lots of carboxy alkyl groups and quaternary ammonium salt groups are contained in demulsifying agent molecules and have strong binding capacity with metal cations, naphthenic acid radicals and other ions with negative charges and particles with surface electronegativity, the oil-soluble salt removing capacity is achieved during demulsifying.

The invention discloses starlike anti-shearing polyacrylamide for a fracturing fluid and a preparation method of the starlike anti-shearing polyacrylamide. The core of the polymer is a thioxanthone modified dendriform polyamide-amine water soluble initiator and the arm of the polymer is a propenamide homopolymer and an acrylamide bipolymer or terpolymer. The preparation method comprises the following steps: modifying a dendriform macromolecule polyamide-amine in chloroform by using 2-epoxy thioxanthone so as to obtain a dendriform multifunctional macromolecular initiator; and initiating monomer polymerization of acrylamide and the like by taking the dendriform multifunctional macromolecular initiator as an initial starting core in an aqueous solution so as to prepare anti-shearing polyacrylamide. The starlike polymer which serves as a thickener is used for the fracturing fluid, is excellent in temperature-resisting and anti-shearing performances and free of residues after gel breaking and provides a powerful guarantee for wide application of fracturing construction operation in oil and gas fields. The preparation method is reliable in principle, strong in operability, mild in condition and relatively high in yield and has a broad market prospect.

The invention discloses an environmentally-friendly hot-melt pressure sensitive adhesive. The environmentally-friendly hot-melt pressure sensitive adhesive is prepared from, by weight, 25-35 parts ofa thermoplastic elastomer, 28-36 parts of modified petroleum resin, 6-10 parts of natural tackifying resin, 12-20 parts of a plasticizer, 2-3 parts of a modifying filler, 0.2-0.3 part of a coupling agent and 0.2-0.3 part of an antioxidant. The present invention also discloses preparation method of the hot-melt pressure sensitive adhesive. The thermoplastic elastomer is used as a matrix for the hot-melt pressure sensitive adhesive, the modified petroleum resin and the natural tackifying resin are used as tackifying resins, and no organic solvent is needed, so the raw materials are safe and environmentally friendly; the petroleum resin is modified, so the compatibility of the petroleum resin and the thermoplastic elastomer is improved, and the thermal stability of the hot-melt pressure sensitive adhesive is improved; and the reinforcing effect of the modifying filler improves the initial viscosity, the glass strength and the thermal stability of the hot-melt pressure sensitive adhesive are improved, so the environmentally-friendly hot-melt pressure sensitive adhesive with excellent performances is prepared.