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47results about How to "Effective regulatory structure" patented technology

Preparation method of doped carbon nitride fluorescent quantum dots

InactiveCN105670620AEffective regulatory structureEffective control of fluorescence propertiesNanotechnologyLuminescent compositionsSolubilityChemical reaction
The invention relates to a preparation method of doped carbon nitride fluorescent quantum dots.According to the preparation method, melamine and compounds corresponding to doped atoms serve as raw materials, while melamine molecules are roasted to form a carbon nitride structure, the doped atoms enter the carbon nitride structure through a chemical reaction, a doped carbon nitride block material is formed, and the block material is subjected to ultrasound crushing in an alcohol solvent to prepare the doped carbon nitride fluorescent quantum dots which are uniform in quantum size and grain size.The dried quantum dots are good in water solubility and dispersibility and have high fluorescent quantum dot yield.The method can be used for preparing the doped carbon nitride quantum dots in batches, the synthesis method is simple, and repeatability is good.The synthesized quantum dots have wide application prospects in the fields of fluorescence detection, light-emitting devices, biological marking and the like.
Owner:SHANDONG AGRICULTURAL UNIVERSITY

Preparation method of thermoplastic polyurethane micro air bag elastomer material

The invention relates to a preparation method of a thermoplastic polyurethane micro air bag elastomer material. The preparation method comprises the following steps of (1) feeding liquid raw materials such as diisocyanate molecules and a solid additive into a twin screw reactor, and carrying out polymerization chain extending reaction to obtain a high molecular weight hot melt; (2) pushing the high molecular weight hot melt into a mixing extrusion molding machine, and carrying out continuous reaction to produce a macromolecular thermoplastic polyurethane melt; (3) continuously adding the obtained macromolecular thermoplastic polyurethane melt, polymer particles and the like in a foaming extrusion molding machine, and then extruding the material from a mold head to an underwater pelletizing chamber in a form of a high-pressure hot melt; and (4) carrying pelletization by process water, sending the pellet-carrying process water to a separation machine by a multi-stage pressure relief and expansion process water pipeline, and carrying out separation, screening and drying to obtain a target product. Compared with the prior art, by adopting the preparation method provided by the invention, the thermoplastic polyurethane elastomer material can be directly prepared from the liquid raw materials such as MDI, so that the energy consumption and the material consumption are greatly lowered, the yield of a product is increased, the production efficiency of the product is improved and the like.
Owner:NANTONG DE NEW MATERIAL CO LTD

Degradable antifouling thermoplastic micro-airbag polymer elastomer material and preparation thereof

The invention relates to a degradable antifouling thermoplastic micro-airbag polymer elastomer material which is prepared from the following ingredients in percentage by weight: 88 to 98% of polymer raw material, 0.05 to 0.5% of nucleating agent, 0.4 to 2% of foaming agent and 0.1 to 10% of environment-friendly degradable organic perfluorosebacamidine material. A preparation method specifically comprises the steps: (1) feeding the polymer raw material, the nucleating agent and the environment-friendly degradable organic perfluorosebacamidine material from a feeding opening in the front end of a twin-screw extruder, feeding the foaming agent from a feeding opening in a middle section of the twin-screw extruder, hot melting and fully mixing all the raw materials, then sending into a static mixer to be further homogenized and then controlling pressure and quantitatively conveying by a melt pump; (2) sending hot melt sent out by the melt pump into an underwater pelletizing chamber to be pelletized, bringing out by technological water to be separated and screening and drying the particles to obtain a target product. Compared with the prior art, the degradable antifouling thermoplastic micro-airbag polymer elastomer material disclosed by the invention effectively achieves performance of antifouling, soiling-resistant, oil-resistant, contamination-resistant, attractive and good touch and is especially suitable for being applied to the fields of shoe materials, food package and the like.
Owner:NANTONG DE NEW MATERIAL CO LTD

Thermoplastic micro-sac polymer elastomer material and preparation method thereof

The invention relates to a thermoplastic micro-sac polymer elastomer material and a preparation method thereof. The material is prepared from the following components in percentage by weight: 0.1-97 percent of a support frame polymer material, 0.1-97 percent of pressure-resistance slow-rebound polymer material, 0.01-0.5 percent of a nucleating agent, and 0.1-10 percent of a foaming agent, wherein the support frame polymer material is a high-molecular-weight, high-hardness, high-crystalline or high-polarity polymer material; the pressure-resistance slow-rebound polymer material is a low-molecular-weight, low-hardness, low-crystalline to no irregular shape, low-polarity / no-polarity polymer material. Compared with the prior art, the material has the advantages that a winding network formed by the micro-sac structure and opening pores achieves an interpenetration structure, the rebound force and other material physical performance are excellent, buffer feedback is quick, contact and comfortable performance are high, exfoliated volume is controllable and the like.
Owner:NANTONG DE NEW MATERIAL CO LTD

Preparation method of electrode used for CO2 electrochemical reduction reaction

The invention relates to a preparation method of an electrode used for CO2 electrochemical reduction reaction. The electrode is prepared with foam copper, a copper wire mesh, a copper foil, a copper plate, a titanium wire mesh or a titanium plate as a substrate. The preparation method includes the steps of uniformly mixing a copper precursor solution being 0.01-2.0 M in concentrate and a template agent being 0.01-1.5 M in concentrate according to the molar ratio of 5:1-1:20 and magnetically stirring the solution for more than 30 min; moving the solution into a reaction kettle, immersing the substrate into the solution and performing a sealing reaction for 4-12 h; moving the substrate out from the reaction kettle, washing and drying the substrate, and performing thermal treatment to the substrate at 300-800 DEG C for 1-5 h under protection of an inert gas or an oxidizing atmosphere to obtain the substrate to which metal oxides are attached; and performing electrochemical reduction to the substrate to which metal oxides are attached in an acidic electrolyte to obtain the electrode. The preparation method is simple in preparation method and is suitable for large-scale production. The electrode is large in specific surface area and is high in CO2 oxygen reduction catalytic performance.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Preparation method of biochar-based composite material

The invention discloses a preparation method of a biochar-based composite material, and the preparation method comprises the following steps: firstly mixing, stirring and lyophilizing self-made orangepeel powder and a urea solution to prepare pretreated orange peel powder; mixing the pretreated orange peel powder and rectorite powder to put into an inert gas for calcination treatment, and performing ball-milling and sieving in a nitrogen-containing atmosphere, pickling, washing, filtering and drying to obtain the biochar-based composite material. The biochar-based composite material has goodstability, large adsorption capacity, strong adsorption capacity, simple preparation method and low preparation cost.
Owner:DONGGUAN LIANZHOU INTPROP OPERATION MANAGEMENT CO LTD

Preparation method and application of super-crosslinked porous polyion liquid material

The invention discloses a method for preparing a super-crosslinked porous polyion liquid material by ion thermal crosslinking and application of the material. The method comprises the following steps:performing quaternization on alkenyl tertiary amine and allyl halide or styrene benzyl halide to form a rigid diene ion liquid monomer; introducing proper complex anions through ion exchange; then performing ionic thermal polymerization in a zinc chloride / sodium chloride composite molten salt system to obtain the super-crosslinked porous ion liquid material. The obtained material has a wide application prospect. The preparation method has the advantages of: (1) high yield, which is up to 94 to 99 percent; (2) large specific area,which is 200m<2> / g or more; (3) full ion liquid framework and high active component content; (4) simple and convenient preparation process, and ready availability of raw materials; (5) wide material application, capability of effectively adjusting the material structure by adjusting raw materials, complex anions and polymerization conditions, and applicability in the fields of catalysis, gas adsorption, wastewater treatment, separation and the like; (6) easiness and convenience in recycling the materials.
Owner:SHAOXING UNIVERSITY +1

Preparation method of super crosslinked porous polyionic liquid material and application of super crosslinked porous polyionic liquid material

The invention provides a method of preparing a super crosslinked porous polyionic liquid material by ionic thermal polymerization and application of the super crosslinked porous polyionic liquid material. The method is characterized in that firstly, alkenyl tertiary amine and thionyl chloride are subjected to quaternization to form a rigid diene ionic liquid monomer; by ionic exchange, proper coordination anions are introduced; next, the ionic thermal polymerization is performed in a zinc chloride / potassium chloride composite molten salt system to obtain the super crosslinked porous polyionicliquid material; and the obtained material has wide application prospect. The method provided by the invention has the advantages that (1) the yield is high, and is 92 to 97 percent; (2) the specificsurface area of the prepared material is large and is 200 m<2> / g or above; (3) the material has a whole ionic liquid framework, and the active component content is high; (4) the preparation process issimple and convenient, and the raw materials can be easily obtained; (5) by adjusting the raw materials, the coordination anions and polymerization conditions, the material structure can be effectively regulated, so that the material can be widely used in the fields of catalysis, gas adsorption, waste water treatment, separation and the like; and (6) the material recovery and reuse are simple andconvenient, and the recovery can be realized through filtering.
Owner:SHAOXING UNIVERSITY +1

Method for preparing iron-cobalt bimetallic monatomic anchored nitrogen-doped graphene cocatalyst and application thereof

The invention relates to a method for preparing an iron-cobalt bimetallic monatomic anchored nitrogen-doped graphene cocatalyst and application thereof. The method comprises the following steps: adding graphene oxide into deionized water, ultrasonically mixing uniformly, adding a mixed solution of a cobalt chloride aqueous solution and a ferric chloride aqueous solution, and ultrasonically dispersing the graphene oxide in the mixed solution uniformly to obtain a solution A; putting the solution A into liquid nitrogen to be quickly frozen, performing freeze drying treatment, and performing high-temperature calcination in argon and ammonia gas atmospheres to obtain iron-cobalt bimetallic monatomic anchored nitrogen-doped graphene which is used as a cocatalyst; adding a loading material into an absolute ethyl alcohol solution for ultrasonic dispersion, compounding with the iron-cobalt bimetallic monatomic anchored nitrogen-doped graphene, mechanically stirring the mixture at room temperature, centrifuging, washing, drying in vacuum, grinding, and annealing to obtain the composite photocatalytic material. Iron-cobalt bimetallic single atoms are uniformly anchored on the surface of the nitrogen-doped graphene, and the nitrogen-doped graphene is well combined with different mesoporous semiconductor materials, so that the nitrogen-doped graphene has excellent photocatalytic hydrogen production performance.
Owner:WETOWN ELECTRIC GRP CO LTD

Preparation method of super-crosslinked porous polyion liquid material and application

The invention discloses a method for preparing a super-crosslinked porous polyion liquid material with ion thermal crosslinking and application of the material. The method comprises the following steps: performing quaternization on alkenyl tertiary amine and chloromethyl cyanide or cyano tertiary amine and allyl halide or styrene benzyl halide; introducing proper complex anions through ion exchange; performing ionic thermal alkenyl polymerization and cyano crosslinking in an aluminum chloride / sodium chloride composite molten salt system to obtain the super-crosslinked porous polyion liquid material. The obtained material has a wide application prospect. The preparation method has the advantages of: (1) high yield, which is up to 91 to 98 percent; (2) large specific area, which is 250m<2> / gor more; (3) full ion liquid framework and high active component content; (4) simple and convenient preparation process, and ready availability of raw materials; (5) wide material application, capability of effectively adjusting the material structure by adjusting raw materials, complex anions and polymerization conditions, and applicability in the fields of catalysis, gas adsorption, wastewatertreatment, separation and the like; (6) easiness and convenience in recycling the materials.
Owner:SHAOXING UNIVERSITY

Manganese-based bimetallic oxide mesoporous material, and preparation method and application thereof

The invention discloses a manganese-based bimetallic oxide mesoporous material, and a preparation method and an application thereof. The preparation method comprises the following steps: (1) dispersing a mesoporous silicon template into a dispersant, adding an aqueous manganese nitrate solution under a stirring condition in a water bath of 25-30 DEG C, continuously stirring and adsorbing for 40-60min to obtain a suspension, sequentially filtering, washing and drying the obtained suspension, and calcining to obtain a compound of manganese oxide and the mesoporous silicon template; and (2) re-dispersing the obtained compound in a dispersant, adding an aqueous ferric nitrate solution under a stirring condition in a water bath of 0 DEG C, stirring and adsorbing for 20-40 min, continuously adding the aqueous manganese nitrate solution, continuously stirring and adsorbing for 20-40 min to obtain a suspension, sequentially filtering, washing and drying the obtained suspension, calcining to obtain a manganese-based bimetallic oxide and SBA-15 compound, and removing the redundant mesoporous silicon template in the obtained compound to obtain the mesoporous silicon template. The manganese-based bimetallic oxide mesoporous material obtained by the invention is used for treating a complex wastewater system by a Fenton-like method.
Owner:ZHEJIANG GONGSHANG UNIVERSITY

Degraded glass ceramic thin film for medical magnesium alloy surface and preparation method of degraded glass ceramic thin film

InactiveCN102886072AAchieve regulated degradationEffective regulatory structureCoatingsProsthesisIonBone tissue
The invention relates to a degraded glass ceramic thin film for a medical magnesium alloy surface and a preparation method of the degraded glass ceramic thin film. The thin film is composed of CaO-PoO5-Na2O-MO, wherein the mol ratio of Ca to P is 1, M is one or combination of more selected from Zn, Sr, Mg, Ag, Ti and Al, the mol percentage of MO is 1-5%, the CaO-PoO5-Na2O is based and the ratio of Ca to P is controlled to be equal to 1; stable gels with various components are prepared by adding one or two different metal ions; a gel layer is evenly coated on the surface of a magnesium alloy substrate by dipping-lifting, and finally, the uniform and compact glass ceramic thin film is obtained after drying and heat treatment. The glass ceramic thin film prepared by using the method not only has excellent biological activity and degradable ability, but also has a controllable degrading rate; the degrading rate can be adjusted to be matched with the growth rate of a bone tissue to be restored, and therefore, various clinical demands are met.
Owner:TIANJIN UNIV

Microbial preparation for treatment of livestock and poultry manure and preparation method thereof

The invention discloses a microbial preparation for treatment of livestock and poultry manure. The microbial preparation comprises the following raw materials by weight: 1-5 parts of actinomycetes, 1-4 parts of Chaetomium torulosum freeze-dried powder, 1-3 parts of rhizobium, 1-3 parts of Trichoderma viride freeze-dried powder, 2-6 parts of geotrichum candidum freeze-dried powder, 20-40 parts of coconut shell powder, 1-2 parts of Chinese fir charcoal, 1-2 parts of bagasse, 1-2 parts of brown sugar, 5-15 parts of kaolin, and 100-150 parts of water. The microbial preparation obtained by the method provided by the invention can effectively regulate the microflora structure of livestock and poultry manure, improve the activity of beneficial microorganism, can form a complex and stable ecological system through the interaction of strains, can rapidly decompose organic matters in livestock and poultry manure to produce heat energy, rapidly raise the material temperature, inhibit or kill germs, worm eggs and other harmful organisms, and improve the decomposition degree.
Owner:WEIFANG SHENGQUAN BIOTECH CO LTD

Preparation method of activity-enhanced edible fungus polysaccharide and application of activity-enhanced edible fungus polysaccharide in losing weight and increasing intestinal beneficial flora

The invention provides a preparation method of activity-enhanced schizophyllum commune polysaccharide, which comprises the following steps: by taking schizophyllum commune sporocarp powder as a raw material, irradiating with limited high-energy electron flow, adding compound enzyme to carry out enzymolysis reaction, then carrying out subcritical deionized water extraction on enzymatic hydrolysate, and carrying out subsequent impurity removal treatment to obtain the schizophyllum commune polysaccharide. The molecular weight of the schizophyllum commune polysaccharide extracted by the method is remarkably reduced, so that the schizophyllum commune polysaccharide not only can effectively improve the diversity of intestinal flora, promote the growth of beneficial intestinal flora and inhibit the growth of potential pathogenic bacteria in intestinal tracts, but also can effectively resist the weight increase, and can be used as a natural auxiliary food which is free from side effects and is used for losing weight and regulating the intestinal flora.
Owner:FARM PROD PROCESSING & NUCLEAR AGRI TECH INST HUBEI ACAD OF AGRI SCI

Nano-silicon anticorrosive agent for preparing metal working fluid and preparation method of nano-silicon anticorrosive agent

PendingCN113106458AEffective adjustment compositionEffective regulatory structureAdditivesNano siliconMetal working fluid
The invention discloses a nano-silicon anticorrosive agent for preparing a metal working fluid and a preparation method of the nano-silicon anticorrosive agent, and belongs to the technical field of metal working compositions. The preparation method comprises the steps that an organic amine compound and water are mixed, and a silane coupling agent is dropwise added under the inert gas protection and stirring conditions; and the mixture is heated to a first temperature after dropwise adding is completed, stirred under the inert gas protection condition, then heated to a second temperature, stirring under the inert gas protection condition, and cooled after stirring is completed to obtain the clear and transparent nano-silicon anticorrosive agent, wherein the second temperature is higher than the first temperature. The preparation method is simple in process, easy to operate, short in processing time, almost free of production danger and production pollution in the preparation process and suitable for industrial application and popularization, the obtained nano-silicon anticorrosive agent can stably exist in the metal working fluid after being used for preparing the metal working fluid, the problems of sedimentation, aggregation or precipitation and the like are avoided, and the prepared metal working fluid has good stability and integrity.
Owner:SHENZHEN FRANCOOL TECH

Application of bifidobacterium breve CCFM1025 in relieving Alzheimer's disease

The invention discloses application of bifidobacterium breve CCFM1025 in relieving Alzheimer's disease, and belongs to the field of microorganisms. The bifidobacterium breve CCFM1025 can significantly improve cognitive and memory disorder of mice with Alzheimer's disease, reduce the content of A beta 1-42 protein in the brains of the mice with Alzheimer's disease, improve the level of brain-derived neurotrophic factors and postsynaptic density protein in the brains of the mice with Alzheimer's disease, and improve the content of interleukin 6 in the serum of the mice with Alzheimer's disease; and the bifidobacterium breve CCFM1025 can regulate intestinal flora and metabolites thereof. The bifidobacterium breve CCFM1025 can be used for preparing pharmaceutical compositions for relieving dementia and Alzheimer's disease and improving cognitive disorder, can also be used as a microecological preparation to be applied to drugs, fermented food or health care products, and has a very wide application prospect.
Owner:JIANGNAN UNIV

A kind of preparation method of thermoplastic polyurethane micro-airbag elastomer material

The invention relates to a preparation method of a thermoplastic polyurethane micro-airbag elastomer material, which comprises the following steps: (1) feeding liquid raw materials such as diisocyanate molecules and solid additives into a twin-screw reactor to carry out polymerization chain extension reaction to obtain high molecular weight (2) Push the high molecular weight hot melt into the mixing extruder to continue the reaction to generate a high molecular thermoplastic polyurethane melt; (3) continue to combine the obtained high molecular thermoplastic polyurethane melt with the polymer Pellets, etc. are added to the foaming extruder, and then extruded from the die head to the underwater pelletizing chamber in the form of high-pressure hot melt; (4) The pellets are carried by the process water and sent to the separation process through the multi-stage pressure release and expansion process water pipeline. Machine place, after separation, screening and drying, the target product will be formed. Compared with the prior art, the present invention can directly produce thermoplastic polyurethane elastomer materials from liquid raw materials such as MDI, which greatly reduces energy consumption and material consumption, and improves product yield and production efficiency.
Owner:NANTONG DE NEW MATERIAL CO LTD

Preparation technology of molybdenum-carbide-doped ruthenium-base alloy diffusion barrier layer used for copper-free seed crystal interconnection

The invention discloses a preparation technology of a molybdenum-carbide-doped ruthenium-base alloy (RuMoC) diffusion barrier layer, and relates to a novel preparation technology of a diffusion impervious layer between copper (Cu) and a silicon-oxide-based insulating medium (SiOC: H) in an ultra-deep submicron integrated circuit back-end interconnection structure. The thermal stable temperature of the RuMoC (5 nm) barrier layer deposited through the preparation technology can reach above 600 DEG C, and the situation that copper atoms diffuse towards the inner portion of a silicon-oxide-based medium body can be restrained effectively. The RuMoC (5 nm) barrier layer prepared through the technology can effectively reduce the electrical resistivity of an interconnection film system, reduce the resistance-capacitance coupling (RC) delay effect of interconnection circuits, increase the operating speed of semiconductor devices and improve the stability of the semiconductor devices.
Owner:SICHUAN UNIV

Method for preparing thermal expansion microspheres based on interfacial polymerization

The invention provides a method for preparing thermal expansion microspheres based on interfacial polymerization, which comprises the following steps: uniformly mixing an oil-phase composition and a water-phase composition to form a suspension, and carrying out an interfacial polymerization reaction process on the suspension to obtain the thermal expansion microspheres, wherein the aqueous phase composition comprises nanoparticles, an amphiphilic peroxide initiator and a suspending agent, and the oil phase comprises low-boiling-point alkane and acrylonitrile polymeric monomers. The thermal expansion microsphere is prepared through interfacial free radical polymerization, a salting-out effect and a polymerization inhibitor do not need to be adopted to prevent a monomer from being dissolvedin a water phase to generate self-polymerization, generation of waste brine is avoided, and the prepared thermal expansion microsphere has the advantages of being low in monomer residual quantity, high in foaming ratio, good in temperature resistance and the like. The thermal expansion microspheres have the advantages of low VOC, no toxicity and the like when being applied to products.
Owner:潘自地

Heterojunction nano array electrode material and preparation method and application thereof

The invention belongs to the technical field of electrocatalytic oxygen evolution electrode materials, and particularly relates to a heterojunction nano array electrode material and a preparation method and application thereof. According to the preparation method, the iron-based current collector is placed in the potassium permanganate aqueous solution, the heterojunction nano array electrode material is obtained through the hydrothermal reaction, and the one-step hydrothermal method adopted in the method has the advantages of being economical, rapid, green, simple, rapid in reaction and capable of being produced on a large scale; wherein the iron-based current collector serves as a carrier and also serves as an iron source, and in-situ growth of an array on the current collector can be realized, so that the mechanical stability of an electrode material is improved, and charge transfer is accelerated. According to the obtained heterojunction nano array electrode material, delta-MnO2 and TM-FeOOH which are good in stability are coupled together to construct a heterojunction, an electronic structure can be effectively regulated and controlled, intrinsic activity can be improved, charge transfer can be promoted, more active sites can be provided, and therefore high-performance OER application is achieved.
Owner:SUN YAT SEN UNIV

Preparation method and application of immobilized photocatalyst PVDF-TiO2@g-C3N4 fiber pad

The invention discloses a preparation method of an immobilized photocatalyst PVDF-TiO2@g-C3N4 fiber pad; a photocatalyst TiO2@g-C3N4 with a special core-shell structure is prepared by a one-step in-situ synthesis method and by regulating and controlling the mass ratio of urea to anatase titanium dioxide, the preparation method is simple, a compact and uniform heterojunction structure can be formed, compounding of photo-induced electrons-holes is effectively inhibited, and excellent photocatalytic activity is achieved; then the electrospinning technology is used, and the TiO2@g-C3N4 catalyst isfixed on a PVDF fiber pad; the preparation method has the advantages that the preparation method is simple, the fiber structure can be effectively regulated and controlled, the separation and the recycling are easy, and the wide application prospect is realized.
Owner:XIAMEN UNIV

Non-starch lily polysaccharide NSLP-1 and application thereof

The invention belongs to the technical field of medicines, and discloses non-starch lily polysaccharide NSLP-1 and application thereof. The non-starch lily polysaccharide NSLP-1 is separated and extracted from lily, and has effects of inflammation resistance, intestinal flora disorder regulation and control, and sleep disorder improvement, and provides a natural and novel drug source for development of prevention or treatment of intestinal flora disorder or diseases induced by intestinal flora disorder.
Owner:GUANGDONG PHARMA UNIV

Preparation method and application of hypercrosslinked porous polyionic liquid material

The invention provides a method for preparing hypercrosslinked porous polyionic liquid material by ion thermal crosslinking and its application. In the method, alkenyl tertiary amine is quaternized with allyl halide or styrene benzyl halide to form Rigid diene ionic liquid monomer, and introduce suitable matching anion by ion exchange, then, carry out ionic thermal polymerization in zinc chloride / sodium chloride composite molten salt system, obtain hypercrosslinked porous polyionic liquid material, the obtained material has Wide application prospects. The advantages of this method: (1) high yield, 94% to 99%; (2) large specific surface area of ​​the prepared material, within 200m 2 / g or more; (3) The material has an all-ionic liquid skeleton with a high content of active components; (4) The preparation process is simple and the raw materials are easy to obtain; (5) The material has a wide range of applications, and can be effectively Adjusting the material structure can be used in catalysis, gas adsorption, wastewater treatment, separation and other fields; (6) The material is easy to recycle and reuse.
Owner:SHAOXING UNIVERSITY +1

A kind of biogel electrolyte composed of pan and modified plla and preparation method thereof

The invention discloses a biogel electrolyte composed of PAN and modified PLLA and a preparation method thereof. The skeleton membrane of the biogel electrolyte composed of PAN and modified PLLA in the present invention is a nanofibrous membrane composed of PAN and modified PLLA, wherein the mass ratio of PAN to modified PLLA is (2.5-4.5):1. The raw material of the present invention has adopted modified PLLA and PAN, utilizes two kinds of materials to utilize the hydrogen bonding between the two, reduces the "passivation effect" that pure PAN produces, improves electrochemical performance, and PLLA is modified, further The mechanical strength of the polymer is stabilized, thereby ensuring the stability of the mechanical and electrochemical properties of the biogel electrolyte composed of the PAN and the modified PLLA of the present invention.
Owner:CENT SOUTH UNIV

Preparation method of HNTs plasticized PAN/P(LLA-EG-MA) polymer electrolyte and product thereof

The invention discloses a preparation method of an HNTs plasticized PAN / P(LLA-EG-MA) polymer electrolyte and a product thereof. An HNTsPAN / P(LLA-EG-MA) cross-linked polymer film is prepared by adopting an electrostatic spinning method, a porous polymer film is formed by mutually overlapping nanofibers, formed pores can provide a good ion channel, the nanofibers are easily activated and gelled by a liquid electrolyte, and meanwhile, the method can effectively regulate and control the fine structure of the fibers. Chemical bonds and hydrogen bonds exist between molecules of the prepared HNTsPAN / P(LLA-EG-MA) cross-linked polymer film, the HNTsPAN / P(LLA-EG-MA) cross-linked polymer film has high structural stability, the thickness of a framework membrane of the blended polymer electrolyte and the diameter size of fibers are uniformly distributed, the HNTsPAN / P(LLA-EG-MA) cross-linked polymer membrane has good amorphism, economy and environmental protection, and the preparation method is high in practicability and has a good industrial prospect.
Owner:CENT SOUTH UNIV

Preparation method and application of ultra-deep gasoline and diesel hydrodesulfurization catalyst

The invention relates to the field of gasoline and diesel oil hydrodesulfurization catalysts, and provides a preparation method of an ultra-deep gasoline and diesel oil hydrodesulfurization catalyst,which comprises the following steps: by using a nitrogen-doped carbon material as a carrier, attaching an active component to the carrier by an impregnation method, performing drying and roasting to obtain the ultra-deep gasoline and diesel oil hydrodesulfurization catalyst, wherein the active component comprises a metal salt and an auxiliary metal salt. According to the invention, a nitrogen-doped carbon material is used as a carrier, and a traditional Co (Ni)-Mo (W) metal active phase is loaded to prepare the novel catalyst; compared with a Co (Ni)-Mo (W) hydrogenation catalyst commonly usedin the industry, the catalyst has the advantages that a nitrogen-doped carbon material formed by introducing N atoms with high charges and spin density into a carbon material has excellent electron donating characteristics, and the electron and morphology structures of a metal active phase can be effectively regulated and controlled through the anchoring effect and the electron donating effect, therefore, the catalyst has higher gasoline and diesel hydrogenation activity and desulfurization effect, and better reserves the octane number of gasoline.
Owner:GUANGDONG UNIV OF PETROCHEMICAL TECH

A kind of thermoplastic micro-airbag polymer elastomer material and preparation method thereof

The invention relates to a thermoplastic micro-airbag polymer elastomer material and a preparation method thereof. The thermoplastic micro-airbag polymer elastomer material includes the following components in weight percentage: supporting skeleton polymer material 0.1-97%, pressure-resistant and slow-rebound 0.1-97% of the polymer material, 0.01-0.5% of the nucleating agent, and 0.1-10% of the foaming agent; the supporting skeleton polymer material is a polymer material with high molecular weight, high hardness, high crystallization or high polarity, so The pressure-resistant slow-rebound polymer material is a low molecular weight, low hardness, low crystallization to amorphous, low polar / non-polar polymer material corresponding to the supporting skeleton polymer material. Compared with the prior art, the polymer elastomer material prepared by the present invention has an intertwined network formed by the micro-airbag structure and open cells to form an interpenetrating structure, excellent material properties such as resilience, neat cushioning and feedback, and a sense of touch and comfort. High, controllable expansion ratio, etc.
Owner:NANTONG DE NEW MATERIAL CO LTD

Functional beef cattle and mutton sheep compound feed additive and preparation method thereof

The invention discloses a functional beef cattle and mutton sheep compound feed additive and a preparation method thereof, and belongs to the technical field of animal feed additives. The additive is prepared from the following components: 5-40 parts of VE (vitamin E), 10-100 parts of VC (vitamin C), 50-150 parts of plant extract, 10-100 parts of probiotic and yeast culture, 100-300 parts of mildew removing agent, 100-300 parts of almond shell, 100-200 parts of potassium magnesium sulfate, 100-200 parts of table salt, 5-25 parts of immune polysaccharide, 2-5 parts of zinc ions and 10-30 parts of phagostimulant. The content of calcium ions in the additive is 5-15 wt%. The additive can effectively relieve the problems of endocrine disorder, anorexia, digestive dysfunction, increase of death and culling rate and the like caused by stress of feeder cattle and lambs entering a fence, and can effectively regulate and control a rumen flora structure and a nutrient metabolism path when being used in the whole fattening period; and the whole health degree of animals is improved, the appetite and the feed intake are improved, and the production performance and the feed conversion rate are improved.
Owner:青筑保定园林景观设计有限公司

Preparation process of molybdenum carbide-doped ruthenium-based alloy diffusion barrier layer for copper-free seed crystal interconnection

The invention discloses a preparation technology of a molybdenum-carbide-doped ruthenium-base alloy (RuMoC) diffusion barrier layer, and relates to a novel preparation technology of a diffusion impervious layer between copper (Cu) and a silicon-oxide-based insulating medium (SiOC: H) in an ultra-deep submicron integrated circuit back-end interconnection structure. The thermal stable temperature of the RuMoC (5 nm) barrier layer deposited through the preparation technology can reach above 600 DEG C, and the situation that copper atoms diffuse towards the inner portion of a silicon-oxide-based medium body can be restrained effectively. The RuMoC (5 nm) barrier layer prepared through the technology can effectively reduce the electrical resistivity of an interconnection film system, reduce the resistance-capacitance coupling (RC) delay effect of interconnection circuits, increase the operating speed of semiconductor devices and improve the stability of the semiconductor devices.
Owner:SICHUAN UNIV

Thermoplastic micro-balloon polymeric elastomer material and preparation method thereof

The invention relates to a thermoplastic micro-balloon polymeric elastomer material and a preparation method thereof. The thermoplastic micro-balloon polymeric elastomer material comprises, by weight,0.1-97% of a support frame polymeric material, 0.1-97% of a pressure-resistant slow-recovery polymeric material, 0.01-0.5% of a nucleating agent and 0.1-10% of a foaming agent. The support frame polymeric material is a high-hardness, high-crystallinity or high-polarity polymeric material; the pressure-resistant slow-recovery polymeric material is low-hardness low-crystallinity amorphous low-polarity / nonpolar polymeric material corresponding to the support frame polymeric material. Compared with the prior art, the thermoplastic micro-balloon polymeric elastomer material has the advantages that, for instance, a tangled network formed by micro-balloon structures and open cells forms mutual-penetrating structure, the material properties, such as recovery, are excellent, buffering feedback isclear, good tough and comfort are provided, and expansion rate is controllable.
Owner:NANTONG DE NEW MATERIAL CO LTD
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