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847 results about "Monoclinic crystal system" patented technology

In crystallography, the monoclinic crystal system is one of the 7 crystal systems. A crystal system is described by three vectors. In the monoclinic system, the crystal is described by vectors of unequal lengths, as in the orthorhombic system. They form a rectangular prism with a parallelogram as its base. Hence two vectors are perpendicular (meet at right angles), while the third vector meets the other two at an angle other than 90°.

Nano copper oxide analogue enzyme and method for measuring hydrogen peroxide by using nano copper oxide analogue enzyme as peroxide analogue enzyme

The invention discloses a nano copper oxide analogue enzyme and a method for measuring hydrogen peroxide by using the nano copper oxide analogue enzyme as a peroxide analogue enzyme. The nano copper oxide analogue enzyme is nano copper oxide powder with a grain diameter ranging from 5 to 8 nanometers; the nano copper oxide is Cuo of a monoclinic system, the space group is C2 / c; and the maximum absorption peaks of the typical ultraviolet-visible absorption spectra of the prepared nano copper oxide are at 280-nanometer positions. The nano copper oxide analogue enzyme is obtained by a chemical precipitation process. The nano copper oxide analogue enzyme has a catalytic property similar to that of peroxidase. When the nano copper oxide analogue enzyme is used in a 4-aminoantipyrine-ol system, the colorimetric detection of hydrogen peroxide can be realized, the hydrogen peroxide detection limit is 0.02mmol / L, and the linear range is 1mmol / L.
Owner:FUJIAN MEDICAL UNIV

Cathode composite material and lithium ion battery using the same

A cathode composite material includes a cathode active material and a coating layer coated on a surface of the cathode active material. The cathode active material includes a layered type lithium nickel cobalt manganese oxide. The coating layer comprises a lithium metal oxide having a crystal structure belonging to C2 / c space group of the monoclinic crystal system. The present disclosure also relates to a lithium ion battery including the cathode composite material.
Owner:TSINGHUA UNIV +1

Vanadate nanofiber photocatalyst and preparation method thereof

The invention relates to a vanadate nanofiber photocatalyst and a preparation method thereof. The nanofiber photocatalyst is pucherite, or silver vanadate, or a compound of pucherite and silver vanadate. Organic vanadic salt, organic bismuth salt and the like with good alcohol solubility are taken as precursor reactors, a spinning solution is prepared by a PVP (Polyvinyl Pyrrolidone) and alcohol system, electrospining is performed by an electrospining device, then high-temperature roasting is performed, and the vanadate nanofiber photocatalyst is obtained. A prepared vanadate nanofiber is in a monoclinic crystal phase, is 30-100nm in diameter, has a narrower band gap, shows good visible light catalytic degradation ability for ofloxacin, a contaminant in water, and can be separated from a solution quickly by precipitation.
Owner:QINGDAO AGRI UNIV

Method for preparing monoclinic system crystalline state cupric oxide and uses thereof

The invention relates to a method for preparing monoclinic crystal system crystalline copper oxide and an application of the monoclinic crystal system crystalline copper oxide. The method comprises the following steps: a. a sodium hydroxide or potassium hydroxide water solution with a concentration of between 5 and 50 percent and a volume of between 30 and 80 percent of the volume of a reaction vessel is added into the reaction vessel, preheated to between 30 and 100 DEG C, added with crystalline copper chloride hydroxide with the addition between 1/6 and 1/3 of the mol number of sodium hydroxide, and reacted for 10 to 60 minutes at a reaction temperature of between 30 and 100 DEG C and under the condition of stirring; b. crystalline copper oxide is prepared after washing, pumping filtration, centrifugation and drying of reacted materials; and c. the crystalline copper oxide is crushed by the physical method, and the activated copper oxide with fine granularity are prepared. The method is easy to realize separation of the copper chloride hydroxide and the copper oxide with other water-soluble background salts, and has a simple technique and low production cost; and the crystalline copper oxide prepared has high yield, high purity, high activity, good quality and is suitable for mass production.
Owner:SHENZHEN SHENTOU ENVIRONMENT TECH CO LTD

Compound barium borofluoride, barium borofluoride non-linear optical crystal, and preparation method and use of the barium borofluoride non-linear optical crystal

The invention discloses a compound barium borofluoride, a barium borofluoride non-linear optical crystal, and a preparation method and a use of the barium borofluoride non-linear optical crystal. The compound barium borofluoride and the barium borofluoride non-linear optical crystal have the same chemical formula of Ba3B6O11F2. The barium borofluoride non-linear optical crystal belongs to a monoclinic system, has a space group P2(1), has cell parameters shown in the patent specification, wherein beta is equal to 101.351(4)deg., and has the molecular weight of 690.88. The powder frequency-doubling effect of the barium borofluoride non-linear optical crystal is 3 times that of KDP (KH2PO4). The compound barium borofluoride is synthesized by a solid-phase reaction method. The barium borofluoride non-linear optical crystal grows by a high-temperature melting method. The barium borofluoride non-linear optical crystal has large mechanical hardness, can be cut, polished and stored easily, and can be widely used in preparation of nonlinear optical devices such as a frequency multiplication generator, an upper frequency converter, a lower frequency converter and an optical parameter resonator.
Owner:XINJIANG TECHN INST OF PHYSICS & CHEM CHINESE ACAD OF SCI

White light LED, enhanced light transfer powder, phosphor powder and method of producing phosphor powder

The invention discloses a white light LED, an enhanced light transfer powder, a phosphor powder and a method of producing phosphor powder that use a plurality of radiating color lights and include a white light nitride heterostructure. The invention provides a novel solid liquid of a luminescence material with a chemical formula BaαY3βAl2α+5βO4α+12β, where α and β have a value ranging 0.1˜4. The crystal lattice structure of the phosphor powder varies from cubic crystal system to monoclinic crystal system accroding to the change of the ratio of α and β. It shows significant yellow color and yellowish orange color and has very high quantum light emitting efficiency and enduring light emitting time. In such novel phosphor powder base, the invention further develops an enhanced light transfer apparatus that is a blue light heterostructure emiting a raidaion with a wavelength λ=450˜475 nm and comprised of polymers and phosphor powder particles filled therein, and the concentration of phosphor powder is 1%˜50%. The novel white semiconductor source has a very high light intensity (I>100 cd) and luminous flux, and its light emitting efficiency is up to 501 m / w.
Owner:TSAI SHIAN MENG CHEN

Method for preparing mesoporous beta-Ga2O3 nanorod photocatalyst by using PEG (polyethylene glycol) as template

The invention belongs to the technical field of photocatalyst materials and preparation thereof, and aims to provide a method for preparing a mesoporous beta-Ga2O3 nanorod photocatalyst by using PEG (polyethylene glycol) as a template. According to the method, gallium-containing compounds and alkaline matters are used as raw materials, the PEG is used as the template, and a hydrothermal synthesis method is adopted to prepare the mesoporous beta-Ga2O3 nanorod photocatalyst. The invention can effectively control the crystal growth, improve the crystal form structure of the catalyst, increase the specific area of the catalyst, generate abundant oxygen vacancies or gallium-oxygen vacancy pairs, and enhance the photoresponse intensity of the catalyst, thereby enhancing the photocatalytic efficiency of the catalyst. The experiment of decomposing methylbenzene by photocatalytic oxidation indicates that the photocatalytic efficiency of the PEG-modified beta-Ga2O3 is 1.2-10 times of that of the beta-Ga2O3 which is not modified by the PEG. The method has the advantages of simple technique and adjustable parameters, and is easy to operate; and the prepared beta-Ga2O3 nanorod photocatalyst is a monoclinic system with complete and regular crystal form, belongs to a mesoporous material, and has the advantages of high photoresponse capacity and high catalytic performance.
Owner:ZHEJIANG UNIV

Levamlodipine besylate crystal and preparation method and application thereof

ActiveCN105111137AClarify the main parametersClear crystal formOrganic chemistry methodsSulfonic acids salts preparationSolubilitySpace group
The invention provides a levamlodipine besylate crystal with the molecular formula being (C20H25ClN2O5) (C6H6O3S) (H2O) 1.5 and the molecular weight being 594.07. Crystallography measurement parameters are a monoclinic system and P21 chirality space groups, and the chirality absolute configuration is determined by crystallography Flack parameter being 0.08(6); the unit cell size is shown in the specification, wherein beta is 95.817(4) degrees, and V is 2880.1(11). The characteristic peak in an X-ray powder diffraction pattern (Cu-Kalpha) is displayed at 2thea being 6.70 degrees, 10.12 degrees, 12.40 degrees, 13.36 degrees, 13.68 degrees, 17.04 degrees, 22.46 degrees and 24.16 degrees. The invention further provides a preparation method and application of the levamlodipine besylate crystal. The levamlodipine besylate crystal has the specific crystal form and the amount of crystal water and specific crystallography main parameters and the exact atom spatial position, the solubleness and stability of existing levamlodipine besylate are improved, the stability and bioavailability of the levamlodipine besylate tablet can be improved, preparation is easy, the cost is low, and the obtained crystal is regular in form, uniform in particle size and suitable for large-scale application and popularization.
Owner:菲洋生物科技(吉林)有限公司

Visible light catalyst BiVO4 and preparation method thereof

The invention discloses a visible light catalyst BiVO4 and a preparation method thereof. The BiVO4 is powder, the crystalline phase is monoclinic crystal serial scheelite structure, and the feature thereof is in a three-dimensional connected pore channel structure. In the preparation method, ethanediol is utilized as solvent, and bismuth salt and vanadium salt are respectively used as a Bi source and a V source for preparing the three-dimensional connected pore channel structural BiVO4. The preparation method is as follows: dissolving bismuth salt and vanadium salt into ethanediol according to the proportion that Bi / V equals to 1:0.5-1:2 to prepare solution the Bi ion concentration of which is 0.05-0.5mol.L<-1>; forming even settled solution, and then transferring the settled solution to a constant-temperature water bath tank of 50-90 DEG C to preserve heat for 2-10 days; and after obtaining flocks, centrifuging, washing, drying and finally calcining obtained powder at the temperature of 350-600 DEG C for 1-3h in air environment. In the invention, no surfactant is utilized, and the catalyst with novel structure and very large specific surface area is obtained after simple heat preservation in the water bath tank and later-stage low temperature heat treatment. The catalyst has smaller particles and higher photocatalysis activity, thus being applied to degrading organic pollutants by visible light catalyst.
Owner:HUAZHONG UNIV OF SCI & TECH

Sofosbuvir monocrystal M and preparation method and applications of sofosbuvir monocrystal M

The invention discloses a sofosbuvir monocrystal M and a preparation method and applications of the sofosbuvir monocrystal M. The sofosbuvir monocrystal prepared according to the preparation method disclosed by the invention belongs to a monoclinic system, and the space group is P21; the unit cell parameters are as follows: a=13.816 (3) A, b=5.973 (2) A, c=17.666 (4) A, and Beta=108.96 (3); the unit cell volume is 1378.7 (3) A3, and the number Z of molecules in a unit cell is 2. Solvents selected in the sofosbuvir monocrystal M disclosed by the invention are methylene chloride, chloroform, ethanol, isopropanol, acetonitrile, and C3-C7 alkyl cyanoacetate or C3-C7 dialkyl carbonate or C3-C7 dialkyl oxalate, and the like, and the sofosbuvir monocrystal is prepared by using a solvent evaporation method. The sofosbuvir monocrystal prepared according to the preparation method disclosed by the invention has good stability.
Owner:汤律进 +3
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