The invention discloses a preparation method of high-entropy
oxide ceramic. The method comprises the following steps that 1, according to
metal atom
mole ratio being 1:1:1:1 or 1:1:1:1:1, four or fiveor less kinds of
metal oxide powder are weighed; the
oxide powder includes MgO, ZnO, NiO, CuO, CaO, CoO, ZrO2, CeO2, Al2O3, Gd2O3, La2O3, Er2O3, Y2O3, Fe2O3, Co3O4 and CaCO3; 2,
powder weighed in step 1 is subjected to ball milling,
drying and
granulation; 3, granulated powder is pressed and molded to form a
green body; 4, the
green body obtained in step 3 is subjected to
thermal treatment; 5, the
green body obtained after
thermal treatment in step 4 is heated to the preset temperature, an
electric field of the preset
electric field intensity is applied to a sample, after flash-burning appears, a power source is converted from the
constant voltage state to the
constant current state, the temperature is kept constant for 1-60 min under the preset
current density, and then
quenching is performed to obtain the needed high-entropy
oxide ceramic. The flash-burning is adopted for preparing the high-entropy
oxide ceramic, the
sintering temperature is remarkably lowered, and the
sintering time is remarkably shortened.