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1322results about How to "Low curing temperature" patented technology

Method for preparing environmentally-friendly adhesive for lignin-based timber

The invention discloses a method for preparing an environmentally-friendly adhesive for a lignin-based timber. The method comprises the following steps of: 1) adding phenol, formaldehyde solution, lignin, first alkali liquor and diluting water into a reactor, heating to the temperature of between 75 and 85 DEG C and reacting for 2.5 to 3.5 hours, wherein the molar ratio of formaldehyde to the phenol is 2.20:1-2.40:1; the formaldehyde solution is added for three times in a mass ratio of 1.5 to 1.0 to 1.0; and the reaction time ratio of the added formaldehyde solution is 1.2 to 1.0 to 1.0; 2) cooling to 70 DEG C, adding a formaldehyde collector and second alkali liquor, and reacting at the temperature of between 65 and 70 DEG C for 20 to 50 minutes; and 3) cooling to the temperature of between 30 and 40 DEG C, adding an intensifier, stirring for 10 to 30 minutes, cooling and discharging. In the method, a 50 to 60 percent petroleum-based phenol raw material can be substituted; the methodis stable in reaction, easy to control and easy for industrial production; formaldehyde emission of a plywood reaches E0 level; adhesive strength meets the requirements of national class I plates; and a new approach is provided for the development of an environmentally-friendly biomass-based timber adhesive and recycling of wastes.
Owner:青岛生物能源与过程研究所

Novel phthalonitrile resin and preparation method thereof

The invention discloses a novel phthalonitrile resin and a preparation method thereof. Compared with a conventional phthalonitrile resin (only 4-nitro phthalonitrile as an end-capping reagent, the novel phthalonitrile resin is introduced with 3-nitro novel phthalonitrile resin to cooperate end capping, and thus the asymmetry of a resin structure is increased and the turbidity of a resin component is increased (see a formula 1). Compared with the conventional phthalonitrile resin, the novel phthalonitrile resin disclosed by the invention has the characteristics of low melting temperature, good solubility, wide processing window, low curing temperature and the like; a prepared resin molded part and a resin-based composite material are low in porosity, excellent heat-resistant quality, and high in mechanical property, and can be applied to the fields of aerospace, a space technology, machine manufacturing, and the like as a light-weight and high-temperature resistant part. The formula is described in the specification.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Method of preparing methyl phenyl polysiloxane

The invention discloses a method for synthesizing organic silicon, in particular provides a method for preparing methyl phenyl silicone resin which has low curing temperature by self and is not sticky repeatedly. The invention uses the monomers of methyl trichlorosilane, dimethyldichlorosilance, phenyl trichlorosilane, dichloromethylphenylsilane, diphenyl dichlorosilane and the like to obtain a methyl phenyl silicone resin with low curing temperature and a paint film which is not sticky repeatedly after being cured by the processes of adjusting the proportion of raw materials, controlling proper reaction temperature and polymerization time, carrying out hydrolysis reaction and polycondensation reaction, etc. The invention has the advantages that the methyl phenyl silicone resin prepared by the method has the characteristics of low curing temperature, being not sticky repeatedly, being clear and transparent, high and low temperature resistance, weather resistance, being insulating and the like; the methyl phenyl silicone resin is in particular fit for dip varnish higher than grade H; and the methyl phenyl silicone resin is used for confecting insulated paint, weather-resistant paint and heat resistant paint higher than grade H, is used for heat resistant parting agent and also can be used in the fields with rigorous using requirements, such as heat resistant water blocking and sand prevention for oil drilling, etc.
Owner:安徽比特海新材料股份有限公司

Sulfur-containing hyperbranched epoxy resin and preparation method thereof

The invention belongs to the technical field of epoxy resins and preparation method thereof and in particular discloses a sulfur-containing hyperbranched epoxy resin and a preparation method thereof. The preparation method comprises the following steps: stirring and reacting a trithiol compound and a diolefin compound at the temperature of 10 DEG C below zero and 20 DEG C for 2-5 hours and preparing an acrylate monomer with polyfunctionality; stirring and reacting the monomer and bithiol secondary amine at the temperature of 20-80 DEG C for 5-10 hours and obtaining a first generation mercapto-terminated hyperbranched polymer NP1-HSH; stirring and reacting the NP1-HSH and methacrylic acid glycidyl ester at the temperature of 10 DEG C below zero and 20 DEG C for 2-5 hours and obtaining a first generation sulfur-containing hyperbranched epoxy resin; and sequentially carrying out the previous three reactions on NP1-HSH to prepare a second-fourth generation sulfur-containing hyperbranched epoxy resin with the molecular weight of about 2,000-30,000 g/mol. The method is simple in process and low in reaction temperature, the obtained product can reduce the curing temperature and is expected to be applied to the fields of reinforcing and toughening of epoxy resins, solvent-free coatings and the like.
Owner:SOUTH CENTRAL UNIVERSITY FOR NATIONALITIES

Low temperature curing epoxy low-gloss powder coating and preparation method thereof

The invention discloses a low temperature curing epoxy low-gloss powder coating, which comprises the following components in part by weight: 100 to 200 parts of epoxy resin, 1 to 10 parts of epoxy curing agent, 0 to 50 parts of delustering agent, 0 to 160 parts of inorganic filling and 0 to 10 parts of addition agent. The invention also discloses a method for preparing the powder coating. The low temperature curing epoxy low-gloss powder coating has the characteristics of simple formula, low curing temperature, stable gloss and free adjustment of a coat, good mechanical properties, good chemical resistance and the like.
Owner:GUANGZHOU QINGTIAN INDAL

GMR angle sensor for vehicles

A GMR angle sensor for vehicles includes a GMR element in which the element resistance is changed in response to an external magnetic field, lead conductors connected to either end of the GMR element, and a protective layer that seals the GMR element and the lead conductors, wherein the protective layer has a laminated structure including an oxidation-resistant inorganic film that ensures that the GMR element and the lead conductors are sufficiently insulated and a silicone-based organic film laminated on the inorganic film.
Owner:ALPS ALPINE CO LTD
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