The invention discloses a preparation method of a
graphite crucible. The preparation method comprises the following steps: S1,
raw material preparation: raw materials comprise
graphite scraps, an Acheson furnace
petroleum coke resistance material, an Acheson furnace
petroleum coke thermal insulation material and medium-temperature
coal pitch; s2, burdening:
graphite is crushed and ground into graphite
powder, then the graphite
powder is mixed with the Acheson furnace
petroleum coke resistance material, the Acheson furnace
petroleum coke resistance material and the Acheson furnace
petroleum coke heat preservation material according to the
mass ratio of 3: 2: 5, the mixture is ground into mixed
powder, the mixed powder is mixed with medium-temperature
coal pitch, the
mass percent of the mixed powder in the mixing process is 65%-85%, and the medium-temperature
coal pitch is obtained; the
mass percent of the medium-temperature coal pitch is 15%-35%; s3, mixing and kneading; s4, profiling is conducted; s5,
roasting; and S6,
processing. A hot-pressing cold-out one-time forming method is adopted, the obtained product is excellent in performance and shows good
thermal shock resistance,
ablation performance, leakage-proof performance and
mechanical strength, and the preparation process has the advantages in the aspects of saving energy, protecting the environment, shortening the period and improving the aging efficiency.