Carbon / phenolic heat insulating composite material and manufacturing process thereof
A composite material and phenolic technology, which is applied in the field of heat-resistant composite materials and their processing, can solve the problems of unfavorable heat-resistant materials, etc., and achieve the effects of excellent ablation performance, good heat insulation and good comprehensive performance
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Embodiment 1
[0021] The carbon / phenolic heat-resistant composite material of the present invention uses viscose-based carbon fiber chopped fiber yarn as a reinforcement, and 616 aminophenolic resin as a matrix, wherein the weight percentage of the 616 aminophenolic resin is 35%. The carbon content of the chopped fiber yarn of viscose-based carbon fiber is 96% by weight, the tensile strength is 0.90GPa, the content of alkali metal or alkaline earth metal is 50μg / g, the linear density is 190tex, and the twist is 100 twist / m , The chopped length is 36mm. 616 aminophenol-formaldehyde resin, with ethanol as solvent, is the polycondensation product of phenol and formaldehyde, and the residual carbon rate of the resin is 59%.
[0022] The manufacturing process of the above-mentioned carbon / phenolic heat-resistant composite material, it is carried out successively according to the following steps:
[0023] (1) at first the chopped fiber yarn of viscose-based carbon fiber is mixed with 616 aminoph...
Embodiment 2
[0027] The carbon / phenolic heat-resistant composite material of the present invention uses viscose-based carbon fiber woven fabric as reinforcement and high-purity phenolic resin as a matrix, wherein the weight percentage of high-purity phenolic resin is 30%. The woven fabric of viscose-based carbon fiber has a carbon content of 95% by weight, a tensile strength of 0.80GPa, an alkali metal or alkaline earth metal content of 60μg / g, a linear density of 170tex, and a twist of 30 twists / m , the thickness is 0.5mm, and the width is 1.0m. The high-purity phenolic resin uses ethanol as a solvent and is a polycondensation product of phenol and formaldehyde, and the residual carbon rate of the resin is greater than 55%.
[0028] The manufacturing process of the above-mentioned carbon / phenolic heat-resistant composite material, it is carried out successively according to the following steps:
[0029] (1) first the woven cloth of viscose base carbon fiber is immersed in the high-purity...
Embodiment 3
[0033] The carbon / phenolic heat-resistant composite material of the present invention uses viscose-based carbon fiber chopped fiber yarn as reinforcement and magnesium phenolic resin as matrix, wherein the weight percentage of magnesium phenolic resin is 32%. The carbon content of the chopped fiber yarn of viscose-based carbon fiber is 95% by weight, the tensile strength is 0.80GPa, the content of alkali metal or alkaline earth metal is 100μg / g, the linear density is 80tex, and the twist is 120 twist / m , The chopped length is 24mm. Magnesium phenolic resin, using methanol as a solvent, is a polycondensation product of phenol and formaldehyde, and the carbon residue rate of the resin is 55%.
[0034] The manufacturing process of the above-mentioned carbon / phenolic heat-resistant composite material, it is carried out successively according to the following steps:
[0035] (1) first the chopped fiber yarn of viscose-based carbon fiber is mixed with magnesium phenolic resin to ma...
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