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Preparation method for glass fiber

A glass fiber and fiber technology, which is applied in the field of glass fiber preparation, can solve problems such as poor performance of composite materials, and achieve the effects of low material cost, short process and uniform color.

Inactive Publication Date: 2017-08-11
合肥钢骨玻璃制品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the composite material is made by mixing two or more materials together through an auxiliary method, there is often a phase interface between the materials due to different properties, which will eventually cause changes in the shear force between the interface layers. Composite materials perform poorly

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A kind of preparation method of glass fiber, comprises the following steps:

[0025] 1. Mix and melt silicon dioxide, aluminum oxide, calcium oxide, magnesium oxide, titanium dioxide, iron oxide, sodium oxide, potassium oxide and nickel oxide at a temperature of 2200 ° C, and then draw to make a rough fiber;

[0026] 2. Put the crude fiber product into the muffle furnace, remove the moisture adsorbed on the surface of the glass fiber, soak the crude fiber product in NaOH solution for 30 minutes, take it out and wash it with distilled water until neutral, then immerse the crude fiber product in dilute HCl, Soak for 30 minutes, take it out and wash it with distilled water until neutral, place it in an oven and dry it at 180°C to obtain a refined glass fiber product;

[0027] 3. Soak the refined glass fiber in NaOH solution with a mass fraction of 15% for 10 minutes, take it out, wash it with distilled water until neutral, take it out and disperse it in anhydrous ethanol w...

Embodiment 2

[0038] A kind of preparation method of glass fiber, comprises the following steps:

[0039] 1. Mix and melt silicon dioxide, aluminum oxide, calcium oxide, magnesium oxide, titanium dioxide, iron oxide, sodium oxide, potassium oxide and nickel oxide at a temperature of 1800°C, and then draw to make rough fiber;

[0040] 2. Put the crude fiber product into the muffle furnace, remove the moisture adsorbed on the surface of the glass fiber, soak the crude fiber product in NaOH solution for 17 minutes, take it out and wash it with distilled water until neutral, then immerse the crude fiber product in dilute HCl, Soak for 30 minutes, take it out and wash it with distilled water until neutral, place it in an oven and dry it at 180°C to obtain a refined glass fiber product;

[0041] 3. Soak the refined glass fiber in NaOH solution with a mass fraction of 10% for 10 minutes, take it out, wash it with distilled water until neutral, take it out and disperse it in anhydrous ethanol with ...

Embodiment 3

[0052]A kind of preparation method of glass fiber, comprises the following steps:

[0053] 1. Mix and melt silicon dioxide, aluminum oxide, calcium oxide, magnesium oxide, titanium dioxide, iron oxide, sodium oxide, potassium oxide and nickel oxide at a temperature of 2200 ° C, and then draw to make a rough fiber;

[0054] 2. Put the crude fiber product into the muffle furnace, remove the moisture adsorbed on the surface of the glass fiber, soak the crude fiber product in NaOH solution for 30 minutes, take it out and wash it with distilled water until neutral, then immerse the crude fiber product in dilute HCl, Soak for 40 minutes, take it out and wash it with distilled water until neutral, place it in an oven and dry it at 200°C to obtain a refined glass fiber product;

[0055] 3. Soak the refined glass fiber in NaOH solution with a mass fraction of 15% for 20 minutes, take it out, wash it with distilled water until neutral, take it out and disperse it in anhydrous ethanol wi...

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Abstract

The invention relates to a preparation method for glass fiber. The method comprises the following steps: 1) mixing and fusing raw materials, and wiredrawing to form a crude fiber product; 2) putting the crude fiber product into a muffle furnace, removing water attached to the glass fiber surface, and then performing acid-base immersion cleaning, thereby acquiring a refined glass fiber product; 3) soaking the refined glass fiber product into a NaOH solution and then taking out, washing with distilled water, taking out and dispersing in absolute ethyl alcohol of a coupling agent KH570, regulating pH and dispersing with an ultrasonic meter, thereby acquiring a semi-finished product of glass fiber; 4) removing surface alkali liquor by spraying the surface of the semi-finished product of glass fiber with warm water, then soaking in clean water, and washing with the assistance of a hot water pump till the pH value is less than 6, thereby acquiring a to-be-finished product of glass fiber; 5) performing thermal shaping treatment on the to-be-finished product of glass fiber, and performing gumming, grouting and drying on the surface, thereby acquiring the end product. The preparation method has the advantages of simple structure, low cost and suitability for large-scale industrial manufacturing.

Description

technical field [0001] The invention belongs to the technical field of glass fiber production, and in particular relates to a glass fiber preparation method. Background technique [0002] With the continuous development of the economy, the demand for glass fiber in industrial smelting, welding and other industries has increased sharply. At present, some alkali-free glass fibers are used, which have a very short life and poor heat insulation. Damaged, thereby endangering personal safety, its acid and alkali resistance, rigidity, anti-aging, high temperature resistance properties need to be improved. [0003] Among many polymer composite materials, fiber-reinforced composite materials have attracted widespread attention because of their excellent comprehensive properties, such as high impact resistance, high modulus, high mechanical properties, and high wear resistance. Glass fiber has the advantages of good corrosion resistance, heat resistance, good mechanical strength, and...

Claims

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Application Information

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IPC IPC(8): C03B37/022C03C25/66
CPCC03B37/022C03C25/66
Inventor 朱明静
Owner 合肥钢骨玻璃制品有限公司
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