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205results about How to "Excellent thermal" patented technology

Pentasil-type molecular sieve containing composition and its preparation method

A molecular sieve containing composition, which can be applied in catalytic cracking reaction for producing more ethylene and propylene, and its preparation method. The composition contains a pentasil-type molecular sieve having a SiO2 / Al2O3 molar ratio of 15-60, prepared by activation and modification with phosphorus, alkaline earth metal and transition metal. The composition essentially includes 85 DIFFERENCE 98% wt of pentasil-type molecular sieve, 1 DIFFERENCE 10% wt of P2O5, 0.3 DIFFERENCE 5% wt of alkaline earth oxide, and 0.3 DIFFERENCE 5% wt of transition metal oxide. The molecular sieve structure and active centers have high thermal and hydrothermal stability. The salient feature of this composition is that when applied as an active component of cracking catalyst for catalytic pyrolysis process, the yield of ethylene is above 18% and the total yield of ethylene and propylene is more than 40%.
Owner:CHINA PETROCHEMICAL CORP +1

Ce:YAG microcrystalline glass used for white light LED and preparation method of Ce:YAG microcrystalline glass

ActiveCN103183473AUnique material compositionHigh transparencyFluorescenceGlass matrix
The invention provides Ce:YAG microcrystalline glass capable of achieving yellow luminescence under the condition of blue light excitation and a preparation method of the Ce:YAG microcrystalline glass, and Ce:YAG fluorescence microcrystals are inlaid uniformly in an oxide glass matrix of the microcrystalline glass. The microcrystalline glass comprises glass components in percentage by mole as follows: 0-10 mol% of SiO2, 0-40 mol% of GeO2, 20-60 mol% of TeO2, 0-25 mol% of B2O3, 0-15 mol% of P2O5, 0-10 mol% of Al2O3, 0-20 mol% of Ae2O, 0-20 mol% of ZnO, 0-15 mol% of BaO, 0-20 mol% of Sb2O3, 0-20 mol% of La2O3 and 0-10 mol% of Bi2O3, wherein Ae is selected from Li, Na or K; and the content of Ce:YAG microcrystals is 1-15 wt% of the oxide glass matrix. The invention further provides a preparation method for the microcrystalline glass. The microcrystalline glass provided by the invention can emit yellow light under the excitation of blue light, the yellow light and the blue light are combined to generate intense white light, and accordingly, the microcrystalline glass and the method can be used for development and application of construction of the white light LED which is excited by a blue light chip.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Method for effectively preparing high-orientation and high-compactness two-dimensional material thin film

The invention relates to the field of preparation and application of two-dimensional materials, in particular to a method for effectively preparing a high-orientation and high-compactness two-dimensional material thin film. The method comprises the following steps: taking a circular tube with a smooth inner surface as a casting die; pouring a solution which contains a two-dimensional material intothe die when the die rotates in the peripheral direction at high speed; uniformly coating the inner surface of the die with the solution by using centrifugal force; forming shear force which drives the two-dimensional material to be regularly arranged layer by layer in an oriented manner in the peripheral direction in the solution in a centrifugal rotating process; and meanwhile, driving the two-dimensional material to be accumulated at high compactness by the centrifugal force so as to obtain the two-dimensional material thin film with high orientation and high compactness. The method is suitable for preparing various two-dimensional materials such as graphene, and composite thin films and laminated heterostructure thin films of the two-dimensional materials; electric property, heat property, mechanical property and the like of the thin film are greatly improved; and the method is used in the field of high-performance electric conduction / heat-conduction thin films, heat management materials, high-strength thin films, electronic / optoelectronic devices, compact energy storage, gas / ion separating films, proton transmitting films and the like.
Owner:深圳烯材科技有限公司

High flux sapo-34 membranes for co2/ch4 separation and template removal method

The present invention provides methods for making improved zeolite and crystalline silicoaluminophosphate (SAPO) membranes, in particular SAPO-34 membranes, on a porous support through improved removal of the organic structure-directing templating agent. A calcining step is performed in an oxygen free atmosphere, such as under a vacuum or inert gas, to remove the organic templating agent. By removing the templating agent in the absence of oxygen, the calcination step can remove a greater amount of the templating agent than comparable template removal steps conducted in the presence of oxygen and the calcination step can be conducted at significantly lower temperatures. The membranes of the present invention provide increased permeance while maintaining comparable selectivity for gas separations, particularly carbon dioxide (CO2) and methane (CH4) separations and separations at high temperatures.
Owner:UNIV OF COLORADO THE REGENTS OF

Innoxious negative ion aqueous polyurethane and preparation method thereof

The invention discloses a preparation method of innoxious negative ion aqueous polyurethane, and aqueous polyurethane prepared by the method. The method comprises the following steps: mixing dicyclohexyl methane diisocyanate and aliphatic diol according to a mol ratio of 2.5 to 4; carrying out reaction for 3 to 5 hours at 70 to 90 DEG C to obtain performed polymers; adding dimethylolbutyric acid with hydrophilic groups for taking the reaction for 3 to 5 hours; adding KOH water solution for emulsifying dispersion; and dripping diamine chain extenders for extending chains to obtain aqueous polyurethane latex emulsion. The invention adopts the aliphatic diisocyanate dicyclohexyl methane diisocyanate resin and the aliphatic polymeric diol, does not contain organic solvents such as NMP, acetone and the like often used for preparing the aqueous polyurethane, and does not contain common use neutralizing agents such as triethylamine and the like. The completely innoxious polyurethane material can be prepared, and the invention can be widely used in the fields of medical and health, food and household articles.
Owner:WANHUA CHEM GRP CO LTD

Method for fabricating round and smooth curved surface microstructure

The invention discloses a method for fabricating a round and smooth curved surface microstructure, which is characterized by comprising the following steps: taking a negative chemically amplified photoresist as a material for fabricating the round and smooth curved surface microstructure; firstly carrying out spin coating of the first layer of the negative chemically amplified photoresist on a substrate, soft baking and exposing, and then directly carrying out spin coating of the second layer of the negative chemically amplified photoresist on the first layer of the negative chemically amplified photoresist, and post-baking; and catalyzing photoresist molecules for cross-linking in an exposure area and an adjacent diffusion area thereof by isotropic diffusion of photo acid generated afterexposure of the first layer of the photoresist during the post-baking process, and developing the cross-linked photoresist molecules to obtain the microstructure with round and smooth curved surface characteristics. Relative to the traditional gray scale mask technology and the traditional photoresist reflowing method, the method for fabricating the round and smooth curved surface microstructure has the characteristics of simple processing, low cost, stable structure and the like.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Electrochemical biosensor for detecting hydrogen peroxide, preparation method and application thereof

The present invention relates to an electrochemical biosensor for detecting hydrogen peroxide, a preparation method and an application thereof. The preparation method comprises the steps of (1) synthesizing the silica-three-dimensional graphene composite material; (2) doping nitrogen and carbon into the synthesized silica-three-dimensional graphene composite material; (3) pretreating a glassy carbon electrode; (4) preparing the glassy carbon electrode modified by the nitrogen-carbon-doped silica-three-dimensional graphene composite material through the dispensing method; (5) putting the glassy carbon electrode into a chloroauric acid solution to prepare gold nanoparticle-nitrogen-carbon-doped silica-three-dimensional graphene glassy carbon electrode through chronoamperometry; (6) dipping the glassy carbon electrode into a double-sulfhydryl-modified GDNA solution and cultivating for 2-4 hours; (7) dipping the composite electrode into a hemin solution for 10-14 hours. The electrochemical biosensor is good in stability and reproducibility, high in specificity and sensitivity, fast and simple and convenient to operate. The electrochemical biosensor can be used for detecting the content of hydrogen peroxide in biological samples, cosmetics and the like.
Owner:广东省汕头市质量计量监督检测所

Carbon nanometer tube field emitting cathode and manufacturing method thereof

The invention relates to a carbon nanometer tube field emitting cathode and a manufacturing method thereof. The carbon nanometer tube field emitting cathode comprises a conductive substrate, a grapheme layer and a carbon nanometer tube layer, wherein the grapheme layer and the carbon nanometer tube layer are sequentially stacked on the conductive substrate. The theory ratio surface area of grapheme reaches up to 2600m<2> / g, the unique two-dimensional structure of the carbon nanometer tube field emitting cathode can conduct effective electric heat transmission, more excellent thermotics and electrics performance is obtained compared with a carbon nanometer tube, the grapheme layer is arranged between the conductive substrate and the carbon nanometer tube layer, the characteristics of the large grapheme ratio surface area and excellent conductive heat dissipation are brought into full play, adhesive force of the carbon nanometer tube layer can be improved, and an emission current and stability are improved.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Er<3+>/Yb<3+> co-doped yttrium lithium fluoride monocrystal and preparation method thereof

InactiveCN102978701AHigh phonon energyPhonon energy low highPolycrystalline material growthFrom frozen solutionsWater vaporOxygen
The invention discloses an Er<3+>/Yb<3+> co-doped yttrium lithium fluoride monocrystal and a preparation method thereof. The yttrium lithium fluoride monocrystal is a rare earth ion Er<3+>/Yb<3+> co-doped monocrystal; the molecular formula is LiY(1-x-y)ErxYbyF4, wherein x is greater than or equal to 0.008 and less than or equal to 0.085, and y is greater than or equal to 0.002 and less than or equal to 0.170; the segregation coefficients of Yb<3+> and Er<3+> in the yttrium lithium fluoride are about 1, and efficient intermediate infrared laser of 2.7 microns can be output; and the yttrium lithium fluoride monocrystal has high transmittance of intermediate infrared laser, has better thermal, mechanical and chemical stabilities than those of glass state materials and has the characteristics of low phonon energy, high optical transmittance of wavebands with width of 300-5500nm, less color center forming amount, low thermal lens effect and the like, thereby being more easily processed and more suitably used in laser devices. In the preparation method disclosed by the invention, a sealing crucible falling technology is used, so that the operation is simple; the raw material is fluorated at high temperature in a sealed water-free and oxygen-free environment, so that the crystal is isolated from air and water vapor during the growth; and therefore, the high-quality Er<3+>/Yb<3+> co-doped LiYF4 monocrystal containing little OH<-> ion and oxide is obtained.
Owner:NINGBO UNIV

Nanometer photo-catalyst used in producing hydrogen by decomposing water under visible light response and application of nanometer photo-catalyst

The invention discloses a nanometer photo-catalyst used in producing hydrogen by decomposing water under visible light response and application of the nanometer photo-catalyst. The catalyst is a nanocomposite which is formed by taking a one-dimensional organic semiconductor nanofiber as a framework, coating the surface of the framework with an inorganic semiconductor titanium dioxide nanolayer and uniformly loading platinum nanoparticles, wherein the organic semiconductor nanofiber is prepared by self-assembling super molecules of perylene diimide and cycle-expanding derivatives, naphthalene diimide derivatives or hexabenzobenzene diimide derivatives with the photochemical stability, D-A structures and visible light response, then titanium dioxide is directly loaded in situ in a body phase organic solution and platinum is reduced and deposited through ultraviolet light in a photo-catalysis aqueous solution system. The catalyst is novel in structure, low in cost and available; the preparation process of the catalyst is simple, environmentally-friendly, low in energy consumption and suitable for preparation in scales; the catalyst is capable of decomposing water in the visible light to prepare the hydrogen, has the actual and wide application prospects in preparation of the hydrogen through decomposing the water in solar light and provides a novel idea and an important reference for forming an efficient photo-catalyst responding to the visible light.
Owner:XINJIANG TECHN INST OF PHYSICS & CHEM CHINESE ACAD OF SCI

Method for preparing in-situ grown carbon nano tube reinforced silver-based electric contact material

The invention relates to preparation methods for electric contact materials, in particular to a method for preparing an in-situ grown carbon nano tube reinforced silver-based electric contact material. The method aims to solve the technical problems that when a common CNTs / Ag composite material preparation method is adopted, carbon nano tubes are not dispersed uniformly, and a large number of structural defects exist. The method comprises the steps that firstly, Ni(NO3)2 / Ag composite powder is prepared; secondly, a plasma method is adopted for preparation of the electric contact material. According to the method, since the plasma reinforced chemical vapor deposition method is adopted for low-temperature in-situ growth of the carbon nano tubes, structural perfection and uniform dispersity of the carbon nano tubes in silver powder are guaranteed, clustering of the carbon nano tubes in CNTs / Ag-based electric contact composite powder is avoided, and the improvement on the performance of the CNTs / Ag-based electric contact composite powder by the carbon nano tubes is realized in a true sense. The method is used for preparing the in-situ grown carbon nano tube reinforced silver-based electric contact material.
Owner:HARBIN INST OF TECH
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