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516 results about "Sodium peroxide" patented technology

Sodium peroxide is the inorganic compound with the formula Na₂O₂. This yellowish solid is the product of sodium ignited in excess oxygen. It is a strong base. This metal peroxide exists in several hydrates and peroxyhydrates including Na₂O₂·2H₂O₂·4H₂O, Na₂O₂·2H₂O, Na₂O₂·2H₂O₂, and Na₂O₂·8H₂O. The octahydrate, which is simple to prepare, is white, in contrast to the anhydrous material.

Oxygen fertilizer and preparation and application methods thereof

The invention discloses a novel oxygen fertilizer and preparation and application methods of the oxygen fertilizer. Mixtures of one or more of calcium peroxide, sodium peroxide and magnesium peroxide act as a core; nano chitosan doped with sodium alginate as the binding agent serves as a wrapping membrane; and the outer layer of the wrapping membrane is further wrapped by paraffin as a conditioner, so that a slow-release oxygen fertilizer is prepared. The oxygen fertilizer contains 70-75% of the core by weight, 20-25% of the wrapping membrane by weight, and 3-10% of the conditioner by weight and the particle diameter of the oxygen fertilizer particles is 3-10mm. The novel oxygen fertilizer prepared by the preparation method disclosed by the invention can supply oxygen to waterlogged plants for a long time and is convenient and simple to apply, simple in production process and environment-friendly, and saves time and labor and can be used widely.
Owner:CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY

Sodium ion doped high-nickel ternary lithium battery positive electrode material and preparation method

The invention provides a sodium ion doped high-nickel ternary lithium battery positive electrode material and a preparation method. The preparation method comprises the following steps: preparing an 811-type NCM (Nickel Cobalt Manganese) ternary positive electrode precursor through a co-precipitation method; after drying and grinding the precursor, mixing the ground precursor with powdery sodium peroxide and lithium oxide; pre-firing and sintering under an oxygen-rich environment to prepare the sodium ion doped high-nickel ternary lithium battery positive electrode material. According to the method provided by the invention, the defects that Ni<2+> is difficulty effectively controlled to be released from and embedded into a lamellar structure in a sintering process so that a structure is changed in a desorption process and the capacity of lithium ions is reduced are effectively overcome; sodium peroxide is changed into a molten state in a pre-firing process and permeates into the precursor, so that the Ni<2+> is oxidized into Ni<3+>; meanwhile, a lithium layer is occupied and an interlayer structure is expanded; the Ni<2+> is prevented from being migrated into the lithium layer ina sintering process; technical effects that nickel and lithium mixed arrangement of the high-nickel NCM positive electrode material is reduced, the migration rate of lithium ions is improved and the circulating performance of the battery is improved are realized.
Owner:CHENDU NEW KELI CHEM SCI CO LTD

All-solid-state integrated pH composite electrode device and preparation method of electrode

The invention relates to an all-solid-state integrated pH composite electrode device and a preparation method of the electrode. The all-solid-state integrated pH composite electrode device comprises an Ag/AgCl reference electrode, an antimony electrode, a copper wire and an insulated rubber sleeve, wherein the antimony electrode is embedded at the bottom of a stainless steel hollow needle of the reference electrode through the insulated rubber sleeve; the reference electrode is formed by taking the stainless steel hollow needle as a substrate, electroplating a silver layer on the surface, performing ultrasonic cleaning by using deionized water, plating an AgCl layer on the surface, cleaning through deionized water, and finally coating the reference electrode by using perfluorinated sulfonic acid resin solution dissolved with supersaturated KCl; the antimony electrode is formed by oxidizing a common antimony electrode in molten sodium peroxide to form an oxidation layer film, coating the antimony electrode by using the perfluorinated sulfonic acid resin solution with the mass percent of 5-10 percent and forming a hydrogen ion selective semi-permeable membrane. The composite electrode has certain mechanical strength and piercing ability, and pH of solids, semi-solids, paste and solutions can be tested.
Owner:JIANGSU UNIV

Method and equipment for mineralizing and degrading organic wastewater

The invention relates to a method and equipment for mineralizing and degrading organic wastewater, and belongs to the fields of chemical industry and environment. The equipment comprises a catalyst and wastewater treatment equipment which uses the catalyst. The catalyst for treating the wastewater comprises elementary substances such as palladium, rhodium, manganese, cobalt, copper, potassium, silver, lanthanum, iron, nickel, tungsten, ruthenium, titanium, cerium, sodium, osmium, gold, platinum, calcium, oxygen, bismuth and the like and oxide, superoxide, hyperoxide, halide, nitrate, sulfate,nitrite, carbonate, hydroxide, phosphate and the like thereof; the catalyst also comprises ozone, hydrogen peroxide, oxygen, sodium superoxide, sodium dioxide, calcium peroxide and calcium superoxide,and can be separately used or combined for use; and the dosage of the catalyst is 0.01g to 100Kg/ton. The wastewater treatment equipment mainly comprises a container, a water inlet pipe, a water outlet pipe, a valve, an ultraviolet lamp, a quartz tube, an aerator and an air pump. The catalyst and the wastewater are added into the container of the water treatment equipment through the water inletpipe at the top of the water treatment equipment; and the organic wastewater is treated through lighting catalysis. The method for treating the organic wastewater does not produce silt, and secondarypollutants. The equipment is simple and easy for operation.
Owner:武钦佩

Method for mineralizing and degrading organic waste water and processing equipment

The invention relates to a method for mineralizing and degrading organic waste water and processing equipment, which belong to the field of chemistry and environment. The method uses a catalyst and waste water treatment equipment using the catalyst. The catalyst for use in waste water treatment comprises simple substances such as palladium, rhodium, manganese, cobalt, copper, potassium, silver, lanthanum, iron, nickel, tungsten, ruthenium, titanium, cerium, sodium, osmium, gold, platinum, calcium, oxygen and bismuth as well as oxides, peroxides, superoxides, halides, nitrates, sulfates, nitrites, carbonates, hydroxides, phosphates and the like of the simple substances, and the catalyst also comprises ozone, hydrogen peroxide, oxygen, sodium superoxide, sodium dioxide, calcium peroxide andcalcium superoxide. The catalyst can be used alone or in combination at a dosage of 0.01 to 60 kilograms per ton. The catalyst and waste water are filled in a container in the water treatment equipment from a water inlet pipe on the top part of the water treatment equipment; and organic waste water is treated by photocatalysis. The method for treating the waste water does not generate silt and secondary pollution. The equipment is simple and easy to operate.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

Method for preparing sodium chromate by mixing chromite and ferrochrome and device for method

The invention discloses a method for preparing sodium chromate by mixing chromite and ferrochrome and a device for the method. The method comprises the following steps: measuring and mixing chromite and ferrochrome with sodium carbonate, sodium nitrate and sodium peroxide; pelleting the mixture with extracted liquid sodium chromate in a pelletizer; drying in a drier; returning part of the clinker to a flame kiln after the material is dried and cooled, so that chromite and ferrochrome are decomposed and oxidized in the form of fused liquid phase in molten salts so as to obtain the clinker of sodium chromate; and continuously soaking, filtering and cleaning after the clinker is cooled so that a chromium chemical primary product of liquid sodium chromate is obtained, wherein the flame kiln comprises a U-shaped kiln body, a partition wall and a low-position molten salt suction port, wherein the partition wall and the low-position molten salt suction port are arranged in the U-shaped kiln body; one or more blowing oxygen lances and one or more charging holes are arranged at the top of the kiln body, and a smoke outlet is arranged on the upper side of the kiln; and one or more oxygen lances are arranged at the bottom of the kiln. According to the method disclosed by the invention, the oxidation rate is as high as 98%, the clinker extraction rate is as high as 99.97%, and the chromium yield is 97.96%.
Owner:HUBEI POLYTECHNIC UNIV

Method for measuring niobium content in tungsten carbide added with niobium or simultaneously added with tantalum and niobium

The invention relates to a method for measuring a niobium content in tungsten carbide added with niobium or simultaneously added with tantalum and niobium, which comprises the following analytical steps that: after a sample is ground and sieved, the obtained product is melted by sodium peroxide, and the product is leached by hot water; after twice precipitations are carried out on the leached solution by using a coprecipitator to precipitate and using a gallotannic acid to precipitate, niobium or niobium and tantalum are separated from the main tungsten and other impurities, and then tartaric acid solution is prepared; when the prepared tartaric acid solution is in the sulphuric acid medium, the niobium and 5-Br-PADAP form a red chelate, the color depth is in positive proportion to the niobium content, hereby, the niobium content can be measured by photometry according to the working curve of the niobium; and if the sample comprises the niobium and tantalum simultaneously, the interference of tantalum to the measurement of the niobium content is eliminated by a method of adding excessive solution of high-concentration tartaric acid to carry out complexing and screening. The method of the invention has high precipitate recovery rate, simple and convenient operation, small interference, and good accuracy and repeatability.
Owner:JIANGXI RARE EARTH & RARE METALS TUNGSTEN GRP

Method for determining content of phosphorus in ferroniobium

The invention provides a method for determining the content of phosphorus in ferroniobium. The method comprises the steps of melting anhydrous sodium carbonate, sodium peroxide and ferrocolumbium, cooling, adding perchloric acid, leaching, heating and boiling until a black muddy solution is changed to a green muddy solution; adding a sodium hydroxide solution and heating until boiling to obtain a mother solution; adding perchloric acid in the mother solution, adding a bismuth salt solution, a sodium thiosulfate solution and an ammonium molybdate mixed solution to enable the phosphorus in the mother liquid, bismuth ions and ammonium molybdate to react in a perchloric acid medium to generate phosphorus-bismuth-molybdenum heteropolyacid, wherein bismuth salt is dissolved in the perchloric acid and the solution is heated until dense perchloric acid smoke occurs, and therefore, the bismuth salt solution is obtained, and the ammonium molybdate mixed liquid is prepared from perchloric acid, ammonium molybdate and arabic gum; adding ascorbic acid to perform reduction reaction to obtain bismuth phosphomolybdenum blue containing a solution to be tested; and measuring the absorbancy of the bismuth phosphomolybdenum blue in the solution to be tested by adopting a spectrophotometric method and calculating the content of the phosphorus. The method is convenient to operate and can accurately determine the content of the phosphorus in the ferroniobium.
Owner:PANGANG GROUP JIANGYOU CHANGCHENG SPECIAL STEEL

Method and device for disinfecting, detoxifying and purifying water by using hydroxyl radicals

The invention relates to a method and a device for disinfecting, detoxifying and purifying water by using hydroxyl radicals. The method and the device mainly solve the technical problems that the existing water treatment method and the existing water treatment device cannot remove residual carcinogenic substances in water, and cannot remove overproof heavy metal and organic compounds. The method adopts the technical scheme that the method comprises the following steps that ozone is released to treated water; singlet-state atomic oxygen is generated through radiation of a plurality of mercury lamp ultraviolet lamp modules at UVC (ultraviolet C) 253.7nm or a plurality of LED (light-emitting diode) ultraviolet lamp modules at DUV (deep ultraviolet) LED 280nm; drinking water is continuously disinfected, detoxified and purified, so that the drinking water reaches a sanitary standard for domestic drinking water, and then is discharged; or reclaimed water of waste water is recycled; and zero discharge is reached. The device using the method comprises an ozone generator, an impeller, an aerator, a housing, the ultraviolet lamp modules, an ultrasonic device, a water inlet, a water outlet, an oxygen outlet, a sodium peroxide generation machine, a sodium peroxide collection tank and a sodium peroxide discharge pipe.
Owner:刘传林

Method for decomposing pesticide residues on fruits and vegetables and disinfecting tableware through hydroxyl radical and device adopting method

The invention relates to a method for decomposing pesticide residues on fruits and vegetables and disinfecting tableware through hydroxyl radical and a device adopting the method, and mainly aims to solve the technical problems that the conventional fruit, vegetable, tableware and medical instrument disinfection method and the conventional fruit, vegetable, tableware and medical instrument disinfection device are low in pesticide residue removal efficiency, and poor in innocent treatment effect and medical instrument disinfection effect. According to the technical scheme disclosed by the invention, the method comprises the following steps of releasing ozone into water, irradiating the water through a UVC 253.7nm mercury lamp and ultraviolet lamp module to generate singlet elemental oxygen for blowing up the water to generate a high-concentration hydroxyl radical aqueous solution for disinfecting, detoxifying and purifying the pesticide residues on the fruits, the vegetables and fresh food or disinfecting tableware and medicament instruments. The device disclosed by the invention comprises an ozone generator, an impeller, an aerator, a shell, the ultraviolet lamp module, an ultrasonic device, a water outlet, a water inlet, a water pump, an oxygen outlet, a sodium peroxide generator, a sodium peroxide collection tank, a sodium peroxide discharging pipe, a hanging mechanism, and a closing cover.
Owner:刘传林

Method for Determining Vanadium Content in a Tungsten Matrix with Added Vanadium or Simultaneously Added Chromium and Vanadium

A method for determining vanadium content in a tungsten matrix with singly added vanadium or simultaneously added chromium and vanadium, characterized in that a test sample is subjected to alkaline melting with sodium peroxide and water leaching followed by dry filtering, the chromium and vanadium in the filtrate are firstly reduced to low valences by a reducing agent, i.e. hydroxylamine hydrochloride, then the filtrate is adjusted to an acidity of 4-6 M with nitric acid, the vanadium is oxidized in a cold state to a high valence by potassium permanganate, and the high-valent vanadium forms a ternary complex with tungstate and orthophosphate, the darkness of the color of the ternary complex is directly proportional to the vanadium content, thus the vanadium content is determined colorimetrically, and the interference of chromium is eliminated with the fact that the potassium permanganate in a cold state in the acidic condition for vanadium determination oxidizes the vanadium but not the chromium. The method of the invention is relatively suitable for determining the macro-amount vanadium content in a tungsten matrix containing macro-amount vanadium singly or containing macro-amount vanadium and chromium simultaneously, the method is fast and accurate with a relative error less than 5%, which can fully satisfy the requirements of the production process for the determination.
Owner:HU YIQI

Method for simultaneously determining iodine, boron, tin and germanium elements in soil

The invention discloses a method for simultaneously determining iodine, boron, tin and germanium elements in soil. The method comprises the following steps of pre-treating raw materials, preparing a determination solution, drawing a working curve and determining the content of each element in the soil, wherein the step of pre-treating the raw materials comprises the step of pre-treating with sodium oxide; a citric acid solution and cation resin are added into the pre-treated sample to prepare the determination solution; the obtained determination solution is determined by adopting an inductively coupled plasma-mass spectrometry. The method disclosed by the invention can be used for simultaneously determining the plurality of elements including iodine, boron, tin and germanium in the soil, and is high in working efficiency and simple to operate; the inductively coupled plasma-mass spectrometry is used for determining; compared with an inductively coupled plasma emission spectroscopy, the method has the advantages of relatively high sensitivity, relatively low detection limit, relatively strong anti-interference capability, relatively high precision and the like. The detection limits of the detected elements that the iodine is 0.10Mug / g, the boron is 0.92Mu g / g, the tin is 0.29Mu g / g and the germanium is 0.02Mug / g, and are lower than the detection limits of the inductively coupled plasma emission spectroscopy.
Owner:广西壮族自治区地质矿产测试研究中心

Composite oxygen producer for adsorbing residual antibiotics in aquaculture water and preparation method thereof

The present invention belongs to the field of aquaculture technology, and discloses a method for preparing a composite oxygen producer for adsorbing residual antibiotics in aquaculture water. The composite oxygen producer is prepared from the following components by weight: 70-90 parts of an oxygen supply component, 15-25 parts of a traditional Chinese medicine compound, 42-68 parts of an adsorption component, 2 -5 parts of a coating agent, 1-3 parts of a stabilizer and 1.3-1.8 parts of a sustained co-solvent. The oxygen supply component comprises 50-60 parts of sodium peroxide and 20-30 parts of calcium peroxide; the traditional Chinese medicine compound includes celandine, Chinese angelica, Radix Astragali, nephelium lappaceum, receptaculum nelumbinis, fruticose breynia juvenile branchlet and leaf, Hydrangea aspera Don and yucca; the adsorption component comprises 20-30 parts of Chinese medical stone, 6 -10 parts of a polymer material, 9-15 parts of diatomaceous earth and 7-13 parts of silica powder. Through compounding of a plurality of effective components, the obtained product has good oxygenation function and residual antibiotic adsorption function.
Owner:SOUTH CHINA UNIV OF TECH

Method for measuring phosphorus content in chromite

The invention relates to a method for measuring phosphorus content in chromite. According to the method, a chromite sample is decomposed by high-temperature alkali fusion of sodium peroxide, the melt is extracted by hot water, phosphorus co-precipitates with elements such as iron, magnesium, manganese and the like, chromium enters the solution in a form of CrO4<2->, sodium hydroxide solution is used for washing so as to remove the chromium. The precipitate is subjected to acidolysis by hydrochloric acid and the precipitate subjected to acidolysis is then transferred into a volumetric flask. The test solution is separated, the pH value of the solution is adjusted by taking paranitrophenol as an indicator, phosphorus-molybdenum heteropoly acid is reduced to be phosphomolybdenum blue by taking ascorbic acid as a reducing agent in hydrochloric acid medium, and the light absorption value of the test solution is measured at the position of 680nm of a spectrophotometer. According to the technical scheme of the method, the design is reasonable, the relative standard deviation is less than 12%, and the recovery rate of standard addition reaches up to 96-99%; compared with the standard sample reference value, the method has the advantages that the analysis data is basically identical, the results are stable and accurate, simplicity and convenience are realized, and the operability is high.
Owner:BLUESTAR LEHIGH ENG INST CO LTD

Greasy dirt flocculation deoiling device for industrial sewage

The invention discloses a greasy dirt flocculation deoiling device for industrial sewage. The invention belongs to the technical field of sewage treatment. Upper elliptic adsorption layers coating thebottom end parts of adsorption floating balls are used for adsorbing greasy dirt flocculation particles on the water surface. After the flocculation operation is finished, sewage is discharged, the adsorption floating balls sink and abut against filtering oil guide mechanisms, meanwhile, an electric push rod presses down a sealing plate to enable the sealing plate to abut against the adsorption floating balls again, an electromagnet is electrified to magnetically attract a magnetic sealing cover plate, the electric push rod resets upward, the magnetic sealing cover plate and a gas stamping mechanism are pulled upwards, the gas stamping mechanism is separated from the filter holes of elliptic floating balls, sodium peroxide in the elliptic floating balls is diffused outwards to the upper elliptic adsorption layers through the filter holes, sodium peroxide powder generates sodium hydroxide and oxygen which can decompose greasy dirt particles when encountering water, the oxygen is used for scattering condensed particles to enable the greasy dirt particles to fall off easily, the gas stamping mechanism releases gas after being pulled to be broken, and the diffusion degree of the sodium peroxide powder is effectively improved.
Owner:施德琴

Auto cooling fluid

The invention discloses auto cooling fluid, comprising the following raw materials in parts: 10-18 parts of diethylene glycol, 11-14 parts of oxalic acid, 13-15 parts of 1,2-propylene glycol, 12-15 parts of ethylene glycol ethyl ether acetate, 8-12 parts of triethyl phosphonoacetate, 8-12 parts of glufosinate-ammonium, 5-8 parts of N-(phosphonomethyl)iminodiacetic acid, 6-8 parts of styrene-acrylic-triazole, 6-7 parts of 1-hydroxybenzotriazole, 6-9 parts of benzotriazole, 2-3 parts of dimeticone, 1-3 parts of hydroxyl silicone oil, 3-4 parts of a dimethyl silicone polymer, 3-5 parts of butanol, 1-3 parts of sodium hydroxide, 2-3 parts of sodium peroxide, 2-4 parts of potassium chlorate, 1-3 parts of silver carbonate, 2-5 parts of silver phosphate and 150-160 parts of purified water. The auto cooling fluid has good stability, the microbial flora can be inhibited and killed, floccules, flotage, sediments and the like are prevented, effective circulation of the cooling liquid is ensured, the fault of a cooling liquid circulating system is relieved and prevented, the anti-corrosion effect is good, corrosion to the cooling liquid circulation system can be reduced and delayed, the fault of the cooling liquid circulating system is reduced, and the service life of the auto cooling liquid is prolonged.
Owner:梁胜光

Method for Determining Chromium Content in a Tungsten Matrix with Added Chromium or Simultaneously Added Chromium and Vanadium

A method for determining chromium content in a tungsten matrix with singly or simultaneously added chromium and vanadium, characterized in that a test sample is subjected to melting with sodium peroxide and hot water leaching; meanwhile said sodium peroxide is also used as an oxidizing agent to oxidize all the chromium to high valences; the main body of tungsten is coordinated by ammonium hydrogen fluoride to prevent tungstic acid from precipitating; precipitation and turbidity are avoided throughout the analysis, titration can be carried out in a quite clear condition with accurate and reliable results. In this invention, the clearness of the solution when titrating is very important for the accuracy of titrimetric analysis; the solution is always clear throughout the determination, ensuring that the interference with determination of chromium from vanadium is accurately and quantitatively eliminated; the interference from vanadium is eliminated by subtraction method, by means of titrating with ferrous ammonium sulfate standard solution after oxidation with potassium permanganate. In this invention, the determination method allows the determination to be carried out in the quite clear condition, and eliminates the interference from vanadium completely and quantitatively, thus the accuracy and speed of the determination of chromium content in a tungsten matrix with singly or simultaneously added chromium and vanadium are improved.
Owner:JIANGXI RARE EARTH & RARE METALS TUNGSTEN GRP
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