3556 results about "Test solution" patented technology

Systems and methods are described for laser ablation of an analyte from a specimen and capturing of the analyte in a dispensed solvent to form a testing solution. A solvent dispensing and extraction system can form a liquid microjunction with the specimen. The solvent dispensing and extraction system can include a surface sampling probe. The laser beam can be directed through the surface sampling probe. The surface sampling probe can also serve as an atomic force microscopy probe. The surface sampling probe can form a seal with the specimen. The testing solution including the analyte can then be analyzed using an analytical instrument or undergo further processing.

The method comprises: reading out the pre-configured test solution; according to the function type in said test solution, calling the relevant functional test script; said functional test script calls a browser to open the relevant webpage window of the Web application system under test, and records the identifier of the webpage window; said functional test script calls the browser interface to input the data and operation of current test solution into said webpage window to get test result.

The present invention relates to a microfluidic electrochemical sensor apparatus and a method for conducting analytical tests with said apparatus for multi-reactant assays. The apparatus of this invention is a multi-layer body made of at least three layers, the first one being a polymer layer (1) comprising a microstructure (5) with at least one integrated microelectrode (4) and conductive tracks (13) for connection to an external electrochemical unit, the second one being a non-porous material serving to cover said microstructure so as to enable microfluidic manipulations and the third one being a porous layer (2) such as a membrane or a glass frit, said porous layer comprising at least one reagent (3) to be solubilized upon contact with a test solution (7) and reacting with an analyte (6) present in said solution to form a product that is transported along said microstructure so as to enable electrochemical detection of said analyte. The invention notably enables the performance of multi-reactant assays in a reduced number of steps.

The present invention relates to a bridge field static load test evaluation method, which is mainly a method for evaluating the bearing capacity and adaptation performance of a bridge by means of a field static load test. The method comprises the following steps: (1) determining specific content and method for collecting relevant data for early stage preparation work; (2) establishing a reasonable and accurate bridge structure finite element model according to the collected data; (3) calculating and analyzing a result according to an endogenous force and a stress of the bridge under dead and live loads, and determining theoretical force bearing safety and live load force bearing characteristics; (4) in combination with a traditional key section of the bridge, determining a bridge test section and completing static load test solution designing; (5) performing the field static test for the bridge and processing the test data; (6) studying an evaluation interval corresponding to a preset test evaluation indicator; and (7) making a reasonable and comprehensive assessment on the structural performance of the bridge. The evaluation method and indicator according to the present invention can more effectively indicate the practical bearing capacity and applicability of the bridge in a refined manner, and improving the reasonability and accuracy of the evaluation result.

The invention belongs to a technique for analyzing elements of an alloy, and relates to a method for measuring the contents of aluminum, titanium, manganese, nickel, tungsten and iron in a cobalt-base alloy. The method adopts an inductively coupled plasma atomic emission spectrometer and is different according to different measured elements and different tungsten contents; when high-content tungsten is dissolved, the volume of test solution needs to be maintained between 20 and 40 mL, or the tungsten is easy to be separated out; by performing interference experiments and spectrogram analyses, the method finds the optimal analytical line, overcomes the interferences caused by a plurality of elements such as major elements of cobalt, chromium, tungsten and the like in the cobalt-base alloy, and improves the measuring accuracy; the sample dissolving speed is accelerated, and the sample dissolving time is shortened to 2 hours from about two or three days; and the method has wide measuring ranges including: 0.05 to 0.30 percent of the aluminum, 0.05 to 0.30 percent of the titanium, 0.05 to 1.00 percent of the manganese, 0.05 to 24.00 percent of the nickel, 0.05 to 20.00 percent of the tungsten, and 0.05 to 3.00 percent of the iron.

A matrix type sustained-release preparation and a manufacturing method therefor are provided wherein dissolution with low pH dependence of a basic drug or a salt thereof at the early stage of dissolution can be ensured in a dissolution test, and wherein as the dissolution test proceeds, a ratio of a dissolution rate of the basic drug or the salt thereof in an acidic test solution to a dissolution rate of the basic drug or the salt thereof in a neutral test solution (dissolution rate in the acidic test solution / dissolution rate in the neutral test solution) decreases with dissolution time at the late stage of dissolution, as compared to the early stage of dissolution. According to the present invention, the matrix type sustained-release preparation contains a basic drug or a salt thereof and at least one enteric polymer, in which solubility of the basic drug or the salt thereof in a 0.1 N hydrochloric acid solution and a neutral aqueous solution, pH 6.0 is higher than in a basic aqueous solution, pH 8.0.

An automated method for testing audio signal quality of cell phone transmissions provides a Mean Opinion Score (MOS) output using inexpensive test components. The test system uses a server computer to eliminate the need for expensive faders used in a bench test system. The server computer manipulates data packets from the reference media file to simulate impairments, including losses, errors, noise and jitter, at a much lower cost than using actual faders. Transmission through two separate radio access networks RANs is provided to simulate two parties communicating using separate mobile devices (an end-to-end test solution) with a single cell phone.

The invention relates to a method for detecting the element content in alloy or ore by utilizing an ICP emission spectrometer, comprising the following steps: placing the alloy or the ore in solvent,heating and leading the alloy or the ore to be dissolved fully in solution to obtain mixed solution; diluting the mixed solution to obtain test solution; selecting the optimal analysis line of each element according to the composition of substrate of the alloy or the ore; preparing a set of corresponding standard solutions with the concentration sequencing from low to high according to the concentration index of each element in the alloy or the ore; introducing the standard solutions to the ICP emission spectrometer to measure the emission light intensity of the element analysis line and to draw a standard curve; introducing the test solution to the ICP emission spectrometer to measure the emission light intensity corresponding to each element; and determining the content of each element according to the standard curve. The method can detect simultaneously the content of the required element and oxide only by one solution, therefore, the invention has simple operation, shortened measuring cycle, stable detection results with high accuracy degree.

A panel chip for supporting biological samples for observation with an imaging microscope. The glass panel defines a top flat surface, a bottom bearing surface, and at least a few channels extending generally parallel to each other from top to bottom surfaces. Each of the channels defines a top access mouth for ingress of biological. The channels are arranged in subgroups made of a number of unit cells. Instead of being cylindroid, these channels may form cross sectional rectangular or arcuate channels, or cross sectionally water droplet like channels. Each channel has such an inner diameter as to accommodate flow through viscosity of a biological sample containing fluid. The porous substrate that is created by slot channel can provide the maximum binding surface area per unit cell or pixel, as compared to cylindrical pores, thus achieving higher sensitivity and better imaging. Also, this panel chip is capable of being used as direct in situ synthesizing of molecules and drugs. Other impurities in test solutions are however allowed to pass freely therethrough and be least prone to blockage.

The invention relates to a detection method of harmful element migrated masses in a plastic packaging container for foods, in particular to a detection method for simultaneously measuring migrated masses of lead, cadmium, chromium, arsenic, antimony and germanium in a plastic packaging container for foods by an ICP-AES (inductively coupled plasma emission spectrometry) method. The detection method comprises the following steps: 1, carrying out a migration test; 2, carrying out a blank test; and 3, carrying out measurement by an inductively coupled plasma emission spectrometer. The ways of RF (radio frequency) power amplification (for a 3% acetic acid simulacrum test solution), ethanol removal (for a 10% ethanol simulacrum test solution) and microwave digestion (for a delicate olive oil test solution) are used to efficiently, simply and quickly measure the migrated masses of various harmful elements in four simulacrums in the plastic packaging container for the foods simultaneously.

A perfusion chamber includes a porous oocyte support structure. A continuously sloped top surface and a receiving well in the support structure entrap the underside of the oocyte, thereby localizing the cell in a predetermined fixed position within the reach of dedicated voltage-clamp microelectrodes. A test solution is delivered continuously at the top of the chamber, above the oocyte, and withdrawn from the bottom of the chamber, below the oocyte. The porosity of the support material enables the continuous perfusion of test solution around the membrane of the oocyte, including its bottom portion that is held firmly in contact with the holding well. The geometry of the holding well is selected such as to ensure the automatic and precise placement of the oocyte by gravity and to optimize the pressure distribution over its membrane, thereby minimizing the probability of rupture or other damage to the cell. The entire top surface of the support structure is sloped inward toward the substantially central well, and the bottom of the well is contoured to conform to the shape of an oocyte of average size.

A system and method for analyzing a chemical composition of a specimen are described. The system can include at least one pin; a sampling device configured to contact a liquid with a specimen on the at least one pin to form a testing solution; and a stepper mechanism configured to move the at least one pin and the sampling device relative to one another. The system can also include an analytical instrument for determining a chemical composition of the specimen from the testing solution. In particular, the systems and methods described herein enable chemical analysis of specimens, such as tissue, to be evaluated in a manner that the spatial-resolution is limited by the size of the pins used to obtain tissue samples, not the size of the sampling device used to solubilize the samples coupled to the pins.

The present invention includes a method and apparatus for the detection of a target material. The method and apparatus includes providing a substrate with a surface and forming a domains of deposited materials thereon. The deposited material can be placed on the surface and bound directly and non-specifically to the surface, or it may be specifically or non-specifically bound to the surface. The deposited material has an affinity for a specific target material. The domains thus created are termed affinity domains or deposition domains. Multiple affinity domains of deposited materials can be deposited on a single surface, creating a plurality of specific binding affinity domains for a plurality of target materials. Target materials may include, for example, pathogens or pathogenic markers such as viruses, bacteria, bacterial spores, parasites, prions, fungi, mold or pollen spores. The device thus created is incubated with a test solution, gas or other supporting environment suspected of containing one or more of the target materials. Specific binding interactions between the target materials and a particular affinity domain occurs and is detected by various methods.

The present invention relates to a capture agent member being used in a magnetic sensor to detect the presence or concentration of a target substance in a test solution by detecting the presence or number of the magnetic marker, wherein the capture agent member contains a capture agent for capturing the target substance and a labeling agent serving as a nucleus for the magnetic marker to agglutinate, and wherein the capture agent is labeled with the labeling agent. The present invention relates to a material which improves detection sensitivity of a biosensor using a magnetic sensor while maintaining reactivity and dispersibility. In particular, according to the present invention, there can be provided a material which enables realization of high sensitivity by using a simple magnetic biosensor such as a semiconductor Hall element and a magnetoresistance effect element.

An Analog / mixed signal automatic test system includes a software architecture that creates a virtual composite instruments through novel software dynamic allocation of low level resources. These virtual composite instruments provide backwards and forwards compatibility to a variety of automatic test equipment, known or available on the market. The virtual composite instruments are free from the normal constraints imposed by hardware implementations. Creation of the virtual composite instruments allows a single piece of automatic test equipment system to emulate many implementations of automatic test equipment, providing higher utilization, and therefore a lower cost test solution for device manufacturers. The test instruments are preferably object controls and are preferably instantiated and controlled by the test system server. This allows multiple users to control the tester simultaneously across, for example, the Internet.

Embodiments of the present invention provide methods and apparatuses for implementing hierarchical design-for-test (DFT) logic on a circuit. The hierarchical DFT logic implements DFT circuitry that can be dedicated to a module, and which can configure DFT circuitry for multiple modules to share a sequential input signal and / or to share a sequential output signal. During operation, the DFT circuitry for a first module can propagate a bit sequence from the sequential input signal to the DFT circuitry of a second module, such that the bit sequence can include a set of control signal values for controlling the DFT circuitry, and can include compressed test vectors for testing the modules. Furthermore, the DFT circuitry for the second module can generate a sequential response signal, which combines the compressed response vectors from the second module and a sequential response signal from the DFT circuitry of the first module.

The invention relates to the field of analytical chemistry and food safety, and provides a high performance liquid chromatography detection method for residual quantity of multiple ultraviolet absorbents in cosmetics. A cosmetic sample of 0.4g is weighed and placed in a plastic centrifuge tube of 50 ml, sample extraction liquid of 20ml is added, after the cosmetic sample of 0.4g and the sample extraction liquid of 20ml are mixed for 2 minutes in a vortex mode, sonic oscillation extraction is carried out for 20 minutes, 8000 revolutions per minute centrifugation is carried out for 10 minutes and, and supernate is to be purified; and after test solutions sequentially pass through microfiltration membranes of 0.45 micrometer and 0.20 micrometer, a high performance liquid chromatograph is adopted to carry out qualitative determination and quantitative assay. The detection method has the advantages of being simple, fast, accurate, efficient, and the like, and can detect 12 ultraviolet absorbents at the same time. Technical indexes of detection minimum, the recovery rate, the degree of precision, and the like all meet relevant demands for ultraviolet absorbent detection in sun block cosmetics at home and abroad. The method is suitable for detection and monitoring of the ultraviolet absorbents in the sun block cosmetics, and has great significance on promoting of import and export trade of cosmetics of our country, ensuring of safety of the cosmetics, and guarantee of human body health.

The invention discloses a content analysis and detection method of twelve compound vitamins for injection. Liposoluble components including vitamin A palmitate, vitamin D3 and racemic alpha-tocopherol are detected under the same high-performance liquid phase method conditions, a test solution is prepared by extracting a preparation content by non-polar organic solvent, and the detection wavelength is 265+ / -3nm. Water-soluble components including cocarboxylase tetrahydrate, riboflavin sodium phosphate, vitamin B6, vitamin C, nicotinamide, folic acid and dexpanthenol are detected under the same high-performance liquid phase method conditions, and the detection wavelength is 210+ / -3nm. Biotin and vitamin B12 are subjected to high-performance liquid phase method based detection, the detection wavelength is 200-600nm, and the preferable detection wavelength for the vitamin B12 is 550+ / -3nm. The method has high applicability.

The invention relates to a test method of steel, in particular to a test method of a micro amount of arsenic or antimony in steel. The test method is based on a principle of a flow injection-hydride generation-atomic absorption spectroscopic methodology, and experiments are determined in a flow-injection sample-injection mode. The method comprises the following steps: a test solution is reduced bya thiourea-ascorbic acid mixed solution and a hydrochloric acid solution to convert arsenic (V) into arsenic (III), and convert antimony (V) into antimony (III); the test solution reacts with a potassium borohydride solution under a carrier band of a carrier solution to generate a great amount of nascent oxygen which reacts with the arsenic (III) or the antimony (III) to generate gaseous AsH3 orSbH3; the AsH3 or the SbH3 is led into a specially-designed quartz tube by high-purity argon gas as carrier gas and is atomized into ground-state atomic vapor; ground-state electrons which are on theoutermost layer of the atom are excited by the light energy of a light source of a hollow cathode lamp to transit to a high energy level; and the amount of abortion light intensity is directly proportional to the concentration of the atom. Accordingly, the arsenic or antimony content in the test solution can be quantitatively analyzed.

The invention discloses a method for detecting pyrethroid pesticide residue amount in smoke by a cigarette filter, belonging to the technical field of tobacco chemical analysis. The method comprises the following steps: placing a sucked filter tip at standard smoking condition into a 150ml of bottle with a tapered plug; adding 100mL of mixed solvent of ethyl acetate and cyclohexane with the volume ratio of 1:1; placing the bottle on an ultrasonic wave generator for extraction for 30min; concentrating to be 0.5mL on a rotary evaporator after drying by anhydrous sodium sulfate; setting the volume to be 2mL by normal hexane to be purified; placing a small graphite carbon black column on a solid phase extractor; activating by 3mL of acetone and 3mL of normal hexane in sequence; transforming the sample test solution to be purified into the small graphite carbon black column; eluting for two times by utilizing 2.5mL of mixed solvent of acetone and normal hexane, wherein the speed does not exceed 5.0mL / min; evaporating and concentrating eluent; setting the volume to be 1.5mL by acetone and normal hexane with the volume ratio of 2:8; and analyzing on GC-ECD. The method of the invention is simple and accurate, and can effectively determine pyrethroid pesticide residue amount in smoke by the cigarette filter.

The invention provides a method for constructing a dual-chamber microbial fuel cell (MFC)-type BOD (biochemical oxygen demand) sensor by using potassium permanganate as cathode electron acceptor, which belongs to the field of waste water quality monitoring. The method specially comprises the steps of constructing a dual-chamber MFC reactor; enriching electricigenic microorganisms on an MFC anode plate, and adjusting an external resistor to obtain maximum MFC output power; respectively adding different concentrations of artificial sewage and potassium permanganate solution into an anode chamber and a cathode chamber of the MFC, calculating the generated electricity of the MFC corresponding to different BOD concentrations according to MFC output current and detection time; and processing the generated electricity and BOD by linear fitting to obtain a sensor detection limit and a linear equation. After a to-be-tested solution with unknown BOD value is added into the anode chamber of the MFC, the generated electricity of the MFC is calculated according to the MFC output current and the detection time; and the BOD value of the to-be-tested solution can be calculated according to the known linear equation. The MFC-type BOD sensor using potassium permanganate as cathode electron acceptor has the advantages that the BOD detection range is widened to be 500mg / L; the detection time is shortened by 50% or more; and the detection relative error is less than 10%. Accordingly, the MFC-type BOD sensor has a high application value.

The invention belongs to the technical field of electrical power systems and provides a power distribution network protocol test analytical method and a system. The method includes acquiring a protocol which is used by a device to be tested; performing a test for the protocol according to pre-built protocol components and specific projects listed in configuration files of the protocol components; and analyzing the specific projects and recording a test result to draw a test solution. According to the power distribution network protocol test analytical method and the system, the test for the protocol is performed according to the pre-built protocol components and the specific projects listed in the configuration files of the protocol components, the specific projects are analyzed, the test result is recorded to draw a test solution, thereby the protocol of the device is subjected to an effective test, devices are convenient to mutually consistent, and the debugging management is facilitated.

The invention discloses a method for determining the impurity content in high-titanium slag, and belongs to the metallurgical chemical field. According to the method, a high-titanium slag sample is molten by a mixed flux; a frit is leached by a sulfuric acid solution to prepare a test solution; and the impurity component in the diluted high-titanium slag test solution is determined by an inductive coupling plasma emission spectrometer. With the invention, the content of the impurity component in high-titanium slag can be determined accurately, simply, and rapidly.

Low concentrations of silicon in an etchant solution are analyzed by adding a predetermined concentration of fluoride ions to a test solution comprising a predetermined volume of the etchant solution, and measuring the concentration of fluoride ions in the test solution. Reaction with silicon ions in the test solution reduces the concentration of fluoride ions, which are present in stoichiometric excess, so that the silicon concentration of the etchant solution can be calculated from the difference between the predetermined and measured concentrations of fluoride ions in the test solution. The method is especially suited for analysis of silicon nitride etchants comprising a high concentration of phosphoric acid.

The invention discloses a method for determining sea cucumber polysaccharide content in a sea cucumber or a sea cucumber product. The method is characterized in that the sea cucumber or the sea cucumber product is enzymolyzed by protease; the sea cucumber polysaccharide produced by the enzymolysis is separated out by adopting alcohol precipitation; then tested solution is prepared by hydrolysis of trifluoroacetate; the tested solution is prepared into fucose standard water solution which is derived by 1-phenyl-3-methyl-5-pyrazolone; the peak area of fucose derivative in the obtained derivatives is measured by high performance liquid chromatography; and the sea cucumber polysaccharide content in the sea cucumber product is obtained by calculating with the fucose as a reference. The invention provides a simple, accurate, reliable and standardized quantitative analysis method for determining the sea cucumber polysaccharide in various sea cucumbers and sea cucumber products.

The invention provides a method for determining the content of tris (2-chloroethyl) phosphate, which comprises the following steps: a sample to be tested is extracted with an organic solvent extractant, the obtained extract is purified via a Waters Oasis HLB extraction column after being concentrated, is concentrated to a definite volume after leacheate which is the organic solvent is collected, and finally is filtered to prepare a specimen test solution; and then the specimen test solution is detected with a gas chromatograph-mass spectrometer according to an external standard method. When the sample to be tested is a solid sample, the sample to be tested is pulverized firstly and then is extracted by ultrasound; and when the sample to be tested is liquid, the sample is extracted by ultrasound. The method for determining the content of the tris (2-chloroethyl) phosphate is rapid and effective, the error rate of is not more than 5 percent, and the detection limit is 0.05mg / kg. The invention provides a reliable and conveniently implementary method for detecting the content of tris (2-chloroethyl) phosphate in rubber, plastics, printing ink and paint products and can meet the needs in research and production.

The invention discloses a method for determining N-methylamino ammate in production of acesulfame. The method mainly comprises the steps of: (1) selecting an analytical chromatographic condition, an ODS column (4.6mm*25cm) or other equivalent chromatographic columns, wherein the wavelength is 250nm, the flow velocity is 1ml / min, the column temperature is 25 DEG C, and the sample amount is 20mu l; (2) preparing tetrabutylammonium hydrogen sulfate solution from deionized water until the molar concentration is 1.0-2.0mmol / L, and preparing a mobile phase from the prepared tetrabutylammonium hydrogen sulfate solution and chromatographic grade methanol according to the volume ratio of 60 to 40; (3) diluting the sample to be tested by an organic solvent according to the volume ratio until the concentration is 0.5-2.0%, so as to prepare a test solution; (4) absorbing the test solution by a microinjector, injecting into an efficient liquid chromatograph, and analyzing by an area external standard method; and (5) recording the content of the N-methylamino ammate in the sample to be tested. By adopting the method disclosed by the invention, the content of the N-methylamino ammate can be accurately and rapidly determined.