The invention discloses a method for preparing
calcium-
magnesium carbonate mineral Cal-xMgxCO3 at a high temperature under
high pressure. The method includes evenly
grinding and mixing analytically-pure
calcium carbonate,
magnesium oxalate powder and
anhydrous oxalic acid to obtain a mixture serving as an initial
raw material, pressing the mixture into a cylinder by a tablet
machine, inserting a cylindrical sample into a
platinum tube, sealing two ends of the
platinum tube by a
welding gun, putting the sample sealed by
platinum in an h-BN tube by taking h-BN as a pressure transfer medium, assembling the sample in the h-BN tube in a high-pressure combined
assembly block, putting the high-pressure combined
assembly block in a cubic press for high-temperature high-pressure reaction, taking out the reacted sample, opening the platinum tube by
a diamond cutter, and naturally air-
drying the sample to obtain
calcium-
magnesium carbonate minerals. By the method, the technical problems such as operation
process complexity, long reaction time, and low purity, low
chemical stability and proneness to water absorption of obtained samples in existing calcium-magnesium carbonate mineral preparation methods are solved.