The invention belongs to the field of nanoparticle preparation, in particular to metallic nano cluster / silicon dioxide hollow nuclear shell structured nanoparticles and a one-step controllable preparation method thereof. The used surfactant is a nonionic surfactant, the organic phase is cyclohexane, toluene and other organic hydrocarbons, and a metalsaline solution and a metal complexing agent are added to form a reversed micellesystem. Meanwhile, the complexed metalsaline solution in the reversed micellesystem is reduced to obtain metallic nanoparticles and then ammonia water and ammoniawater are added directly in the solution to obtain size and shape controllable hollow silicon dioxide nuclear shell material with metallic nano clusters distributed uniformly on the inner wall of thecavity. The method has the advantages of simple process, easy operation and great yield and can obtain size and shape controllable metallic nano cluster / silicon dioxide hollow nuclear shell structured nanoparticles.
The invention relates to a method for enhancing a Raman spectrum by using shell isolated nano particles, relating to the field of detection of laser Raman spectrums. The invention provides the universal method which has easy and fast preparation, low cost, strong Raman signal, good repeatability and accurate result, and is used for enhancing the Raman spectrum by using the shell isolated nano particles. The method comprises the following steps of: preparing the shell isolated nano particles with nuclear shell structures taking metal nano particles as kernels and extremely-thin shell inert materials as outer shells; uniformly scattering the shell isolated nano particles on the surface of a sample to be measured; and directly detecting the surface enhanced Raman spectrum.
The invention discloses a micro hemispherical resonator gyro and a preparation method thereof, belonging to the field of micro / nano processing and manufacturing. The preparation method comprises the following steps of: performing ICP etching on a high-resistance siliconwafer to obtain a silicon body 1; depositing polycrystalline silicon and etching to obtain a preliminary electrode 3; depositing carbon dioxide on the front, and imaging to form a carbon dioxidemask 4; etching to obtain a hemispherical harmonic oscillator cavity 5 and an electrode 6; removing the carbon dioxidemask 4, and performing ICP etching on the back to obtain a support body cavity 7; depositing carbon dioxide insulating layers 8 on the front and back sides; depositing polycrystalline silicon on the front and back sides to obtain a hemispherical harmonic oscillator 9, a support body 10 and a signal loading electrode 11; and thinning and polishing on the front, removing excessive polycrystalline silicon and etching carbon dioxide to obtain the movable hemispherical harmonic oscillator 9. According to the invention, the support body cavity is processed, the carbon dioxide and polycrystalline silicon are deposited, and the size of the support surface of the support body is easily controlled; and electroconductive polycrystalline silicon is deposited and filled by use of a processing electrode tank, and the shortcoming of excessively small working area of a drive electrode and a sensitive electrode is overcome.
The invention relates to a liquid-drop-generation capillary microfluidic chip and a preparing method thereof. The liquid-drop-generation capillary microfluidic chip adopts a capillary as a function unit for generating and collecting liquid drops, and comprises a microfluidic chip etched with microchannels and the capillary. By combination of the microfluidic chip and the capillary, the liquid-drop-generation capillary microfluidic chip achieves introduction of two incompatible liquids on the microfluidic chip, achieves liquid drop generation at the intersection of the microfluidic chip and the capillary, and directly collects liquid drops in the capillary. The liquid-drop-generation capillary microfluidic chip is simple in structure and convenient to operate, overcomes the problem that liquid uniformity and the like are liable to damage in traditional liquid drop collection-generation and collection methods, and achieves integration of liquid drop generation and capillary collection.
The invention discloses multi-touch system and method in the technical field of computer vision. The method includes: establishing spatial correspondence between a Kinect camera and a projection screen; allowing a computer to preprocess an image captured by the Kinect camera; extracting a hand image from the preprocessed image; acquiring coordinates and directions of fingers in the hand image by finger contact detection algorithm; tracking finger contacts by minimum distance first algorithm; recognizing the finger contacts by means of template matching to obtain corresponding operational information of the finger contacts; and transmitting the operational information to the computer which analyzes the operational information and controls corresponding operations for the image in the current screen according to analysis results. Man-machine interactive multi-touching is achieved by the Kinect camera detecting acts of human fingers on the projection screen, and replaces the mouse and keyboard, and the operation is well performed in a real-time manner. The projection screen needs to be planar only, and adaptability of screen operation is increased greatly.
The invention provides technology for preparing porous heat insulation plates by sintering iron tailings, comprising the following steps: breaking and then grinding shale and the iron tailings, sieving and measuring the ground shale and iron tailings to ensure the fineness is 20-80mu m; adding toughening agents, cosolvents and foaming agents into the ground shale and iron tailings in proportion and mixing the above materials, adding water to the mixture for prilling, after natural drying, distributing raw material balls on the moulds, then placing the moulds into a kiln to be sintered by way of sectional heating, and finally stacking the products after demoulding the cooled plates. The technology utilizes a great number of iron tailings with the highest addition up to 40%, saves energy andis beneficial to environmental protection. The volume density and pore sizes and distribution of the plates can be controlled by the addition and sintering schedules of the foaming agents. The prepared plates enjoy uniform pore distribution, high strength and good heat preservation and insulation properties.
Owner:XIAN RES & DESIGN INST OF WALL & ROOF MATERIALS CO LTD +1