The invention provides a preparation method of a
solid wood
fiber / SiO2
aerogel composite
thermal insulation material. The preparation method comprises the following steps: 1, immersing
balsa wood in amixed solution of NaOH and NaSO3, boiling the liquid, moving out the
balsa wood, washing the
balsa wood with
distilled water, adding H2O2, boiling the liquid, moving out the balsa wood, washing the balsa wood with
distilled water to obtain a wood
fiber substrate; 2, by means of tetraethoxysilane and
methyltrimethoxysilane as a mixed
silicon source and absolute ethyl
alcohol as a
solvent, uniformly mixing the components with water and the wood
fiber substrate, adding
hydrochloric acid until the pH value is 2-3, fully hydrolyzing the fiber substrate, adding
ammonia water until the pH value is 8-9, performing standing treatment to form gel, and performing aging,
surface modification,
solvent exchange and normal pressure
drying on the gel to obtain the
solid wood fiber / SiO2
aerogel compositethermal insulation material. According to the method provided by the invention, the excellent properties of the balsa wood and the SiO2
aerogel are combined, so that the integrity of the SiO2 aerogelis improved, the problems that the fir absorbs water easily and the
utilization rate is low are solved, and meanwhile, the heat preservation property of the balsa wood is improved. The preparation equipment is simple, convenient and low in cost, and has a good development prospect and further in-depth development and research value.