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437results about How to "Adapt to industrial production" patented technology

Purifying method for ultra-pure aluminum

The invention relates to a purifying method for ultra-pure aluminum. The purifying method specifically comprises the following steps: injecting molten aluminum with purity being 4N6 into a cast iron crucible, and heating the molten aluminum by a heating wire on the outer wall of the cast iron crucible for preserving the temperature of the molten aluminum to be 680-700 DEG C; stretching seed crystals above the cast iron crucible into a position 2-3cm under the liquid level of the molten aluminum, and introducing cooling gas to the other ends of the seed crystals to cool and crystallize the molten aluminum; spirally rotating the seed crystals in the cast iron crucible, thereby enabling the molten aluminum to carry out rotary motion in the cast iron crucible; and after the crystallizing is ended, quickly pulling out the seed crystals with crystallized ingots, and finally enabling the crystal seeds and the formed crystallized ingots to be in shape of inverted mushroom. The purifying method has the advantages of greatly reducing the purifying cost, and greatly improving the purifying efficiency and the purifying purity, and is suitable for industrial production.
Owner:NANTONG TADE ELECTRONICS MATERIAL TECH

High-purity DHA algae oil ethyl ester and preparation method for transferring high-purity DHA algae oil ethyl ester into glyceride

The invention discloses a DHA algae oil ethyl ester and a preparation method thereof. The method comprises the following steps: carrying out ethyl-esterifying on crypthecodinium cohnii DHA grease and then purifying trough a secondary molecular distillation method to obtain high-purity DHA ethyl ester. The invention further discloses a DHA glyceride and a method for transferring the DHA algae oil ethyl ester into glyceride. The method comprises the following steps: mixing the DHA algae oil ethyl ester with glycerinum in a material tank, feeding the mixed material in a reactor having immobilized lipase, performing transesterification to replace out the ethanol, recycling through a condenser, and flowing the reacted mixture back to the material tank, circularly reacting for 5-60 hours, and finally returning to the material tank, wherein the glyceride product is obtained by performing molecule distillation on the material. The method disclosed by the invention is suitable for the industrial production, the DHA greased produced from the microorganism is used as the raw material, the percent content of the DHA is greatly improved, the ethyl ester is transferred into the glyceride, the ethanol is avoided, the side effect after eating is not generated, and the utilization degree of the DHA algae oil ethyl ester in vivo is effectively improved.
Owner:JIANGSU ZHONGBANG PHARMA

Binary nanometer cooperative reinforcing and toughening silicon carbide ceramics and preparing method thereof

The invention discloses a method for preparing binary nanometer cooperative reinforcing and toughening silicon carbide ceramics, and silicon carbide powder, yttrium aluminum garnet, nano particles and nano crystal whickers are taken as the main raw materials. The method comprises the following steps: 1) the main raw materials, a binder and a dispersant are added into de-ionized water, after being ball-milled and mixed, water-base silicon carbide slurry is prepared; 2) the water-base silicon carbide slurry is sprayed and dried by adopting a spray granulation technology; 3) the obtained silicon carbide granulating powder is formed by adopting pre-pressing of dry pressing and final pressing of cold isostatic pressing; and 4) the obtained green body of silicon carbide is put in a vacuum non-pressure sintering furnace to be treated, thus obtaining the binary nanometer cooperative reinforcing and toughening silicon carbide ceramics. The invention also discloses the binary nanometer cooperative reinforcing and toughening silicon carbide ceramics prepared in the method. The silicon carbide ceramics have the advantages of large flexural strength, good fracture toughness and the like.
Owner:ZHEJIANG UNIV

A method for preparing expandable graphite or graphene by utilizing waste cathode carbon formed in electrolytic aluminum production

A method for preparing expandable graphite or graphene by utilizing waste cathode carbon formed in electrolytic aluminum production is disclosed. The method includes (1) a step of crushing, adding a strong oxidant and water into the crushed product, stirring, rolling or wet-grinding the mixture, and performing a hydrothermal oxidation reaction; (2) a step of controlling the temperature, pressurizing, feeding supercritical or liquid carbon dioxide, mixing the mixture by stirring the mixture, allowing the mixture to stand, adjusting the temperature and pressure, performing separation to obtain aqueous slurry and graphite oxide slurry fluid, and washing the graphite oxide slurry fluid with water to remove impurities; and (3) a step including 1) a manner of performing atomization, expansion and stripping to remove the carbon dioxide; or 2) a manner of adding a reactant for reduction, and then performing atomization, expansion and stripping to remove the carbon dioxide, or further performing denitrification and deoxygenation; or 3) a manner of adding a fluorinating agent, heating the mixture, performing a fluorinating reaction, and performing atomization, expansion and stripping to remove the carbon dioxide. Expanded graphite powder, graphene powder, denitrified deoxygenated graphene powder or fluorinated graphene powder which are prepared by the method have excellent properties. The method is simple, efficient, clean, free of secondary pollution, low in energy consumption and suitable for industrial production.
Owner:长沙紫宸科技开发有限公司

Cornus officinalis total saponins obtained by response surface method optimized ultrasonic-microwave synergetic extraction and method for extracting total saponins from cornus officinalis

The invention provides a method for extracting cornus officinalis total saponins by response surface method optimized ultrasonic-microwave synergetic extraction. The method comprises the following steps: (1) treating materials to obtain cornus officinalis powder; (2) performing ultrasonic-microwave synergetic extraction to obtain a total saponin sample solution; and (3) purifying by macroporous resin, concentrating and drying eluent to obtain powdered cornus officinalis total saponins. The cornus officinalis total saponins can be prepared by the extracting method. According to the method, the cavatition effect of ultrasonic wave and the high-performance infrared heating effect of microwave are combined, so that a sample can be quickly, effectively and reliably treated, the extraction time is shortened, the extraction efficiency is improved, the material-liquid ratio, the microwave power, the ultrasonic power and the extraction time can be respectively limited while the extract structure is guaranteed, and the extraction rate of the cornus officinalis total saponins is 13.96mg / g and is increased by up to 20 percent. The method has high raw material utilization rate, is effective and saves time, can be used for greatly saving cost, and is suitable for industrial production.
Owner:SHAANXI NORMAL UNIV

Layered vacuum insulation board core material and preparation method thereof

The invention discloses a layered vacuum insulation board core material and a preparation method thereof. The thickness of the vacuum insulation board core material is between 5 and 50mm, the coefficient of heat conductivity is between 0.018 and 0.03 W / mK, and the vacuum insulation board core material is formed by overlying a plurality of layers of glass fiber mats and can be prepared into vacuum insulation boards with high-efficient thermal insulation. According to the layered vacuum insulation board core material, continuous glass fiber with 6 to 13 mu m of diameter and 5 to 20mm of length is used and cannot be sucked into the deep parts of human lungs after being authenticated by world health organization, so that the layered vacuum insulation board core material is safe and harmless, meets the requirements of materials, can be used at ease for a long time and solves the problems of sanitation and safety of vacuum insulation board products.
Owner:周介明 +1

Lead-cadmium compound conditioner for rice field soil as well as preparation and application methods thereof

The invention discloses a lead-cadmium compound conditioner for rice field soil as well as preparation and application methods of the lead-cadmium compound conditioner. The conditioner is composed of the raw materials in mass fractions: 30-50% of calcium carbonate, 5-10% of hydroxyapatite, 20-30% of sepiolite and 20-30% of zeolite; the preparation of the conditioner comprises the following steps of: weighing various raw materials according to the mass fractions of the components of the lead-cadmium compound conditioner; continuously stirring the various raw materials in a stirring device for at least 30 min, and thoroughly stirring and evenly mixing all the materials; and the method of application of the conditioner comprises the following steps of: (1) analyzing the total quantity of lead and cadmium in the rice field and the content of lead and cadmium in exchange state; (2) determining the pollution level of the rice field soil by using an evaluation model; (3) applying the lead-cadmium compound conditioner according to the lead-cadmium pollution level in the rice field, and applying the lead-cadmium compound conditioner to the slightly polluted rice field at 100-150 kg / mu, to the mildly polluted rice field by 150-300 kg / mu and to medium-polluted rice field at 300-600 kg / mu, and balancing and stabilizing for 10-15 days; and (4) analyzing and measuring the content of lead and cadmium in exchange state in the rice field, and if the fixed rate is lower than 90%, additionally applying the conditioner at 100-150 kg / mu.
Owner:廖柏寒 +1

Industrial production method of azilsartan

The invention provides an industrial production method of azilsartan. The method comprises the following steps: 1) replacing hydroxylamine hydrochloride and organic alkali or inorganic alkali in a polarity aprotic solvent and centrifuging to obtain a homogeneous system, adding candesartan C6 alkyl ester (a compound shown in formula IV) and reacting at 90-110 DEG C to obtain a compound shown in formula III; and 2) dissolving the compound shown in formula III and a carbonylation reagent in the polarity aprotic solvent, adding in the organic alkali or inorganic alkali and reacting at 0-40 DEG C to obtain a compound shown in formula II, and carrying out alkaline hydrolysis to obtain azilsartan. By adopting the preparation method, the production cost of azilsartan is greatly reduced, an expensive and unstable hydroxylamine solution is not used, the reaction temperature is lowered, the product quality is well improved, the requirement for medicinal level is met, and individual impurity is controlled below 0.1%, which is superior to the ICH requirement of the EU (European Union).
Owner:合肥远志医药科技开发有限公司

Device system for purifying by utilizing gas separation membrane

The invention discloses a device system for purifying by utilizing a gas separation membrane. The device system comprises a mixing device, a pretreatment unit and three gas separation membrane units, wherein two ends of the mixing device are respectively communicated with a raw material gas and the pretreatment unit; a gas passes through the pretreatment unit and enters a gas inlet of the first gas separation membrane unit; an impermeable gas of the first gas separation membrane unit is communicated with a gas inlet of the second separation membrane unit; impermeable gases of the first and second gas separation membrane units pass through a mixed flow tank, and are communicated with a gas inlet of the third separation membrane unit; an impermeable gas outlet of the third separation membrane unit is provided with a backpressure control valve, and is communicated with a gas inlet of the mixing device for cyclic purification; the impermeable gas of the second separation membrane unit is a tail gas; the permeable gas of the third separation membrane unit is a product gas. According to the invention, three membrane units are used for purifying independently so as to completely purify gases, such as helium, hydrogen, carbon dioxide, and the recycling rate is relatively high; the device system is simple and compact in structure, and is applied to industrial production.
Owner:甘泳

Preparation technology for edge-sealing strip subjected to co-extrusion molding

The invention relates to the technical field of preparation of edge-sealing strips, and concretely relates to a preparation technology for an edge-sealing strip subjected to co-extrusion molding. The preparation technology comprises the following technological steps: step A, performing co-extrusion on a substrate-layer raw material and a hot-melt-adhesive-layer raw material possessing a same color, so as to prepare the edge-sealing strip possessing the substrate layer and the hot-melt-adhesive layer; B, cooling and curing the edge-sealing strip; and C, for usage, using hot wind or a hot gas or laser to melt the hot-melt-adhesive layer of the edge-sealing strip, so as to enable the face of the edge-sealing strip, which possesses the hot-melt-adhesive layer, to be adhered to a product to be subjected to edge sealing. The adhesive force of the hot-melt-adhesive layer is high, and degumming phenomenon is avoided. By employing hot wind or the hot gas or laser for melting the hot-melt-adhesive layer, edge sealing is performed. Seamless connection between the edge-sealing strip and a product to be subjected to edge sealing, such as medium density fiberboards, shaving boards, plywood and other artificial plates, is realized, and a hot melt adhesive is not needed for coating, so that a production process of coating a hot melt adhesive is saved, the product quality and the production efficiency are substantially improved, the production and application cost is reduced, and the preparation technology is relatively suitable for industrialized production.
Owner:DONGGUAN HUALI INDUSTRIES CO LTD
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