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12728results about How to "Mild conditions" patented technology
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Preparation method for propellant fuel
InactiveCN108910843AShorter ignition delay timeHazard reductionOrganic chemistryHydrazineEvaporationIgnition delay
The invention discloses a preparation method for propellant fuel. The preparation method comprises the following steps: uniformly mixing hydrazine or a methyl derivative thereof with a tetrahydrofuransolution of borane to perform a reaction, and after the reaction, performing rotary evaporation on the tetrahydrofuran solution to obtain a first product; adding a first solvent into the first product, then performing washing, and then performing rotary evaporation to remove the first solvent, so as to obtain a hydrazinoborane derivative. According to the method, hydroboration is carried out on ahighly-volatile hydrazine fuel and a methylated derivative of hydrazine, the obtained borohydride of the hydrazine is a colorless non-volatile liquid or a white solid, has no volatility and greatly reduces hazard of the hydrazine fuel, and is a novel aerospace propellant fuel since the ignition delay time of the hydrazine borofluoride is extremely short.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS
Nanometer functionalization surface modification method based on o-dihydroxybenzene derivatives
ActiveCN103435829AUniversalMild conditionsSemi-permeable membranesCoatingsSurface modificationChaetopyranin
The invention provides a simple universal nanometer functionalization surface modification method based on o-dihydroxybenzene derivatives. The method comprises that: dopamine is used to perform surface decoration on a basis material for one or more times, then the basis material subjected to surface decoration is subjected to nanometer functionalization decoration for one or more times; and nanometer functional materials such as various organic or inorganic nanometer particles, nanometer wires, nanometer sols, nanometer tubes and the like are fixedly disposed on the surface of the basis material, so that the material surface is improved in hydrophilicity, hydrophobicity, roughness and anti-pollution capability, or the material is enhanced in biocompatibility and performances such as antibiosis, catalysis and the like, or the material is endowed with new conductive, optical, thermodynamical performances and the like and enhanced in mechanical strength.
Owner:YANTAI LVSHUIFU MEMBRANE MATERIAL
Process for the production of biofuel from plant materials
InactiveUS20070259412A1Rapid productionEfficient and cost-effective useBiofuelsLignin derivativesCelluloseBiofuel
An integrated process for the production of ethanol from woody plant material is provided, the process comprising: contacting a continuous flow of the plant material with a counter-current continuous flow of an aqueous ethanol solution at elevated temperature and pressure to provide plant material depleted of lignin; removing ethanol from the lignin-depleted plant material; contacting a continuous flow of the lignin-depleted plant material with water at elevated temperature and pressure to solubilize xylose within the plant material; and hydrolyzing cellulose present in the plant material to form glucose, which in turn is fermented to produce ethanol.
Owner:VERTICHEM CORP
High-durability super-hydrophobic self-cleaning coating material and preparation method thereof
InactiveCN101962514AHas the following advantages: (1) cleanlinessHas the following advantages: (1) has the functionAntifouling/underwater paintsPaints with biocidesDouble bondDimethyl siloxane
The invention belongs to the technical field of a new chemical material, and in particular relates to a high-durability super-hydrophobic self-cleaning coating material and a preparation method thereof. The coating material of the invention is prepared by curing and drying nanoparticles with photo-catalytic activity, a low-surface-free-energy polymer and a cross-linking agent at the room temperature, wherein the low-surface-free-energy polymer consists of one or more of polysiloxane fluoride, dimethyl silicone polymer and polyphenylene methyl siloxane, which contain active groups, such as hydroxyl alkoxy group, carbon-carbon double bond, silanol group, siloxy group, and the like; the cross-linking agent is hydrogen-containing silicone oil or aminosilane; and the mass content of the photo-catalytic nanoparticles in the coating ranges from 10 to 60 percent. The coating is formed into a micro-nanostructure by nanoparticle self-organization; a super-hydrophobic self-cleaning coating with lotus effect is prepared from the coating and a cross-linked filming matrix with low surface energy; the persistence of a lotus-shaped super-hydrophobic characteristic of the coating is realized by using the photo-catalytic decomposition characteristic of an organic pollutant for the nanoparticles; and thus the material is suitable for large-area construction and has high weathering resistance andprominent self-cleaning characteristic.
Owner:FUDAN UNIV
Preparation method and applications of porous metal organic skeleton material
ActiveCN104370820AGood application effectEasy to operateOther chemical processesGroup 8/9/10/18 element organic compoundsMetal-organic frameworkSolvent
The invention relates to a preparation method of a porous metal organic skeleton material. The porous metal organic skeleton material comprises at least a metal ion and at least an organic compound that can be matched with the metal ion. The material can be prepared by dissolving metal compounds, organic ligand, and sustained-released alkali into a solvent and carrying out direct water (solvent) thermal synthesis at a certain temperature under a certain pressure so as to obtain the porous metal organic skeleton material. The operation of the provided preparation method is simple, the preparation method is suitable for massive industrial production and is suitable for the synthesis of porous metal organic skeleton membrane, and the provided porous metal organic skeleton material is used to absorb, separate, and store gas.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
Spirofluorene xanthene material, and preparation and use thereof
InactiveCN101440082ATest thermal stabilityThe synthesis steps are simpleOrganic chemistrySolid-state devicesVitrificationNonlinear optics
The invention discloses a spirofluorene xanthene material and a preparation method and an application method thereof, and relates to application of the material in the fields such as organic electroluminescence, photovoltaic cell, organic electrical storage, organic nonlinear optics, chemical and biological sensing, organic laser and so on. The material has the following structure. The material has the advantages that (1) the material is prepared through a one pot process and has simple steps and mild conditions; (2) the material has the advantages of spirobifluorene materials, and shows high thermal stability and vitrification temperature; and (3) the material has high hole or electron mobility and so on. An electroluminescent device prepared by utilizing the material achieves satisfactory results in aspects such as illumination, luminous efficiency, voltage withstand stability and so on.
Owner:NANJING UNIV OF POSTS & TELECOMM
Composite photocatalyst prepared from stephanoporate mineral and method thereof
InactiveCN101322944ALow costReduce the risk of poisoningMolecular sieve catalystsWater/sewage treatment by irradiationPoisoning riskLight energy
The invention relates to the preparation of an inorganic functional material, in particular to a photochemical catalyst prepared by taking a porous mineral as a carrier for carrying an n-typed semiconductor with a large energy gap and a method thereof. The natural porous mineral and an artificial porous mineral are used for preparing the carrier to carry the n-typed semiconductor and a compound semiconductor with photochemical catalysis function; the catalyst prepared is applied to the degradation of organic pollutants by photochemical catalysis or to serving as the filling of paints which can reproduce after being poisoned. The carrier prepared by the invention has large specific surface area, strong adsorption capacity, good adhesive force and low environment cost, can remarkably improve the efficiency of the photochemical catalyst and lower the poisoning risk of the catalyst; the sol of the semiconductor or the compound semiconductor has a photoresponse range covering visible light area and ultraviolet light area, thus being capable of effectively utilizing the light energy and being beneficial to reduce the cost of the light sources; the sol-gel dipping method is adopted to realize loading, which has the advantages of mild condition, even distribution, simple technique and convenience for mass production.
Owner:JILIN UNIV
Polydopamine-based biofunction modification method
InactiveCN102000658AImprove deformation resistanceImprove stabilityPretreated surfacesCoatingsAir atmosphereMetallic materials
The invention discloses a polydopamine-based biofunction modification method. The method comprises the following steps of: soaking clean inorganic / metal materials in dopamine alkaline aqueous solution with a pH value of 7.2 to 10, introducing oxygen to fully oxidize the clean inorganic / metal materials to obtain a monolayer polydopamine modification layer, drying, placing the material in the air atmosphere at 50 to 200 DEG C, performing thermal oxidation to obtain a multi-layer firmly-combined high-reactivity polydopamine layer, and soaking the treated material into the amino-containing and sulfydryl-containing biofunctional molecular solution to obtain a firmly combined biofunction simulate modification layer on the surface of the materials. The polydopamine modification layer obtained bythe method has excellent anti-deformation performance, stability and reactivity, can directly react with amino or the sulfydryl in the biomolecule to immobilize the bioactive molecule on the surface by covalent bonds; moreover, the process is simple, the condition is mild, and the method is easy to implement.
Owner:CO WITH LTD LIABILITY OF MEDICAL SCI +1
Integrated processing of plant biomass
InactiveUS7649086B2Rapid productionEfficient and cost-effective useBiofuelsLignin derivativesCelluloseWoody plant
An integrated process for the production of ethanol from woody plant material is provided, the process comprising: contacting a continuous flow of the plant material with a counter-current continuous flow of an aqueous ethanol solution at elevated temperature and pressure to provide plant material depleted of lignin; removing ethanol from the lignin-depleted plant material; contacting a continuous flow of the lignin-depleted plant material with water at elevated temperature and pressure to solubilize xylose within the plant material; and hydrolyzing cellulose present in the plant material to form glucose, which in turn is fermented to produce ethanol.
Owner:VERTICHEM CORP
Chemical/ionic/physical compounding cross linking hydrogel and preparation method thereof
The invention relates to chemical / ionic / physical compounding cross linking hydrogel and a preparation method thereof. The hydrogel is polymerized in a way that olefin monomer M1, a chemical cross-linking agent M2, multivalent ion biomacromolecule M3, an ionic cross-linking agent M4 and a physical cross-linking agent M5 are dissolved in water. The method comprises the following steps: preparing chemical / physical cross linked gel prepolymerization liquid, preparing chemical / ionic / physical cross linked gel prepolymerization liquid and preparing and purifying chemical / ionic / physical compounding cross linked gel. According to the invention, the characteristics and properties of the chemical cross-linking agent, the physical cross-linking agent and the ionic cross-linking agents are taken into consideration comprehensively, the compounding cross linking of molecular chains is realized; the prepared hydrogel is optically transparent and has higher mechanical ductility and rebound elasticity; the mechanic, optical and thermal performances and other performances can be regulated conveniently by controlling technology parameters and conditions; and the prepared hydrogel can be used in the fields such as tissue engineering, food industry, agricultural irrigation, daily chemical engineering, oil production, dye adsorption and biological medicine.
Owner:TIANJIN POLYTECHNIC UNIV
Method for preparing biodiesel by solid acid-base catalyst
InactiveCN1580190AWide variety of sourcesNo pollution in the processBiofuelsLiquid hydrocarbon mixture productionWater bathsBiodiesel
The invention relates a kind of preparation method of bio-diesel oil under the condition of solid ac and alk catalyzing. The character is that under the condition of solid ac and alk catalyzing, gain the bio-diesel oil using the craft of exchange reaction of soja oil with carbinol. Afer the reaction, apart catalyser from reaction liquor by centrifugal machine till delimination in quiet placing, the above is rough output, the below is admixture of glycerol and carbinol. Distil the of above to gain bio-diesel oil and to gain the pure glycerin in the same way. The distilled carbinol can be used again and again. The invention has many advantages, for example, its raw material can be rebirth, its craft is easy and only need normal equipment. Even treat the used oil, the whole process is easier compared with the method in solid ac and alk catalyzing, besides, the process will not produce foul water so it is environmental. Every plant of the bio-diesel accords with standards compared with foreign similar competitive grade and the main plants are close to its of 0# (GB252-1994, superior product)diesel of China.
Owner:BEIJING UNIV OF CHEM TECH
CaSO* crystal whisker with desulfurized gypsum as raw material and preparing method
InactiveCN101550602AReduce pollutionShort processPolycrystalline material growthFrom solid stateWhiskersCalcium sulphate crystals
The present invention relates to a CaSO4 crystal whisker with desulfurized gypsum as raw material and a preparing method. A technical scheme includes: mixing desulfurized gypsum, water and habit modifier fully for forming suspension; wherein, mass concentration of desulfurized gypsum is 1-8%, mass concentration of habit modifier is 5-20%; or stirring the above suspension 1-3 hours under conditions of normal pressure, 100-128 deg c and 120-210 r / min stirring speed, adding calcium sulphate crystal whisker by weight of 0.5-1% as inoculating crystal, reacting 1-3 hours, adding modifying agent, or stirring the above suspension 3-8 hours, adding the modifying agent directly; or stirring the above suspension 3-8 hours, and adding the modifying agent directly, the amount of the modifying agent is 0.4-1% of the suspension weight, stirring 0.5-1 hours; then pump filtering, washing and three-section drying for obtaining three various type calcium sulphate crystal whisker. The method uses a normal pressure salt solution crystallization method for preparing CaSO4 crystal whisker which has short process flow, geniality condition and low cost, and is an efficient purpose for realizing resource utilizing.
Owner:WUHAN UNIV OF SCI & TECH
Method for preparing white carbon black by utilizing silicon tetrachloride
The invention discloses a method for preparing white carbon black by utilizing silicon tetrachloride. The method comprises the following steps: mixing deionized water and low molecular fatty alcohol at the molar ratio of 1:4-4:4, and adding a proper amount of surfactant; slowly adding a certain amount of the silicon tetrachloride at the room temperature; and obtaining the white carbon black through the steps of preparing reaction solution, curing the reaction solution, sedimentation and abstersion, pulpifying and spray drying, wherein the concentration of the silicon tetrachloride is controlled to be 0.2-1.0 mol.1-1, and modifiers such as 0.01-0.1mol.1-1 of Hexamethyl disilazane and the like can be added in the preparation process of the hydrophobic white carbon black. The grain diameter of the prepared white carbon black is 50-350nm and the specific surface area is 100-300m<2>.g-1; and the method has high economic value and the prepared white carbon black has good hydrophobic effect.
Owner:HENAN UNIV OF SCI & TECH
Preparation method and application of heterogeneous Fenton-like catalyst
InactiveCN102909073ALow costEfficient degradationOrganic-compounds/hydrides/coordination-complexes catalystsWaste water treatment from textile industryFiberCarbon fibers
Disclosed are a preparation method and application of heterogeneous Fenton-like catalyst. The preparation method includes the steps of firstly, dissolving complexing agent and metal salt in distilled water to respectively prepare complexing agent and metal salt solutions; secondly dropwise adding the metal salt solution into the complexing agent solution under the action of a magnetic mixer, and mixing for 20-60 after dropwise addition to obtain metal complex solution; and thirdly, impregnating activated carbon fiber in the metal complex solution for 1-24h, and subjecting taken-out activated carbon fiber to distilled water washing and drying to obtain the heterogeneous Fenton-like catalyst. The preparation method is simple, and conditions are mild. Environment-friendly hydrogen peroxide is used as oxidant, no extra ultraviolet light or even visible light is needed, and the heterogeneous Fenton-like catalyst is capable of efficiently degrading organic pollutants such as dye within a wide pH range of 2-10. The heterogeneous Fenton-like catalyst is well repeatable, and secondary pollution of the homogeneous Fenton reagent caused by iron ions is avoided.
Owner:ZHEJIANG SCI-TECH UNIV
Organic/inorganic composite porous isolating membrane, preparation method thereof and electrochemical device
ActiveCN103441230AImprove breathabilityImprove conductivityHybrid capacitor separatorsCell seperators/membranes/diaphragms/spacersPorous coatingInorganic particle
Owner:DONGGUAN AMPEREX TECH +1
Method for preparing large-scale graphene through supercritical carbon dioxide exfoliation
ActiveCN102515155AReduce forceReduce the number of layersGrapheneBulk chemical productionMicrometerGraphite
The invention relates to a method for preparing large-scale graphene through supercritical carbon dioxide exfoliation. Supercritical carbon dioxide is adopted as an exfoliant, a surfactant is adopted as a dispersant, graphite powder and the dispersant are put in an autoclave, the carbon dioxide is pumped in the autoclave and circularly flows in a supercritical state, and then the pressure is reduced quickly to be normal pressure; the process is repeated so that the materials undergo pressure increment and pressure reduction several times; and the layers of the graphene is controlled by controlling the times of pressure increment and pressure reduction, so as to prepare the large scale graphene. Compared with the prior art, the invention has the advantages as follows: large-scale (hundreds of micrometers) high-quality graphene can be prepared; the method belongs to physical exfoliation, the treatment conditions are mild, and the quality of the graphene cannot be damaged; besides, the carbon dioxide used in the method is nontoxic, cheap and easy to obtain, and the technology is simple.
Owner:上海利物盛纳米科技有限公司
Preparation method of star polycarboxylic acid high-performance water reducing agent
ActiveCN102887979AExtended Dionon Design-Structure-PropertyExpanding the theoretical connotation of the design-structure-performance of moleculesWater reducerPollution
The invention relates to a preparation method of a star polycarboxylic acid high-performance water reducing agent. Polybasic alcohol and (methyl) acrylic acid used as main raw materials for esterification are esterified and polymerized to prepare the star polycarboxylic acid high-performance water reducing agent material: the (methyl) acrylic acid and polybasic alcohol used as reactants are esterified under the action of a catalyst to firstly prepare a star polymerizable active terminal, and free-radical polymerization reaction is carried out with unsaturated polyethenoxy ether, molecular weight regulator and unsaturated carboxylic acid monomer under the action of an initiator to prepare the star polycarboxylic acid high-performance water reducing agent. The invention is easy to control, and has the advantages of high polymerization degree, low cost and no pollution; the esterification reaction is carried out form an active core, and the free-radical polymerization is carried out to generate the chain arm, thereby implementing the polycarboxylic acid high-performance water reducing agent in a star molecular structure; and under the condition of common doping amount and low doping amount, the star polycarboxylic acid high-performance water reducing agent has better cement paste flowability and holding capacity than the traditional linear and comb polycarboxylic acid water reducing agents, and has favorable cement adaptability and concrete application performance.
Owner:GUIZHOU DR SHI TECH
Preparation method of colloid of mono-dispersed silver nano particles and nano silver powder and conductive ink thereof
The invention relates to a preparation method of colloid of mono-dispersed silver nano particles and nano silver powder, and conductive ink prepared on the basis of the nano silver powder. The method comprises the following steps of: dropwise adding a reducing agent solution in a constant-flow manner to the mixed solution of silver salt precursor and a dispersant to obtain a reaction system; after reaction is finished, obtaining the colloid of the mono-dispersed silver nano particles; performing centrifugation on the colloid of the mono-dispersed silver nano particles; cleaning the precipitate with a cleaning agent and drying to obtain the nano silver powder; and mixing the nano silver powder, a terpene alcohol compound solvent and auxiliaries to prepare the conductive ink. The method forpreparing the colloid of mono-dispersed silver nano particles provided by the invention has simple and quick process, high product output, mild preparation conditions, and no need of protection of inert gas. The terpene alcohol compound solvent used for preparing the conductive ink can uniformly disperse the nano silver powder and can maintain long-time stability. The terpene alcohol compound solvent can keep the conductive ink and a substrate in a good spread state.
Owner:INST OF CHEM CHINESE ACAD OF SCI
Alkalization modifying method of luffa and use thereof
InactiveCN101239303AEasy to makeImprove performanceOther chemical processesWater/sewage treatment by sorptionWater bathsNatural resource
The present invention provides a luffa alkalization modification method and an application in the metal ion adsorption, belongs to natural high polymer material modification or wastewater disposal technical field. The method is mixing the natural luffa with m moderate NaOH alcohol solution, alkalization under the temperature 25-80 Celsius degree, or alkalization by microwave interval radiation 1-10 min, then obtaining alkalization luffa by reflowing, washing, filtering, drying in the thermostatic waterbath. The luffa comes from variety of natural resources, and biodegradation, and treating process is relatively simple, partly substituting high molecular synthetic material in aspect of the sewage treatment, and having advantages such as friendly to the environment.
Owner:SHANGHAI UNIV
Method for preparing galvanic deposit calcium phosphorus mineralized layer superfine fibre bone material
The invention relates to a method for preparing superfine fiber bone materials of an electrodeposition calcium phosphate mineralized layer, which comprises the following steps: firstly, high-polymer superfine fibers are prepared on the surface of a metal electrode by adoption of electrostatic spinning and taken as an electrochemical deposition template; a layer of bone salt ingredients which are rich in calcium and phosphor is deposited on the surface of the fibers by the constant-voltage or constant-current deposition technology; mineralized superfine fibers are soaked into 0.1 to 1.0 mol per liter of NaOH solution for 1 to 24 hours; mineralized electro spinning fibers are subjected to die stamping into blocks under the pressure of between 10 and 40 MPa; and the porous bone materials with a porosity between 50 and 90 percent and a pore diameter between 50 and 500 micrometers are processed by the salt particle leaching / gas foaming technology, and are used for bone defect restoration after freeze-drying sterilization. The porous bone materials prepared by the method have better biocompatibility; and the electrochemical deposition technology can prepare organic-inorganic composite materials with higher bone salt content within a shorter period; and the preparation time is short and the preparation conditions are mild.
Owner:DONGHUA UNIV
Preparation method of nano-particle@minisize metal organic frame material
InactiveCN107349964AAvoid reunionShort diffusion pathMaterial nanotechnologyOrganic-compounds/hydrides/coordination-complexes catalystsMetal-organic frameworkBiological imaging
The invention relates to a preparation method of a nano-particle@minisize metal organic frame material. The preparation method comprises the following steps of 1, preparing nano-particles modified by polyvinylpyrrolidone; 2, adding the obtained nano-particles into an MOF growth reaction solution, the addition amount of an adjusting agent is controlled, and the nano-particle@minisize metal organic frame material is obtained. The method is simple and easy to implement, mild in condition and high in applicability, and the prepared nano-particle@minisize metal organic frame material can effectively prevent nano-particle aggregation, meanwhile has the advantages of being good in size selectivity, and short in diffusion range between the surface of the metal organic framework and the active center of nano-particles, and has the wide application prospect in the fields of catalysis, biological imaging and the like.
Owner:BEIJING UNIV OF CHEM TECH
Modified polypropylene master batch, melt-blow cloth, preparation method and application thereof
InactiveCN107286473ALarge specific surface areaHigh conductivityFiltration separationNon-woven fabricsGraphene derivativesAntioxidant
The invention provides a modified polypropylene master batch, melt-blow cloth, a preparation method and an application thereof. The modified polypropylene master batch is mainly produced from, by weight, 77-90% of polypropylene, 5-20% of a graphene material and 1-5% of an additive. The graphene material includes any one or more of graphene, graphene oxide and graphene derivative. The additive includes any one or more of a coupling agent, a dispersant and an antioxidant and preferably includes the coupling agent, the dispersant and the antioxidant. The modified polypropylene master batch, when being used for manufacturing the melt-blow cloth, not only improves antibacterial and electrification property but also increases the filtering efficiency and dust capacity of the melt-blow cloth.
Owner:SHANDONG SHENGQUAN NEW MATERIALS CO LTD
Multifunctional double-layer core-shell structure magnetic nano particle, preparation method and application thereof
InactiveCN101923932ARapid enrichmentRapid separation and purificationInorganic non-active ingredientsInorganic material magnetismMagnetite NanoparticlesSuperparamagnetism
The invention relates to a multifunctional double-layer core-shell structure magnetic nano particle. In the invention, a magnetic nano particle with a particle size of 1-300 nm is used as a core and coated with a double-layer shell consisting of a SiO2 layer with a thickness of 1-200 nm and a hydrolyzed silane coupling agent layer is 1-100 nm thick and comprises one or more multifunctional groups; the particle size and the shell layer thickness can be controlled through regulating the volumes, the weight ratios and the reaction time of the magnetic core, a silicon dioxide precursor, a silane coupling agent and a catalyst in a preparation process; the total particle size of the nano particle can be as small as 5-50 nm and as large as 700-800 nm; the nano particle can have superparamagnetism, paramagnetism and ferromagnetism according to the change of the magnetic core particle size; and one or more bioactive molecules can be connected into the shell layer of the magnetic nano particle or to the surface of the shell layer through a chemical method or a physical method. The invention also provides a preparation method of the multifunctional double-layer core-shell structure magnetic nano particle and application thereof. The particle preparation method has the advantages of simplicity, moderate condition, low cost and easy realization of industrial production. The nano particle can obtain different functions through connecting different bioactive molecules and can be applied to the fields of protein enrichment, biological detection, separation and purification, targeted drug carriers, cell imaging and medical imaging.
Owner:NANJING UNIV
CsPbX3 inorganic perovskite quantum dot light-emitting diode (LED) prepared through solution method
ActiveCN105206718ASimple preparation processMild conditionsSemiconductor devicesEvaporationVisible spectral range
The invention discloses a CsPbX3 inorganic perovskite quantum dot light-emitting diode (LED) prepared through a solution method. ITO glass is spin-coated with a PEDOT:PSS hole injection layer, then a hole transmission layer and metal halide perovskite quantum dots are spin-coated, and an electron transmission layer is deposited through heat evaporation or magnetron sputtering; afterwards, metal electrodes of the LED are deposited through heat evaporation, and the CsPbX3 inorganic perovskite quantum dot LED which gives out light evenly is obtained. The light-emitting color of the prepared quantum dot LED can be adjusted by changing the halogen ratio of a quantum dot light-emitting layer material and can cover the entire visible spectrum range.
Owner:NANJING UNIV OF SCI & TECH
Ball milling preparation method of graphene
The invention provides a ball milling preparation method of graphene. The ball milling preparation method comprises the following steps of: putting a mixture of graphite carbon and an alkyl six-membered aromatic ring or condensed ring polyether nonionic surfactant in the mass-volume ratio of 1: 2 to 1: 15, and deionized water in a ball milling jar, and fixing the ball milling jar on a ball mill for ball milling at a rotating speed ranging from 200 to 500 rpm for 5-30 hours; next, transferring the ball milled mixture to deionized water for centrifuging at a rotating speed ranging from 3000 to 8000 rpm for 10-30 minutes, and then obtaining a black upper-layer colloidal suspension for preparing graphene aqueous solutions with different concentrations. The graphene produced by the ball milling preparation method provided by the invention is dispersed in aqueous solutions and is high in concentration; the surfactant can be easily removed by using ethanol, which is friendly to environment and advantageous for wide application of graphene. The adopted ball milling equipment is simple, convenient to operate and safe to run; no new surface oxygen-containing functional group defect is introduced by ball milling; furthermore, the ball milling preparation method is mild and simple in preparation process, and high in yield.
Owner:CENT SOUTH UNIV
Wear-resistant optical layers and moulded bodies
ActiveUS20060159923A1Mild conditionsIncrease variabilityMaterial nanotechnologyImpression capsHydrogenWear resistant
A composition comprising a blocked and / or unblocked isocyanate compound and surface-modified nanoscale solid particles that comprise on the surface thereof organic radicals which comprise groups with an active hydrogen or precursors of such groups.
Owner:INST FUR NEUE MATERIALIEN GEMEINNUTZIGE GMBH
Preparation method of nanofluid for improving oil recovery
ActiveCN103937478AIncrease profitGood dispersionFluid removalDrilling compositionActive agentSurface-active agents
The invention discloses a preparation method of a nanofluid for improving oil recovery. The preparation method comprises the following steps: taking 2.0-4.0g of nanopowder, adding 60-80mL of deionized water to the nanopowder and carrying out ultrasonic dispersion at a room temperature for 30-60 minutes; dissolving 2.0g of a silane coupling agent in absolute ethyl alcohol; mixing the nano-base solution with the ethanol solution of the silane coupling agent in a three-neck boiling flask, heating while stirring to the range of 70 to 75 DEG C, reacting for 4-6 hours, filtering, washing by using an anhydrous solvent a plurality of times, and drying in a vacuum drying box at 60-70 DEG C for 12 hours to obtain modified nanoparticles; putting 0.1-0.5g of nanoparticles in the three-neck boiling flask, adding 200-300mL of water, heating to the range of 60-75 DEG C by use of a water bath, mixing a surfactant with PEG (Poly Ethylene Glycol), adding 100mL of mixed solution of the surfactant and the PEG, mechanically stirring for 6-8 hours, washing the stirred dispersion 2-3 times, adjusting the pH value to the range of 8-9, and adding deionized water to 1L, thereby obtaining the water-based nanofluid.
Owner:NORTHEAST GASOLINEEUM UNIV
Polypeptide medicament sustained release microsphere or microcapsule preparation with uniform grain size and preparation method thereof
ActiveCN101559041ASmall particle sizeRegulated release ratePeptide/protein ingredientsMetabolism disorderMicrosphereMedicine
The invention discloses a polypeptide medicament sustained release microsphere or a microcapsule preparation with uniform grain size, a preparation method thereof and application. The average grain size of the microsphere or the microcapsule preparation is between 50 nanometers and 100 microns, and the grain size distribution coefficient CV value is less than 20 percent. The polypeptide medicament has a definite structure, has functions of therapy or adjuvant therapy of type-2 diabetes, and is preferably one or more of GLP-1, Exenatide, Exendin-4 and derivatives and analogs thereof. The microsphere or the microcapsule preparation uses a microsphere or a microcapsule with uniform grain size as a substrate to prepare the polypeptide medicament into a sustained release preparation through an embedding mode, and by changing the grain size of the microsphere or the microcapsule, the sustained release cycle is adjustable between one week and one month, and the microsphere or the microcapsule preparation can be applied to the therapy or the adjuvant therapy of the type-2 diabetes and body weight control. Besides, the microsphere or the microcapsule preparation has the advantages of simple preparation process and mild preparation course, and can protect the biological activity of the embedded polypeptide medicament.
Owner:辉粒药业(苏州)有限公司
Method for preparing chitin and its chitosan and chitosan oligosaccharide
InactiveCN101144097ATake advantage ofImprove production conditionsMicroorganism based processesFermentationSolubilityBioreactor
The present invention relates to a method for preparing chitin and chitosan oligosac charide. The method comprises the steps that usual raw materials such as the crust of shrimp and crab, the insect crust or the fungal mycelia, etc. are micronized through the dry process or wet process; the carapace material of the obtained fine powder raw material is decalcified with the chemical process, and then is defatted and deproteinized with the method of micro-organism compound enzyme coarse enzyme liquid co-enzymolysis, and the insect and fungus fine powder thereof is directly defatted and deproteinized; a whole cell immobilizing bioreactor of a chitin deacetylase high-yield producing strain is prepared, to perform the circulatory deacetylation to the chitin and then obtain chitosan with corresponding degree of deacetylatoion; obligate anaerobic acid-producing bacterium and high-yield producing chitosan bacterium are utilized, the chitosan is submerged and fermented in the liquid, to obtain chitosan oligosaccharide with high water solubility. The present invention has the advantages that the method is helpful to fully utilize the resources, and makes the waste to the worth, at the same time, the default of the manufacturing process of the chemical process can be avoided, the production efficiency is improved, the energy is saved, the consumption is reduced, the byproduct with corresponding high value added can be produced, the comprehensive economic benefits of the relative secondary industry are obviously improved, the industrial development is promoted, and the multi-win effect is attained.
Owner:重庆百奥帝克微生态科技有限公司
Super-hydrophobic textile prepared from modified polyester fiber based on dopamine and preparation method thereof
The invention provides a super-hydrophobic textile prepared from a modified polyester fiber based on dopamine and a preparation method thereof, the preparation method comprises the steps that a polyester fabric is soaked into different buffer solutions in sequence, nano-particles produced by dopamine polymerization are deposited on the fiber surface adhered with polydopamine, the fiber is finally treated by a low surface energy modifier to obtain the super-hydrophobic textile; the buffer solution at east comprises two kinds of different buffer solutions, namely, a phosphate buffer solution of the dopamine and a trihydroxymethyl aminomethane buffer solution of the dopamine. According to the super-hydrophobic textile prepared from the modified polyester fiber based on the dopamine and the preparation method thereof, the characteristic that the sizes of polydopamine nano particles produced by dopamine polymerization in different buffer solution systems is utilized, autoxidation polymerization of dopamine is utilized to be adhered to and deposited on the fiber surface to form a rough structure required by the super-hydrophobic surface, and the super-hydrophobic surface can be prepared after the rough structure is treated by the low surface energy; the reaction process is simple, the condition is mild; and the water drop contact angle of the super-hydrophobic surface prepared by the invention is more than 150 degree.
Owner:SHAANXI UNIV OF SCI & TECH
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