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78 results about "Reactive deposition" patented technology

Interface control for film deposition by gas-cluster ion-beam processing

Methods are disclosed for gas-cluster ion-beam deposition of thin films on silicon wafers rendered free of native oxides by termination of the surface bonds and subsequent reactive deposition. Hydrogen termination of the surface of silicon renders it inert to reoxidation from oxygen-containing environmental gasses, even those found as residue in vacuum systems, such as those used to deposit films. Nitrogen termination improves the interface with overlying metal-oxide thin films. The film is formed in intimate contact with the silicon crystal surface forming a nearly ideal interface.
Owner:JDSU OPTICAL

Reactive deposition for the formation of chip capacitors

Methods for the production of ceramic chip capacitors include the deposition of at least two layers of electrical conductor and at least one layer of a dielectric between electrical conducting layers. The compositions in the dielectric layer are deposited from a flow in which flowing reactants react to form particles in a reaction driven by light at a light reaction zone. In some embodiments, a plurality of dielectric layers is deposited. Suitable dielectric materials include barium titanate. A collection of barium titanate particles can be formed in the coating process having an average diameter less than about 90 nanometers. Thus, ceramic chip capacitors can be formed with barium titanate particles having an average diameter less than about 90 nanometers.
Owner:NANOGRAM

Lithium titanate composite electrode material with fluoride surface coating layer and preparation method thereof

The invention discloses a lithium titanate composite electrode material with a fluoride surface coating layer and a preparation method thereof. The coating layer of the composite electrode material is fluoride (MxFy) of one or more types of metals, wherein M is lithium, magnesium, strontium, barium, aluminum or lead, the thickness of the coating layer is 0.1-100nm, the coating layer accounts for 0.01-20% of the mass ratio of the composite electrode material, and lithium titanate is a crystal material with a spinel structure. According to the preparation method, a water-soluble salt of M and ammonium fluoride are used as raw materials, and n the surface of lithium titanate is in situ coated with fluoride through in situ chemical reaction deposition in combination with inert atmosphere heat treatment. The coating layer of the composite electrode material can shield active spots on the surface of the lithium titanate electrode material so that the lithium titanate electrode material can not bloat and has the advantages of good rate performance, high capacity retention ratio and excellent cycle performance; and the lithium titanate composite electrode material is simple and convenient in process, low in cost and suitable for large-scale production and has a wide market prospect.
Owner:SOUTHWEST PETROLEUM UNIV

Niobium-doped titanium dioxide coated glass and preparation method thereof

The invention discloses a preparation method of a niobium-doped titanium dioxide coated glass. The preparation method adopts a chemical vapor deposition method, and comprises the following steps of (1) mixing a titanium source and a niobium source, so as to obtain a source material mixture; or, mixing the titanium source, the niobium source and a solvent, so as to obtain the source material mixture; (2) converting the source material mixture into vapor-phase reaction gas by an air bubbling or evaporating and gasifying method; (3) carrying the vapor-phase reaction gas to the pretreated high-temperature glass substrate by carrying gas, reacting, and depositing, so as to obtain the niobium-doped titanium dioxide coated glass. The prepared niobium-doped titanium dioxide coated glass has the advantages that the bonding force of a film layer is excellent, and the physical stability and chemical stability are good; the thin film is made of anatase-phase titanium dioxide, and the mass concentration of the niobium-doped material is 0.5 to 15%; the photo-induced super-hydrophilicity is realized; the niobium-doped titanium dioxide coated glass is prepared at high temperature, and is suitablefor the low-cost preparation of large-area coated film; the cleaning is easy, and the stain-resistant property is realized.
Owner:ZHEJIANG UNIV

Chromium carbide modified iron-based metal bipolar plate and preparation method thereof

The invention provides a chromium carbide modified iron-based metal bipolar plate for a fuel battery and a preparation method thereof. An iron-based alloy metal plate is subjected to surface modification by using plasma carburization and a combined thermal reactive deposition and diffusion surface modification process. The modified surface of the metal plate is a chromium carbide diffusion layer with high conductivity and corrosion resistance, the thickness is 1-30 microns, and the corrosion speed is lower than 10 microamperes/square centimeter. When the pressure is 150-200 N/square centimeter, the contact resistance is 10-20 micro-ohms*square centimeter, and a chromium carbide diffusion layer is made of Cr3C2 and/or Cr7C3 and/or Cr23C6. According to the method provided by the invention, the corrosion resistance of the metal bipolar plate can be obviously improved in a condition of ensuring the intensity of the bipolar plate and not influencing battery properties of the bipolar plate. The chromium carbide diffusion layer with the modified surface and a base body are in metallurgical combination. Furthermore, components of the chromium carbide diffusion layer can be controlled by adjusting isothermal diffusion temperature and time.
Owner:DALIAN JIAOTONG UNIVERSITY

Production device for silicon oxide film and production method thereof

The invention provides a production method of silicon oxide, and the production method comprises the following steps of: warming a heating device, setting a to-be-filmed substrate, and introducing nitrogen to remove the impurity gas in the reaction chamber; bringing the reaction precursor ethyl silicate into the reaction chamber by the nitrogen carrier gas; conveying the oxygen in an oxygen source to an ozone generator, conveying the generated ozone into the reaction chamber; performing reactive deposition on the surface of the to-be-filmed substrate by the precursor ethyl silicate and the ozone in the reaction chamber, so as to prepare the silicon oxide film. In the production method of the silicon oxide film provided by the invention, a thermal reaction mode is used, plasma damage of the to-be-filmed substrate is avoided, and the production device of the silicon oxide film is simple, the technological process is easy to control, and the deposition temperature of the silicon oxide film is lowered effectively. Moreover, the silicon oxide film is deposited on the top layer of the Low-E glass, the properties, such as acid and alkali corrosion resistance, oxidation resistance, heat and humidity resistance and high temperature resistance, of the functional glass are improved greatly.
Owner:林嘉佑

AlCrSiN/VSiN multi-layer nano-coating and preparation method thereof

The invention provides a preparation method of an AlCrSiN / VSiN multi-layer nano-coating. The preparation method of the AlCrSiN / VSiN multi-layer nano-coating comprises the following steps that (a) cathode electric arcs are used for achieving evaporative deposition of an Al50Cr50N transition layer on the surface of a matrix; and (b) a VSi target is sputtered through a high-power pulse magnetic control power supply, a direct-current arc power supply is used for achieving cathode evaporation of an AlCrSi target, and reactive deposition of the AlCrSiN / VSiN multi-layer nano-coating is achieved in the mixed atmosphere of Ar gas and N2 gas. According to the preparation method of the AlCrSiN / VSiN multi-layer nano-coating, the electric arc ion plating technique and the high-power pulse magnetron sputtering technique are used in a quasi coupling mode, so that the element V is prevented from being diffused outwards rapidly through a multi-layer nanostructure and a composite nanostructure, the high-temperature mechanical performance, the high temperature resistance and the oxidization resistance of the coating are improved, and the diffusion reaction between titanium and the coating at a high temperature is restrained; and under the synergistic effect of the multi-layer nanostructure, the composite nanostructure and the doped element V, the surface of the AlCrSiN / VSiN multi-layer coating has high temperature oxidization resistance, self-lubrication performance and high abrasion resistance, and the AlCrSiN / VSiN multi-layer nano-coating which is of the multi-layer nanostructure and has high bonding force, excellent temperature resistance and self-lubrication performance is finally obtained.
Owner:GUANGDONG UNIV OF TECH

Method for preparing surface SiC-C coating of carbon material in graphite-heating-element furnace

InactiveCN106915975AImprove bindingPlay a crack deflection roleChemical vaporsHeating furnace
The invention relates to a method for preparing a surface laminated SiC-C coating of a carbon material in a graphite-heating-element heating furnace. The method is characterized by comprising the steps: vacuumizing the graphite-heating-element heating furnace subjected to high-temperature treatment, and heating the graphite-heating-element heating furnace to 1,100 DEG C to 1,250 DEG C; then, introducing argon gas into the heating furnace, starting to introduce hydrogen gas into the heating furnace 15 to 30 minutes later, and starting to introduce trichloromethylsilane (MTS) into the heating furnace 15 to 30 minutes later when the internal environment of the furnace is stable; carrying out a chemical vapor deposition reaction in the furnace for 5 to 10 hours, then, stopping to introduce trichloromethylsilane, starting to introduce propylene gas into the heating furnace 15 to 30 minutes later, carrying out a gas-phase reaction to pyrolyze a carbon interface layer, and continuing to introduce the hydrogen gas and the argon gas according to original gas flow; stabilizing the furnace inside temperature to 900 DEG C to 1,100 DEG C, stopping to introduce the propylene gas 1 to 5 hours later, introducing trichloromethylsilane into the heating furnace again 15 to 30 minutes later, and continuing to carry out a reaction, so as to deposit an SiC coating; and carrying out repeated deposition on the SiC coating and the C interface layer for 5 to 10 times in this way, thereby obtaining the surface laminated SiC-C coating of the carbon material in the graphite-heating-element heating furnace. The chemical vapor deposited silicon carbide coating and the pyrolytic carbon layer are uniform and dense, and the protection and service life of the carbon material caused by the coating is prolonged due to the laminated structure.
Owner:SUZHOU HONGJIU AVIATION THERMAL MATERIALS TECH CO LTD

Method for low-temperature reactive sputtering deposition of nanometer alpha-Al2O3 coating

The invention belongs to the technical field of metal oxide coatings and discloses a method for low-temperature reactive sputtering deposition of a nanometer alpha-Al2O3 coating. The method comprisesthe following steps: manufacturing Al powder and alpha-Al2O3 powder into a composite material through a powder metallurgy method; after cutting the composite material to reach the size required for equipment, mounting the composite material of the required size on a target station for radio frequency magnetron sputtering as a deposition target material, and mounting a workpiece substrate on a sample table in a deposition cavity; after removing residual steam in the deposition cavity, vacuumizing to achieve base pressure, and then injecting a gas mixture of Ar and O2 for pre-oxidation treatment; and adjusting the partial pressure of O2 in the gas mixture of Ar and O2 to reach the range of 15% to 25%, adjusting the temperature of the workpiece substrate to reach the range of 550 DEG C to 750DEG C, starting a radio frequency magnetron sputtering film coating system, and starting reactive deposition so as to obtain the nanometer alpha-Al2O3 coating. The nanometer alpha-Al2O3 coating obtained through the method disclosed by the invention is of a nanocrystalline structure, is high in toughness, can be firmly combined with the workpiece substrate, and has a stable alpha-phase structure at relatively low temperature.
Owner:SOUTH CHINA UNIV OF TECH +1
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